ChemicalBook > CAS DataBase List > Methyl 4-broMo-1-Methyl-1H-iMidazole-2-carboxylate
Methyl 4-broMo-1-Methyl-1H-iMidazole-2-carboxylate
- Product Name
- Methyl 4-broMo-1-Methyl-1H-iMidazole-2-carboxylate
- CAS No.
- 864076-05-1
- Chemical Name
- Methyl 4-broMo-1-Methyl-1H-iMidazole-2-carboxylate
- Synonyms
- methyl 4-bromo-1-methyl-imidazole-2-carboxylate;Methyl 4-broMo-1-Methyl-1H-iMidazole-2-carboxylate;4-bromo-1-methyl-1H-Imidazole-2-carboxylic acid methyl ester;1H-Imidazole-2-carboxylic acid, 4-bromo-1-methyl-, methyl ester
- CBNumber
- CB22594110
- Molecular Formula
- C6H7BrN2O2
- Formula Weight
- 219.04
- MOL File
- 864076-05-1.mol
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Methyl 4-broMo-1-Methyl-1H-iMidazole-2-carboxylate Property
- Boiling point:
- 304.3±34.0 °C(Predicted)
- Density
- 1.67±0.1 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- pka
- 1.20±0.60(Predicted)
- Appearance
- Off-white to light brown Solid
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
AK Scientific
- Product number
- 3528AC
- Product name
- Methyl4-bromo-1-methyl-1H-imidazole-2-carboxylate
- Packaging
- 1g
- Price
- $184
- Updated
- 2021/12/16
American Custom Chemicals Corporation
- Product number
- HCH0369393
- Product name
- METHYL-4-BROMO-1-METHYL-1H-IMIDAZOLE-2-CARBOXYLATE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $503.33
- Updated
- 2021/12/16
Alichem
- Product number
- 864076051
- Product name
- Methyl4-bromo-1-methyl-1H-imidazole-2-carboxylate
- Packaging
- 10g
- Price
- $545
- Updated
- 2021/12/16
Crysdot
- Product number
- CD11041790
- Product name
- Methyl4-bromo-1-methyl-1H-imidazole-2-carboxylate
- Purity
- 95+%
- Packaging
- 25g
- Price
- $950
- Updated
- 2021/12/16
Alichem
- Product number
- 864076051
- Product name
- Methyl4-bromo-1-methyl-1H-imidazole-2-carboxylate
- Packaging
- 25g
- Price
- $950.4
- Updated
- 2021/12/16
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Methyl 4-broMo-1-Methyl-1H-iMidazole-2-carboxylate Chemical Properties,Usage,Production
Synthesis
1313196-09-6
124-41-4
864076-05-1
1. 1-(4-bromo-1-methyl-1H-imidazol-2-yl)-2,2,2-trichloroacetophenone (0.266 g, 868 μmol, 1 eq.) was suspended in methanol (1.41 mL, 34.7 mmol, 40 eq.) and the reaction was heated to reflux for 3 hr. followed by standing overnight at room temperature. 2. Sodium methanolate (15.6 mg, 86.8 μmol, 0.1 eq.) was added to the reaction mixture and stirring was continued for 3 hours at room temperature. 3. After completion of the reaction, the mixture was concentrated under vacuum. 4. 4. The concentrated residue was purified by silica gel column chromatography to afford the target compound methyl 1-methyl-4-bromo-1H-imidazole-2-carboxylate as a light brown solid (155 mg, 81% yield). 5. Mass spectrometry analysis showed m/z = 219.1, 221.1 [M+H]+, confirming the structure of the product.
References
[1] Patent: WO2017/76852, 2017, A1. Location in patent: Page/Page column 53
[2] Patent: US2012/295885, 2012, A1. Location in patent: Page/Page column 32
Methyl 4-broMo-1-Methyl-1H-iMidazole-2-carboxylate Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from Methyl 4-broMo-1-Methyl-1H-iMidazole-2-carboxylate manufacturers
Career Henan Chemical Co
- Product
- Methyl 4-broMo-1-Methyl-1H-iMidazole-2-carboxylate 864076-05-1
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2019-12-23
864076-05-1, Methyl 4-broMo-1-Methyl-1H-iMidazole-2-carboxylateRelated Search:
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