ChemicalBook > CAS DataBase List > 1-Bromo-9H-carbazole

1-Bromo-9H-carbazole

Product Name
1-Bromo-9H-carbazole
CAS No.
16807-11-7
Chemical Name
1-Bromo-9H-carbazole
Synonyms
1-broMocarbazole;-broMo-9H-carbazole;1-bromo-9H-carbozle;-broMo-9H-carbazole;1-broMo-9H-carbazole;1-Bromocarbazole >9H-Carbazole, 1-broMo-
CBNumber
CB22595627
Molecular Formula
C12H8BrN
Formula Weight
246.1
MOL File
16807-11-7.mol
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1-Bromo-9H-carbazole Property

Melting point:
123-124℃ (acetic acid )
Boiling point:
409.2±18.0 °C(Predicted)
Density 
1.617±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
powder to crystal
pka
16.14±0.30(Predicted)
color 
White to Light yellow
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Safety

HS Code 
2933998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TCI Chemical
Product number
B4816
Product name
1-Bromocarbazole
Purity
>98.0%(GC)
Packaging
200mg
Price
$34
Updated
2024/03/01
TCI Chemical
Product number
B4816
Product name
1-Bromocarbazole
Purity
>98.0%(GC)
Packaging
1g
Price
$97
Updated
2024/03/01
TRC
Product number
B678900
Product name
1-Bromo-9H-carbazole
Packaging
5mg
Price
$60
Updated
2021/12/16
TRC
Product number
B678900
Product name
1-Bromo-9H-carbazole
Packaging
25mg
Price
$75
Updated
2021/12/16
SynQuest Laboratories
Product number
3H31-9-1C
Product name
1-Bromo-9H-carbazole
Purity
99%
Packaging
25g
Price
$493
Updated
2021/12/16
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1-Bromo-9H-carbazole Chemical Properties,Usage,Production

Chemical Properties

White to yellow powder or crystals.

Uses

1-Bromo-9H-carbazole is a useful research chemical, mainly used as a pharmaceutical intermediate and an intermediate in organic synthesis.

Preparation

A 1-Bromo-9H-carbazole is synthesized as follows：Under noble gas protection, by 3,6- bis- Tert-butyl carbazole is dissolved in 1,2- dichloroethanes, adds hydrobromic acid, controlling reaction temperature to be slowly added dropwise hydrogen peroxide, dropping is completely Overnight, reactant liquor is washed, and separates organic layer for natural temperature reaction, is dried, and adds methyl alcohol dispersion, obtains the tertiary fourth of bromo- 3, the 6- of 1- bis- Base carbazole；Then 1- bromo- 3,6- di-t-butyl carbazole and isopropanol solvent are added in reaction bulb, controlling reaction temperature slowly adds Enter alchlor reaction, add water after terminating terminating reaction, through extraction, organic layer sodium hydrate aqueous solution is washed, and is dried overnight, concentrate Obtain crude product, methylene chloride-methanol mixed solvent is recrystallized to give product 1-Bromo-9H-carbazole.
Production method of 1-bromocarbazole

Definition

1-Bromo-9H-carbazole is a bromide-substitution of carbazole. The carbazole ring system is essentially planar (r.m.s. deviation of 0.024? for the non-H atoms). It is a photoelectric material intermediate and be used to synthesize OLED materials.

1-Bromo-9H-carbazole Preparation Products And Raw materials

Raw materials

Preparation Products

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1-Bromo-9H-carbazole Suppliers

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View Lastest Price from 1-Bromo-9H-carbazole manufacturers

Henan Fengda Chemical Co., Ltd
Product
1-Bromo-9H-carbazole 16807-11-7
Price
US $50.00-1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-22
Shanghai Daken Advanced Materials Co.,Ltd
Product
9H-Carbazole, 1-bromo- 16807-11-7
Price
US $0.00/KG
Min. Order
1KG
Purity
98.00%
Supply Ability
150KG /month
Release date
2021-11-12
Hebei Xinsheng New Material Technology Co., LTD.
Product
1-Bromo-9H-carbazole 16807-11-7
Price
US $35.00-25.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
20 Ton
Release date
2023-10-08

16807-11-7, 1-Bromo-9H-carbazoleRelated Search:

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