5-Bromo-6-chloro-1H-indole

Product Name: 5-Bromo-6-chloro-1H-indole
CAS No.: 122531-09-3
Chemical Name: 5-Bromo-6-chloro-1H-indole
Synonyms: 5-bromo-6-chloro-indole;5-bromo-6-chloro-1H-indole;1H-Indole, 5-broMo-6-chloro-;5-bromo-6-chloro-1H-indole(5-?Bromo-?6-?Chloroindole)
CBNumber: CB22504739
Molecular Formula: C8H5BrClN
Formula Weight: 230.49
MOL File: 122531-09-3.mol

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5-Bromo-6-chloro-1H-indole Property

Boiling point:: 358℃
Density: 1.772
Flash point:: 170℃
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 15.14±0.30(Predicted)
Appearance: White to off-white Solid
InChI: InChI=1S/C8H5BrClN/c9-6-3-5-1-2-11-8(5)4-7(6)10/h1-4,11H
InChIKey: SMZUROGBNBCCPT-UHFFFAOYSA-N
SMILES: N1C2=C(C=C(Br)C(Cl)=C2)C=C1

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B682438
Product name: 5-Bromo-6-chloro-1H-indole
Packaging: 0.25g
Price: $55
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB29903
Product name: 5-Bromo-6-chloro-1H-indole
Packaging: 2g
Price: $100
Updated: 2021/12/16

AK Scientific

Product number: J96365
Product name: 5-Bromo-6-chloro-1H-indole
Packaging: 100mg
Price: $10
Updated: 2021/12/16

Matrix Scientific

Product number: 091920
Product name: 5-Bromo-6-chloro-1H-indole
Purity: 95+%
Packaging: 250mg
Price: $198
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB29903
Product name: 5-Bromo-6-chloro-1H-indole
Packaging: 5G
Price: $200
Updated: 2021/12/16

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5-Bromo-6-chloro-1H-indole Chemical Properties,Usage,Production

Uses

5-Bromo-6-chloro-1H-indole was used in the study to prepare indole derivatives as intermediates for agrochemicals and drugs.

Synthesis

29682-39-1

1826-67-1

122531-09-3

Under nitrogen protection, 1-bromo-2-chloro-4-nitrobenzene (57.4 g, 0.243 mol) was dissolved in tetrahydrofuran (THF, 500 mL) and cooled to -40°C. At this temperature, vinylmagnesium bromide (1 M solution of THF, 728 mL, 0.728 mol) was added slowly and dropwise. After the dropwise addition was completed, the reaction mixture was kept stirred at -40°C for 1 hr. Subsequently, the reaction was quenched by addition of aqueous ammonium chloride (NH4Cl) and gradually warmed to room temperature. The reaction mixture was extracted with ethyl acetate, the organic layers were combined, dried over anhydrous magnesium sulfate (MgSO4), filtered and concentrated. The crude product was purified by column chromatography (using 5-bromo-6-chloro-1H-indole as reference) to afford the target product 5-bromo-6-chloro-1H-indole (8.40 g, 15% yield).

References

[1] Patent: KR101601357, 2016, B1. Location in patent: Paragraph 0285-0287

5-Bromo-6-chloro-1H-indole Preparation Products And Raw materials

Raw materials

Preparation Products

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5-Bromo-6-chloro-1H-indole Suppliers

China 127 India 3 United Kingdom 1 United States 5 Global 136

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View Lastest Price from 5-Bromo-6-chloro-1H-indole manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 5-bromo-6-chloro-indole 122531-09-3
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-10-13

Career Henan Chemical Co

Product: 5-bromo-6-chloro-indole 122531-09-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: KG/T
Release date: 2019-12-18

122531-09-3, 5-Bromo-6-chloro-1H-indoleRelated Search:

5-bromo-6-chloro-indole

1H-Indole, 5-broMo-6-chloro-

5-bromo-6-chloro-1H-indole

5-bromo-6-chloro-1H-indole(5-?Bromo-?6-?Chloroindole)

122531-09-3