2-(Piperidin-4-yl)pyriMidine hydrochloride
- Product Name
- 2-(Piperidin-4-yl)pyriMidine hydrochloride
- CAS No.
- 690261-64-4
- Chemical Name
- 2-(Piperidin-4-yl)pyriMidine hydrochloride
- Synonyms
- 2-(Piperidin-4-yl)pyrimidine, HCl;2-(Piperidin-4-yl)pyriMidine hydrochloride
- CBNumber
- CB22566908
- Molecular Formula
- C9H14ClN3
- Formula Weight
- 199.68056
- MOL File
- 690261-64-4.mol
2-(Piperidin-4-yl)pyriMidine hydrochloride Property
- storage temp.
- Inert atmosphere,Room Temperature
- Appearance
- Off-white to light yellow Solid
Safety
- HS Code
- 2933599590
N-Bromosuccinimide Price
- Product number
- P994178
- Product name
- 2-(Piperidin-4-yl)pyrimidinehydrochloride
- Packaging
- 500mg
- Price
- $265
- Updated
- 2021/12/16
- Product number
- 3H31-5-8S
- Product name
- 2-(Piperidin-4-yl)pyrimidinehydrochloride
- Purity
- 97%
- Packaging
- 250mg
- Price
- $288
- Updated
- 2021/12/16
- Product number
- 076015
- Product name
- 2-(Piperidin-4-yl)pyrimidine hydrochloride
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $357
- Updated
- 2021/12/16
- Product number
- CHM0388601
- Product name
- 2-(PIPERIDIN-4-YL)PYRIMIDINE HYDROCHLORIDE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $505.3
- Updated
- 2021/12/16
- Product number
- 076015
- Product name
- 2-(Piperidin-4-yl)pyrimidine hydrochloride
- Purity
- 95+%
- Packaging
- 500mg
- Price
- $245
- Updated
- 2021/12/16
2-(Piperidin-4-yl)pyriMidine hydrochloride Chemical Properties,Usage,Production
Synthesis
182416-05-3
690261-64-4
General procedure for the synthesis of 2-(piperidin-4-yl)pyrimidine hydrochloride from tert-butyl 4-(pyrimidin-2-yl)piperidine-1-carboxylate: tert-butyl 4-(pyrimidin-2-yl)piperidine-1-carboxylate prepared in step A (4.64 g, 17.6 mmol) was dissolved in dioxane solution (50 mL) of 4N HCl and stirred for 2.25 h at room temperature. Upon completion of the reaction, the reaction mixture was concentrated to afford 4.16 g of 2-(piperidin-4-yl)pyrimidine hydrochloride in 100% yield without further purification. The product was characterized by 1H NMR (500 MHz, CD3OD): δ 8.95 (d, J = 5.5 Hz, 2H), 7.60 (t, J = 5.0 Hz, 1H), 3.53 (dt, J = 13.0, 3.5 Hz, 2H), 3.35 (tt, J = 4.0, 11.0 Hz, 1H), 3.20 (br t, J = 13.8 Hz, 2H), 2.30 (br d, J = 14.0 Hz, 2H), 2.11-2.20 (m, 2H).ESI-MS analysis: calculated value C9H13N3 [M+H]+ 163, measured value 164 (M+H).
References
[1] Patent: WO2004/41777, 2004, A2. Location in patent: Page 48
[2] Patent: WO2004/94371, 2004, A2. Location in patent: Page 72
[3] Patent: US2008/81803, 2008, A1. Location in patent: Page/Page column 31
2-(Piperidin-4-yl)pyriMidine hydrochloride Preparation Products And Raw materials
Raw materials
Preparation Products
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