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Mirogabalin

Product Name
Mirogabalin
CAS No.
1138245-13-2
Chemical Name
Mirogabalin
Synonyms
Asapiprant;2-((1R,5S,6S)-6-(aminomethyl)-3-ethylbicyclo[3.2.0]hept-3-en-6-yl)acetic acid;DS5565;A200-0700;Milobarin;mirobalin;Miluobalin;Mirogabalin;Mirogabalin HCl;DS5565;A200-0700
CBNumber
CB23051612
Molecular Formula
C12H19NO2
Formula Weight
209.28
MOL File
1138245-13-2.mol
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Mirogabalin Property

Boiling point:
357.5±15.0 °C(Predicted)
Density 
1.104±0.06 g/cm3(Predicted)
storage temp. 
Store at -20°C
solubility 
DMF:0.5(Max Conc. mg/mL);2.39(Max Conc. mM)
Ethanol:1.25(Max Conc. mg/mL);5.97(Max Conc. mM)
PBS (pH 7.2):0.5(Max Conc. mg/mL);2.39(Max Conc. mM)
Water:5.36(Max Conc. mg/mL);25.61(Max Conc. mM)
form 
A crystalline solid
pka
4.65±0.10(Predicted)
color 
Light yellow to light brown
InChI
InChI=1S/C12H19NO2/c1-2-8-3-9-5-12(7-13,6-11(14)15)10(9)4-8/h4,9-10H,2-3,5-7,13H2,1H3,(H,14,15)/t9-,10-,12-/m1/s1
InChIKey
FTBQORVNHOIASH-CKYFFXLPSA-N
SMILES
[C@]12([H])[C@]([H])([C@@](CN)(CC(O)=O)C1)C=C(CC)C2
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Cayman Chemical
Product number
22475
Product name
Mirogabalin
Purity
≥98%
Packaging
1mg
Price
$68
Updated
2024/03/01
Cayman Chemical
Product number
22475
Product name
Mirogabalin
Purity
≥98%
Packaging
5mg
Price
$152
Updated
2024/03/01
TRC
Product number
M364940
Product name
Mirogabalin
Packaging
1mg
Price
$140
Updated
2021/12/16
TRC
Product number
M364940
Product name
Mirogabalin
Packaging
2.5mg
Price
$305
Updated
2021/12/16
ChemScene
Product number
CS-6008
Product name
Mirogabalin
Purity
99.31%
Packaging
50mg
Price
$450
Updated
2021/12/16
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Mirogabalin Chemical Properties,Usage,Production

Description

Mirogabalin is a calcium channel blocker with analgesic effects. It binds to the α2δ-1 and α2δ-2 subunits of voltage-dependent Ca2+ channels. Mirogabalin has potent and sustained analgesic effects (ED50 = 2.5 mg/kg) in rats with diabetes induced by streptozotocin (STZ; ). Mirogabalin does not inhibit activities associated with CNS adverse effects of analgesics, such as rotarod performance (ID50 = 9.4 mg/kg) or locomotor activity (ID50 = 43.9 mg/kg), at its effective dose. Formulations containing mirogabalin are in clinical trials for diabetic peripheral neuropathic pain.

Uses

Mirogabalin is a two alpha2delta ligand which is investigated for the treatment of peripheral neuropathic pain, postherpetic neuralgia and fibromyalgia, showing promising results in patients with diabetic peripheral neuropathy.

brand name

Mirogabalin (brand name Tarlige; developmental code name DS-5565) is a gabapentinoid medication developed by Daiichi Sankyo.

Side effects

The most typical clinical adverse reactions of mirogabalin were dizziness (7.6%) and somnolence (5.1%). However, the occurrence rate was lower than with pregabalin, whose adverse effects were reported to include somnolence, balance disorder, fatigue, and peripheral edema, with an occurrence rate of 8.0%, 4.0%, 4.0%, and 4.0%, respectively[1].

Synthesis

1138246-20-4

1138245-13-2

1. (1R,5S,6S)-[6-(tert-butoxycarbonylaminomethyl)-3-ethylbicyclo[3.2.0]hept-3-en-6-yl]acetate (9.82 g, 23.7 mmol) was added to 100 mL of 4N hydrochloric acid-ethyl acetate solution. 2. The reaction mixture was stirred at room temperature for 1 hour. 3. After completion of the reaction, the solvent was removed by distillation under reduced pressure. 4. The residue was dissolved in dichloromethane. 5. 5. Triethylamine was added dropwise to the above solution and the resulting white powder was subsequently collected by filtration. 6. The collected powder was washed with dichloromethane and then dried to give 4.02 g of white powder. 7. Finally, the powder was washed with ethanol and ethyl acetate to afford the target compound 2-((1R,5S,6S)-6-(aminomethyl)-3-ethylbicyclo[3.2.0]hept-3-en-6-yl)acetic acid as a white powder (2.14 g, 43% yield).

Mode of action

Mirogabalin is an analog of the neurotransmitter, gamma-aminobutyric acid (GABA). It is a potent and specific ligand of the α2δ subunit of voltage-dependent Ca2+channels, which reduces calcium (Ca2+) influx and neurotransmission in dorsal root ganglia (DRGs), inhibiting neurotransmitter release in presynaptic neuron endings.

References

[1] Hui Tang. “The Clinical Application and Progress of Mirogabalin on Neuropathic Pain as a Novel Selective Gabapentinoids.” Mediators of Inflammation 2023 (2023): 4893436.

