4,5-DICHLORO-3,6-PYRIDAZINEDIOL
- Product Name
- 4,5-DICHLORO-3,6-PYRIDAZINEDIOL
- CAS No.
- 6641-32-3
- Chemical Name
- 4,5-DICHLORO-3,6-PYRIDAZINEDIOL
- Synonyms
- 4,5-DICHLORO-3,6-PYRIDAZINEDIOL;4,5-DICHLOROPYRIDAZINE-3,6-DIOL;4,5-Dichlor-3,6-dihydroxy-pyridazin;3(2H)-Pyridazinone, 4,5-dichloro-6-hydroxy-;4,5-dichloro-1,2-dihydropyridazine-3,6-dione
- CBNumber
- CB2288820
- Molecular Formula
- C4H2Cl2N2O2
- Formula Weight
- 180.98
- MOL File
- 6641-32-3.mol
4,5-DICHLORO-3,6-PYRIDAZINEDIOL Property
- Melting point:
- 295
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- White to off-white Solid
Safety
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 096986
- Product name
- 4,5-Dichloropyridazine-3,6-diol
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $651
- Updated
- 2021/12/16
- Product number
- HCH0022583
- Product name
- 4,5-DICHLOROPYRIDAZINE-3,6-DIOL
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $1258.83
- Updated
- 2021/12/16
- Product number
- 096986
- Product name
- 4,5-Dichloropyridazine-3,6-diol
- Purity
- 95+%
- Packaging
- 1g
- Price
- $1445
- Updated
- 2021/12/16
- Product number
- CM164029
- Product name
- 4,5-Dichloropyridazine-3,6-diol
- Purity
- 95%
- Packaging
- 25g
- Price
- $982
- Updated
- 2021/12/16
- Product number
- CD11076435
- Product name
- 4,5-Dichloropyridazine-3,6-diol
- Purity
- 95+%
- Packaging
- 25g
- Price
- $1040
- Updated
- 2021/12/16
4,5-DICHLORO-3,6-PYRIDAZINEDIOL Chemical Properties,Usage,Production
Synthesis
1122-17-4
6641-32-3
General procedure for the synthesis of 4,5-dichloropyridazine-3,6-diol from 2,3-dichloromaleic anhydride: water (170 mL) and hydrazine dihydrochloride salt (41.9 g, 398.8 mmol) were added to a round bottom flask. The solution was heated to reflux followed by the addition of 2,3-dichloromaleic anhydride (66.6 g, 398.9 mmol) in batches. The reflux condition was maintained and the reaction mixture was stirred continuously for 30 minutes. Upon completion of the reaction, the solution was cooled to room temperature and the precipitated solid was collected by filtration to afford the target product 4,5-dichloropyridazine-3,6-diol (i.e., 4,5-dichloro-1,2-dihydropyridazine-3,6-dione, 65 g, 90% yield) as a white solid. Mass spectral analysis showed (M + H)+ = 181.0.
References
[1] Patent: US2006/287323, 2006, A1. Location in patent: Page/Page column 7
[2] Zhurnal Obshchei Khimii, 1954, vol. 24, p. 1216,1219; engl. Ausg. S. 1205, 1206
4,5-DICHLORO-3,6-PYRIDAZINEDIOL Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4,5-DICHLORO-3,6-PYRIDAZINEDIOL manufacturers
- Product
- 4,5-Dichlor-3,6-dihydroxy-pyridazin 6641-32-3
- Price
- US $0.00-0.00/KG
- Min. Order
- 1g
- Purity
- 98%minHPLC
- Supply Ability
- 50kgs/month
- Release date
- 2021-11-13