ChemicalBook > CAS DataBase List > 6-NITROQUINOLINE

6-NITROQUINOLINE

Product Name
6-NITROQUINOLINE
CAS No.
613-50-3
Chemical Name
6-NITROQUINOLINE
Synonyms
40 kg;6-NitroquinoL;6-Nitrochinolin;6-NITROQUINOLINE;6-nitro-quinolin;6-Nittroquinoline;Quinoline,6-nitro-;6-Nitroquinoline>6-Nitroquinoline98%;6-Nitro Quinoline - 50g
CBNumber
CB2332655
Molecular Formula
C9H6N2O2
Formula Weight
174.16
MOL File
613-50-3.mol
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6-NITROQUINOLINE Property

Melting point:
151-153 °C(lit.)
Boiling point:
305.12°C (rough estimate)
Density 
1.2190 (estimate)
refractive index 
1.6820 (rough estimate)
storage temp. 
Sealed in dry,Room Temperature
Water Solubility 
Slightly soluble in water
form 
powder to crystal
pka
3.24±0.10(Predicted)
color 
Needles from water or alc
BRN 
136138
InChI
InChI=1S/C9H6N2O2/c12-11(13)8-3-4-9-7(6-8)2-1-5-10-9/h1-6H
InChIKey
SMHPLBXIVNQFBA-UHFFFAOYSA-N
SMILES
N1C2C(=CC([N+]([O-])=O)=CC=2)C=CC=1
CAS DataBase Reference
613-50-3(CAS DataBase Reference)
EPA Substance Registry System
6-Nitroquinoline (613-50-3)
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Safety

Hazard Codes 
Xn
Risk Statements 
20/21/22-40
Safety Statements 
7-22-36-45
WGK Germany 
3
RTECS 
VC1900000
HS Code 
29339900
Toxicity
mma-sat 100 mmol/plate MUREAV 58,11,78
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H351Suspected of causing cancer

Precautionary statements

P201Obtain special instructions before use.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P308+P313IF exposed or concerned: Get medical advice/attention.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
N24005
Product name
6-Nitroquinoline
Purity
98%
Packaging
25g
Price
$104
Updated
2025/07/31
TCI Chemical
Product number
N0252
Product name
6-Nitroquinoline
Purity
>98.0%(GC)(T)
Packaging
5g
Price
$39
Updated
2025/07/31
TCI Chemical
Product number
N0252
Product name
6-Nitroquinoline
Purity
>98.0%(GC)(T)
Packaging
25g
Price
$147
Updated
2025/07/31
Usbiological
Product number
285429
Product name
6-Nitroquinoline
Packaging
10g
Price
$319
Updated
2021/12/16
TRC
Product number
N900683
Product name
6-Nitroquinoline
Packaging
50mg
Price
$45
Updated
2021/12/16
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6-NITROQUINOLINE Chemical Properties,Usage,Production

Chemical Properties

beige to light brown powder

Safety Profile

Mutation data reported. Whenheated to decomposition it emits toxic fumes of NOx. Seealso other nitroquinoline entries.

Synthesis

5332-25-2

613-50-3

GENERAL STEPS: 6-bromoquinoline (0.5 mmol), copper(II) trifluoromethanesulfonate (45 mg, 0.125 mmol), potassium nitrite (KNO2, 128 mg, 1.5 mmol), and anhydrous dimethylsulfoxide (DMSO, 0.6 mL) were sequentially added to a pre-dried oven-dried pressure tube under nitrogen protection. The pressure tube was sealed with a PTFE screw cap with a micro-valve and purged by nitrogen for 5 min to remove air. Subsequently, the reaction mixture was stirred at room temperature for 10 minutes and then gradually warmed up to 130°C and the reaction was continued at this temperature for 48 hours. Upon completion of the reaction, the mixture was cooled to room temperature, washed with excess ice water and extracted with ethyl acetate (3 x 10 mL). The organic phases were combined, dried over anhydrous sodium sulfate (Na2SO4), filtered and concentrated under reduced pressure to give the crude product. The crude product was purified by column chromatography on silica gel (for entries 1-18 in Table 2) or basic alumina (for entries 19-23 in Table 2), using a solvent mixture of ethyl acetate and hexane as eluent, and the target product, 6-nitroquinoline, was finally obtained in good yield.

References

[1] Tetrahedron Letters, 2012, vol. 53, # 12, p. 1511 - 1513
[2] Tetrahedron, 2013, vol. 69, # 31, p. 6409 - 6414

6-NITROQUINOLINE Preparation Products And Raw materials

Raw materials

N-Methyl-4-nitroaniline Acrolein Sodium sulfide ARSENIC ACID,HEMIHYDRATE Sodium 3-nitrobenzenesulphonate Glycerol Vanadium(V) oxide Sulfuric acid 4-Nitroaniline

Preparation Products

6-Aminoquinoline
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6-NITROQUINOLINE Suppliers

Americas 1 Austria 1 Belgium 2 China 174 Europe 3 Germany 8 India 29 Japan 4 Switzerland 2 The Netherlands 1 Ukraine 2 United Kingdom 12 United States 26 Global 265
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View Lastest Price from 6-NITROQUINOLINE manufacturers

Henan Aochuang Chemical Co.,Ltd.
Product
6-NITROQUINOLINE 613-50-3
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1Ton
Release date
2022-10-12
Hong Kong Tiansheng New Material Trading Co., Ltd
Product
6-Nitroquinoline 613-50-3
Price
US $2.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100kg
Release date
2021-09-24
Hong Kong Tiansheng New Material Trading Co., Ltd
Product
6-Nitroquinoline 613-50-3
Price
US $2.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
100KG
Release date
2021-09-24

613-50-3, 6-NITROQUINOLINERelated Search:

2-METHYL-6-NITROQUINOLINE 6-NITROQUINOLINE 5-NITRO-1,10-PHENANTHROLINE-2,9-DICARBOXYLIC ACID 4-HYDROXY-6-NITROQUINOLINE 5-Nitro-1,10-phenanthroline 5-Amino-6-nitroquinoline 6-BROMO-5-NITROQUINOLINE 2-METHYL-8-NITROQUINOLINE 2-NITROQUINOLINE 1,2,3,4-TETRAHYDRO-7-NITROQUINOLINE 6-CHLORO-5-NITROQUINOLINE 2-BROMO-4-NITROQUINOLINE 2-CHLORO-3-NITROQUINOLINE 6-Methoxy-8-nitroquinoline, GC 99% 5-NITROQUINOLINE 98+% 2-CHLORO-6-NITROQUINOLINE 4-NITROQUINOLINE N-OXIDE POWDER,4-NITROQUINOLINE N-OXIDE 98+%,4-Nitroquinoline-N-oxide, HPLC 98% 8-HYDROXY-6-NITROQUINOLINE

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