3-QuinolinaMine, 7-Methoxy-
- Product Name
- 3-QuinolinaMine, 7-Methoxy-
- CAS No.
- 87199-83-5
- Chemical Name
- 3-QuinolinaMine, 7-Methoxy-
- Synonyms
- 3-QuinoliMine, 7-Methoxy-;7-Methoxyquinolin-3-aMine;7-Methoxy-3-quinolinaMine;3-QuinolinaMine, 7-Methoxy-
- CBNumber
- CB22595021
- Molecular Formula
- C10H10N2O
- Formula Weight
- 174.2
- MOL File
- 87199-83-5.mol
3-QuinolinaMine, 7-Methoxy- Property
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- Appearance
- Light yellow to yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M341748
- Product name
- 7-Methoxyquinolin-3-amine
- Packaging
- 50mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- CHM0145648
- Product name
- 3-AMINO-7-METHOXYQUINOLINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $505.3
- Updated
- 2021/12/16
- Product number
- W8947
- Product name
- 7-Methoxyquinolin-3-ylamine
- Packaging
- 1g
- Price
- $536
- Updated
- 2021/12/16
- Product number
- CM124102
- Product name
- 7-methoxyquinolin-3-amine
- Purity
- 97%
- Packaging
- 5g
- Price
- $1052
- Updated
- 2021/12/16
- Product number
- CD11039489
- Product name
- 7-Methoxyquinolin-3-amine
- Purity
- 97%
- Packaging
- 5g
- Price
- $1114
- Updated
- 2021/12/16
3-QuinolinaMine, 7-Methoxy- Chemical Properties,Usage,Production
Synthesis
39977-95-2
944401-87-0
881668-93-5
87199-83-5
A mixture of 5-methoxy-3-nitroquinoline and 7-methoxy-3-nitroquinoline (780 mg, 3.82 mmol) was dissolved in ethyl acetate (75 mL) and the reaction mixture was purged with nitrogen for several minutes. Subsequently, 10% palladium/carbon catalyst (54 mg) was added and a hydrogen gas balloon was connected to the reaction flask. The reaction mixture was stirred overnight at room temperature under hydrogen atmosphere. Upon completion of the reaction, the solvent was removed by distillation under reduced pressure and the residue was purified by silica gel column chromatography (100% ethyl acetate) to isolate two isomers: 5-methoxyquinolin-3-amine and 7-methoxyquinolin-3-amine. The final target product 5-methoxyquinolin-3-amine (80 mg, 12% yield) was obtained as a yellow powder. Its structure was confirmed by 1H NMR (CD3OD): δ 8.40 (d, 1H), 7.69 (d, 1H), 7.40 (d, 1H), 7.30 (t, 1H), 6.85 (d, 1H).LC/MS analysis showed that the molecular ion peak of the target isomer (m/z): 175.0 (MH+), with a retention time (Rt) of 1.54 min; the non molecular ion peak (m/z) of the target isomer: 175.0 (MH+) with a retention time (Rt) of 1.53 min.
References
[1] Patent: WO2007/84786, 2007, A1. Location in patent: Page/Page column 117-118
3-QuinolinaMine, 7-Methoxy- Preparation Products And Raw materials
Raw materials
Preparation Products
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