3-(Boc-amino)-3-methylpip...
- Product Name
- 3-(Boc-amino)-3-methylpip...
- CAS No.
- 169750-96-3
- Chemical Name
- 3-(Boc-amino)-3-methylpip...
- Synonyms
- 3-(Boc-amino)-3-methylpip...;3-(Boc-aMino)-3-Methylpiperidine;3-Amino-3-methylpiperidine, 3-BOC protected;tert-Butyl 3-methylpiperidin-3-yl-carbamate;tert-butyl n-(3-methylpiperidin-3-yl)carbamate;(3-Methyl-piperidin-3-yl)-carbamic acid tert-butyl ester;(3-Methyl-3-piperidinyl)carbamic acid 1,1-dimethylethyl ester;Carbamic acid, N-(3-methyl-3-piperidinyl)-, 1,1-dimethylethyl ester;tert-Butyl (3-methylpiperidin-3-yl)carbamate, 3-[(tert-Butoxycarbonyl)amino]-3-methylpiperidine
- CBNumber
- CB22525095
- Molecular Formula
- C11H22N2O2
- Formula Weight
- 214.3
- MOL File
- 169750-96-3.mol
3-(Boc-amino)-3-methylpip... Property
- Boiling point:
- 308.4±31.0 °C(Predicted)
- Density
- 1.01±0.1 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 12?+-.0.20(Predicted)
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B630050
- Product name
- 3-(Boc-amino)-3-methylpiperidine
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- Y1662
- Product name
- 3-(Boc-amino)-3-methylpiperidine
- Packaging
- 1g
- Price
- $167
- Updated
- 2021/12/16
- Product number
- Y1662
- Product name
- 3-(Boc-amino)-3-methylpiperidine
- Packaging
- 5g
- Price
- $402
- Updated
- 2021/12/16
- Product number
- CHM1052023
- Product name
- TERT-BUTYL N-(3-METHYLPIPERIDIN-3-YL)CARBAMATE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $450.59
- Updated
- 2021/12/16
- Product number
- 4H51-1-2V
- Product name
- 3-Amino-3-methylpiperidine, 3-Boc protected
- Packaging
- 1g
- Price
- $525
- Updated
- 2021/12/16
3-(Boc-amino)-3-methylpip... Chemical Properties,Usage,Production
Synthesis
1196506-86-1
169750-96-3
General procedure for the synthesis of tert-butyl (3-methylpiperidin-3-yl)carbamate from the compound (CAS:1196506-86-1): benzyl 3-((tert-butoxycarbonyl)amino)-3-methylpiperidine-1-carboxylate (78 mg, 0.22 mmol, prepared according to the method described in WO09/140320) was dissolved in EtOH (5 mL) , which was degassed by bubbling N2 (g) into the solution for 10 min. Pd/C (10 wt%, 24 mg, 0.022 mmol) was added. A gas bladder attached to a three-way cork filled with H2 was connected to the flask. The flask was evacuated and backfilled with H2 (repeated 3 times). The mixture was stirred at room temperature for 2 hours. Degassing was again carried out by bubbling N2 (g) into the solution for 10 min, followed by filtration through diatomaceous earth. The filtrate was concentrated to give racemic-tert-butyl (3-methylpiperidin-3-yl) carbamate (42 mg, 0.20 mmol, 88% yield) as a clear, colorless oil.MS (ESI, cationic) m/z: 215.1 (M + 1).
References
[1] Patent: WO2012/148775, 2012, A1. Location in patent: Page/Page column 124; 125
[2] Patent: WO2009/140320, 2009, A1. Location in patent: Page/Page column 73
3-(Boc-amino)-3-methylpip... Preparation Products And Raw materials
Raw materials
Preparation Products
3-(Boc-amino)-3-methylpip... Suppliers
- Tel
- --
- Fax
- --
- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
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View Lastest Price from 3-(Boc-amino)-3-methylpip... manufacturers
- Product
- tert-butyl (3-methylpiperidin-3-yl)carbamate 169750-96-3
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2020-01-09