Mirogabalin Preparation Products And Raw materials

Raw materials

Preparation Products

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Mirogabalin Suppliers

Nanjing Tianhai Pharmaceutical Technology Co., Ltd.
Tel
025-58351158 13851454004
Fax
025-83271564
Email
3494688757@qq.com
Country
China
ProdList
210
Advantage
58
Nanjing Becas pharmatech Ltd.
Tel
13912903754
Email
info@becaspharma.com
Country
China
ProdList
2763
Advantage
58
Anhui Cheer-Our Medical technology Co.,Ltd
Tel
0551-63535381 13485700777
Email
gaylen@cheer-our.com
Country
China
ProdList
96
Advantage
58
NANJING ZENJI PHARMACEUTICALS
Tel
025-58231105-8151 15190133791;
Email
marketing@zenjipharma.com
Country
China
ProdList
420
Advantage
58
NANJING ZENJI PHARMACEUTICALS
Tel
025-58231105-8151
Fax
025-83172562
Email
marketing@zenjipharma.com
Country
China
ProdList
420
Advantage
58
Hangzhou Chemtrue Bio-Tech Co.,Ltd.
Tel
0571-86828652 18857119830
Fax
0571-83522824
Email
sales@chemtrue-bio.com
Country
China
ProdList
252
Advantage
58
Nanjing Vcare PharmaTech Co., Ltd
Tel
025-58741518 13327700685
Email
sales@vcarepharmatech.com
Country
China
ProdList
496
Advantage
58
Beijing HwrkChemical Technology Co., Ltd
Tel
18515581800 18501085097
Fax
010-89508210
Email
sales.bj@hwrkchemical.com
Country
China
ProdList
9400
Advantage
55
Adamas Reagent, Ltd.
Tel
400-6009262 16621234537
Fax
021-64823266
Email
chenyj@titansci.com
Country
China
ProdList
14101
Advantage
59
Anhui Lianchuang Biological Medicine Co.,Ltd
Tel
0551-68779238 18056025720
Email
sales3@lcywhx.com
Country
China
ProdList
157
Advantage
57
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View Lastest Price from Mirogabalin manufacturers

Shaanxi Dideu New Materials Co. Ltd
Product
Mirogabalin 1138245-13-2
Price
US $0.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
1000kg
Release date
2025-06-21
Shaanxi Dideu Medichem Co. Ltd
Product
Mirogabalin 1138245-13-2
Price
US $1.00-4.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
1KG 100K
Release date
2025-05-19
Cangzhou Kangrui Pharma Tech Co. Ltd.,
Product
Mirogabalin 1138245-13-2
Price
US $0.00-0.00/g
Min. Order
50g
Purity
99%
Supply Ability
20kgs
Release date
2025-02-28

1138245-13-2, MirogabalinRelated Search:


  • 2-((1R,5S,6S)-6-(aminomethyl)-3-ethylbicyclo[3.2.0]hept-3-en-6-yl)acetic acid
  • Mirogabalin
  • Asapiprant
  • [(1R,5S,6S)-6-(Aminomethyl)-3-ethylbicyclo[3.2.0]hept-3-en-6-yl]acetic acid
  • A200-0700
  • DS5565
  • DS5565;A200-0700
  • 2-[(1R,5S,6S)-6-(aminomethyl)-3-ethyl-6-bicyclo[3.2.0]hept-3-enyl]acetic acid
  • MIROGABALIN; DS-5565
  • DS 5565;DS-5565;DS5565
  • Bicyclo[3.2.0]hept-3-ene-6-acetic acid, 6-(aminomethyl)-3-ethyl-, (1R,5S,6S)-
  • Miluobalin
  • Mirogabalin HCl
  • Milobarin
  • mirobalin
  • Mirogabalin free base
  • Mirogabalin Impurity
  • Mirogabalin base
  • Mirogabalin-d2,15N
  • Mirogabalin Impurity 65
  • Mirogabalin Impurity 35 Hydrochloride
  • Mirogabalin Impurity 13 Hydrochloride
  • Mirogabalin Impurity 18 Hydrochloride
  • Mirogabalin Impurity 76
  • Mirogabalin Impurity 78
  • Mirogabalin Impurity 80
  • Mirogabalin Impurity 6 Maleate
  • Mirogabalin Impurity 81
  • Mirogabalin Impurity 82
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  • Mirogabalin Impurity 150
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  • Mirogabalin Impurity 141
  • Mirogabalin Impurity 142
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  • Mirogabalin Impurity 144
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  • Mirogabalin Impurity 147 (N-Nitroso Mirogabalin)
  • Mirogabalin Impurity 148 (N-Nitroso Mirogabalin Impurity 103)
  • Mirogabalin Impurity 149
  • Mirogabalin Impurity 129 (N-Nitroso Mirogabalin Impurity 32)
  • Mirogabalin Impurity 130
  • Mirogabalin Impurity 131
  • Mirogabalin Impurity 132
  • Mirogabalin Impurity 133
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  • Mirogabalin Impurity 135
  • Mirogabalin Impurity 135 Sodium Salt
  • Mirogabalin Impurity 136
  • Mirogabalin Impurity 137
  • Mirogabalin Impurity 138
  • Mirogabalin Impurity 139
  • Mirogabalin Impurity 84
  • Mirogabalin Impurity 85
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  • Mirogabalin Impurity 4 Monomer