14-HydroxyMyristic acid
- Product Name
- 14-HydroxyMyristic acid
- CAS No.
- 17278-74-9
- Chemical Name
- 14-HydroxyMyristic acid
- Synonyms
- 14-HydroxyMyristic acid;Tetradecanoic acid, 14-hydroxy-;14-Hydroxytetradecanoic acid, 98 +%;14-Hydroxytetradecanoic acid - [H72227]
- CBNumber
- CB22549701
- Molecular Formula
- C14H28O3
- Formula Weight
- 244.37
- MOL File
- 17278-74-9.mol
14-HydroxyMyristic acid Property
- Melting point:
- 86-87 °C(Solv: acetone (67-64-1))
- Boiling point:
- 387.1±15.0 °C(Predicted)
- Density
- 0.970±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 4.78±0.10(Predicted)
- Appearance
- Off-white to light yellow Solid
N-Bromosuccinimide Price
- Product number
- 6904CJ
- Product name
- 14-Hydroxytetradecanoicacid
- Packaging
- 100mg
- Price
- $208
- Updated
- 2021/12/16
- Product number
- 6904CJ
- Product name
- 14-Hydroxytetradecanoicacid
- Packaging
- 1g
- Price
- $575
- Updated
- 2021/12/16
- Product number
- A209054
- Product name
- 14-Hydroxytetradecanoicacid
- Purity
- 95%
- Packaging
- 1g
- Price
- $382
- Updated
- 2021/12/16
- Product number
- CD13020556
- Product name
- 14-Hydroxytetradecanoicacid
- Purity
- 95+%
- Packaging
- 1g
- Price
- $396
- Updated
- 2021/12/16
- Product number
- A209054
- Product name
- 14-Hydroxytetradecanoicacid
- Purity
- 95%
- Packaging
- 50mg
- Price
- $85
- Updated
- 2021/12/16
14-HydroxyMyristic acid Chemical Properties,Usage,Production
Definition
ChEBI: A long-chain fatty acid that is myristic (tetradecanoic) acid substituted at position 14 by a hydroxy group.
Synthesis
1147745-12-7
17278-74-9
The general procedure for the synthesis of 14-hydroxytetradecanoic acid from the compound (CAS: 1147745-12-7) as a starting material is as follows: a solution of potassium hydroxide (8.60 g, 153 mmol) in water (100 mL) was added to a solution of the above ester (9.20 g, 30.6 mmol) in methanol (100 mL), and the reaction mixture was heated and reacted for 2 days at 60 °C. . After completion of the reaction, the mixture was cooled to room temperature and subsequently washed with hexane (2 x 70 mL) and concentrated under vacuum. Then, concentrated hydrochloric acid (32%, 20 mL, 0.65 mol) was added dropwise and the mixture was extracted with ethyl acetate (2 × 150 mL). The organic layers were combined, dried over anhydrous magnesium sulfate and evaporated to dryness to give 14-hydroxytetradecanoic acid as a white solid. Yield: 7.10 g (95%). Thin layer chromatography (TLC) analysis (silica gel plate, chloroform:methanol = 85:15): rf = 0.50. 1H NMR spectrum (300 MHz, CDCl3, δH): 3.66 (t, J = 6.6 Hz, 2H); 2.36 (t, J = 7.4 Hz, 2H); 1.72-1.52 (m, 4H); 1.29 (bs, 18H).
References
[1] Patent: US2016/289283, 2016, A1. Location in patent: Paragraph 0254; 0255; 0256; 0257
14-HydroxyMyristic acid Preparation Products And Raw materials
Raw materials
Preparation Products
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