3-(Boc-amino)-2-piperidone

Product Name: 3-(Boc-amino)-2-piperidone
CAS No.: 99780-98-0
Chemical Name: 3-(Boc-amino)-2-piperidone
Synonyms: 3-Boc-aMino-2-piperidinone;3-(Boc-amino)-2-piperidone;_x000D_3-(Boc-amino)-2-piperidone;tert-Butyl (2-oxopiperidin-3-yl)carbaMate;tert-butyl N-(2-oxopiperidin-3-yl)carbamate;(+/-)-3-<(tert-butoxycarbonyl)amino>-2-piperidone;1,1-Dimethylethyl?N-(2-oxo-3-piperidinyl)carbamate;Carbamic acid, N-(2-oxo-3-piperidinyl)-, 1,1-dimethylethyl ester
CBNumber: CB22500771
Molecular Formula: C10H18N2O3
Formula Weight: 214.26
MOL File: 99780-98-0.mol

More

Less

3-(Boc-amino)-2-piperidone Property

Boiling point:: 405.6±34.0 °C(Predicted)
Density: 1.11±0.1 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 11.05±0.20(Predicted)
Appearance: White to off-white Solid

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P501Dispose of contents/container to..…

More

Less

N-Bromosuccinimide Price

TRC

Product number: B621138
Product name: 3-(Boc-amino)-2-piperidone
Packaging: 500mg
Price: $90
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0299986
Product name: 3-(BOC-AMINO)-2-PIPERIDONE
Purity: 95.00%
Packaging: 5MG
Price: $496.39
Updated: 2021/12/16

AK Scientific

Product number: 7000AC
Product name: tert-Butyl(2-oxopiperidin-3-yl)carbamate
Packaging: 1g
Price: $144
Updated: 2021/12/16

Crysdot

Product number: CD11000199
Product name: tert-Butyl(2-oxopiperidin-3-yl)carbamate
Purity: 95+%
Packaging: 5g
Price: $211
Updated: 2021/12/16

Chemenu

Product number: CM179771
Product name: tert-Butyl(2-oxopiperidin-3-yl)carbamate
Purity: 95%
Packaging: 5g
Price: $224
Updated: 2021/12/16

More

Less

3-(Boc-amino)-2-piperidone Chemical Properties,Usage,Production

Synthesis

1892-22-4

24424-99-5

99780-98-0

General procedure for the synthesis of 3-(Boc-amino)-2-piperidinone from 3-aminopiperidin-2-one and di-tert-butyl dicarbonate: To a 500 mL round-bottomed flask were added 3-aminopiperidin-2-one (10 g, 87.61 mmol, 1.00 equiv), methanol (200 g, 6.24 mol, 71.25 equiv), and triethylamine (20 mL). A solution of di-tert-butyl dicarbonate (20 g, 91.64 mmol, 1.05 equiv) in methanol (100 mL) was added slowly and dropwise with stirring at 0 °C. The reaction mixture was stirred at room temperature overnight. After completion of the reaction, the mixture was concentrated under vacuum. The crude product was purified by column chromatography to afford 16 g (85% yield) of 3-(Boc-amino)-2-piperidone as a white solid.

References

[1] Patent: WO2017/75056, 2017, A1. Location in patent: Paragraph 0410
[2] Journal of Medicinal Chemistry, 1986, vol. 29, # 2, p. 251 - 260
[3] Farmaco, 2004, vol. 59, # 4, p. 271 - 277
[4] Patent: WO2004/98589, 2004, A1. Location in patent: Page 163

3-(Boc-amino)-2-piperidone Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

3-(Boc-amino)-2-piperidone Suppliers

China 36 India 2 United States 6 Global 44

Bide Pharmatech Ltd.

Tel: 400-164-7117 13681763483
Fax: +86-21-61629029
Email: product02@bidepharm.com
Country: China
ProdList: 39966
Advantage: 60

ShangHai AmK Pharmaceutical Technology Co., Ltd.

Tel: 微信 17321281695 18019252918
Fax: 17321281695
Email: sale@amkchem.com
Country: China
ProdList: 15136
Advantage: 55

Hangzhou J&H Chemical Co., Ltd.

Tel: 0571-87396432
Fax: 0571-87396431
Email: sales@jhechem.com
Country: China
ProdList: 14912
Advantage: 59

Accela ChemBio Inc.

Tel: +1(858) 699-3322
Fax: +1(858) 876-1948
Email: marketing@accelachem.com
Country: United States
ProdList: 6024
Advantage: 65

Nanjing YaoCheng Pharmaceutical Co., Ltd.

Tel: 025-57043319 15261831516
Fax: 025-57043319
Email: 307514552@qq.com
Country: China
ProdList: 251
Advantage: 50

Shanghai YuanYe Biotechnology Co., Ltd.

Tel: 021-61312847; 18021002903
Fax: QQ:3008007432
Email: 3008007409@qq.com
Country: China
ProdList: 71826
Advantage: 60

Shanghai JingSi Biological Technology Co., Ltd

Tel: 18221840760
Fax: QQ:2990760589
Email: 2990760589@qq.com
Country: China
ProdList: 241
Advantage: 58

JiangYin Ruisheng Chemical Co., Ltd.

Tel: 13003356808
Fax: QQ:1485751188
Email: 1485751188@qq.com
Country: China
ProdList: 403
Advantage: 55

Amatek Scientific Co. Ltd.

Tel: 0512-56316828
Fax: 0512-56316826
Email: info@amateksci.com
Country: China
ProdList: 28785
Advantage: 58

Aikon International Limited

Tel: 025-66061636 18013972705
Fax: (3)02557626880
Email: qqyang@aikonchem.com
Country: China
ProdList: 15814
Advantage: 58

More

Less

View Lastest Price from 3-(Boc-amino)-2-piperidone manufacturers

Career Henan Chemical Co

Product: 3-(Boc-amino)-2-piperidone 99780-98-0
Price: US $0.01/KG
Min. Order: 1KG
Purity: 98%; 99%
Supply Ability: 1kg; 10kg; 25kg
Release date: 2020-01-07

99780-98-0, 3-(Boc-amino)-2-piperidoneRelated Search:

3-(Boc-amino)-2-piperidone

tert-Butyl (2-oxopiperidin-3-yl)carbaMate

3-Boc-aMino-2-piperidinone

(+/-)-3-<(tert-butoxycarbonyl)amino>-2-piperidone

tert-butyl N-(2-oxopiperidin-3-yl)carbamate

Carbamic acid, N-(2-oxo-3-piperidinyl)-, 1,1-dimethylethyl ester

_x000D_3-(Boc-amino)-2-piperidone

1,1-Dimethylethyl?N-(2-oxo-3-piperidinyl)carbamate

99780-98-0