ChemicalBook > CAS DataBase List > (3-AMINO-5-NITROPHENYL)METHANOL

(3-AMINO-5-NITROPHENYL)METHANOL

Product Name: (3-AMINO-5-NITROPHENYL)METHANOL
CAS No.: 90390-46-8
Chemical Name: (3-AMINO-5-NITROPHENYL)METHANOL
Synonyms: 3-Amino-5-nitrobenzenemethanol;(3-AMINO-5-NITROPHENYL)METHANO;(3-AMINO-5-NITROPHENYL)METHANOL;3-(Hydroxymethyl)-5-nitroaniline;Benzenemethanol, 3-amino-5-nitro-
CBNumber: CB2377203
Molecular Formula: C7H8N2O3
Formula Weight: 168.15
MOL File: 90390-46-8.mol

Less

(3-AMINO-5-NITROPHENYL)METHANOL Property

Boiling point:: 425.9±30.0 °C(Predicted)
Density: 1.432±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 13.71±0.10(Predicted)
Appearance: Light yellow to green yellow Solid

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

Less

N-Bromosuccinimide Price

TRC

Product number: A622758
Product name: (3-Amino-5-nitrophenyl)methanol
Packaging: 100mg
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: W9312
Product name: (3-Amino-5-nitrophenyl)methanol
Packaging: 5g
Price: $330
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: AAA0007123
Product name: (3-AMINO-5-NITROPHENYL)METHANOL
Purity: 95.00%
Packaging: 250MG
Price: $444
Updated: 2021/12/16

Matrix Scientific

Product number: 074465
Product name: (3-Amino-5-nitrophenyl)methanol
Purity: 95+%
Packaging: 1g
Price: $559
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: AAA0007123
Product name: (3-AMINO-5-NITROPHENYL)METHANOL
Purity: 95.00%
Packaging: 0.5G
Price: $780
Updated: 2021/12/16

Less

(3-AMINO-5-NITROPHENYL)METHANOL Chemical Properties,Usage,Production

Synthesis

71022-43-0

90390-46-8

(ii) Synthesis of 3-amino-5-nitrobenzyl alcohol: 3,5-dinitrobenzyl alcohol (129.1 g, 0.65 mol) from step (i) was dissolved in methanol (1500 mL) and heated to reflux. Ammonium sulfide solution (450 mL, containing 20 wt% H2O, 442.9 g, 1.30 mol) was added slowly over 45 min. The resulting non-homogeneous mixture was refluxed for 2 hours, followed by stirring at 25 °C for 18 hours. Upon completion of the reaction, the mixture was filtered through a diatomaceous earth pad and the filtrate was acidified with 2N hydrochloric acid and the methanol was evaporated under reduced pressure. The remaining acidic aqueous solution was washed with ether (3×) and then alkalized with 6N sodium hydroxide solution. The alkalized aqueous solution was extracted with ether (4×). The organic phases were combined, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give 95.8 g (88% yield) of 3-amino-5-nitrobenzenemethanol as an orange solid, which could be used in the next reaction without further purification. The product was characterized by 1H NMR (300 MHz, CD3OD): δ 7.46 (m, 1H), 7.38 (m, 1H), 6.98 (m, 1H), 4.57 (s, 2H).

References

[1] Tetrahedron Letters, 2003, vol. 44, # 29, p. 5477 - 5481
[2] Chinese Chemical Letters, 2011, vol. 22, # 7, p. 785 - 788
[3] Journal of Medicinal Chemistry, 1984, vol. 27, # 9, p. 1111 - 1118
[4] Bioorganic and medicinal chemistry letters, 2002, vol. 12, # 22, p. 3263 - 3265
[5] Journal of Labelled Compounds and Radiopharmaceuticals, 2002, vol. 45, # 3, p. 257 - 268

(3-AMINO-5-NITROPHENYL)METHANOL Preparation Products And Raw materials

Raw materials

Preparation Products

Less

(3-AMINO-5-NITROPHENYL)METHANOL Suppliers

China 41 India 1 United States 5 Global 47

Wuhan Chemwish Technology Co., Ltd

Tel: 86-027-67849912
Fax: 86-027-87531808
Email: sales@chemwish.com
Country: China
ProdList: 35896
Advantage: 56

Chengdu HappySyn Pharmaceutical Technology Co., Ltd.

Tel: 028-85114309 18982182443
Email: yangli@happysyn.com
Country: China
ProdList: 2152
Advantage: 55

Shanghai Topbiochem Technology Co., Ltd

Tel: +86-21-60341587
Fax: +86-21-61294319
Email: sales@topbiochem.com
Country: China
ProdList: 6175
Advantage: 58

Shanghai T&W Pharmaceutical Co., Ltd.

Tel: +86 21 61551611
Fax: +86 21 50676805
Country: China
ProdList: 9891
Advantage: 58

Shanghai Witofly Chemical Co.,Ltd

Tel
Email: sales@witofly.com
Country: China
ProdList: 2864
Advantage: 52

Cool Pharm, Ltd

Tel: 021-60455363 18019463053
Fax: 50966098
Email: sales@coolpharm.com
Country: China
ProdList: 12346
Advantage: 58

SuZhou ShiYa Biopharmaceuticals, Inc.

Tel: 0512-0512-52358471 17715136450
Fax: 05125235 6881
Email: sales@shiyabiopharm.com
Country: China
ProdList: 12127
Advantage: 58

Wuhan Chemwish Technology Co.， Ltd

Tel: 027-67849912
Fax: 027-87531808
Email: sales@chemwish.com
Country: China
ProdList: 9148
Advantage: 60

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Sichuan BaiPeng Biotechnology Co., Ltd.

Tel: 028-65791793 18140026355
Fax: QQ568470422
Email: 568470422@qq.com
Country: China
ProdList: 9997
Advantage: 58

Wuxi AppTec

Tel: 022-59987777 13552403979
Email: jia_guoqiang@wuxiapptec.com
Country: China
ProdList: 22345
Advantage: 58

Aikon International Limited

Tel: 025-58859352 18068836627
Fax: (5)02557626880
Email: dt3@aikonchem.com
Country: China
ProdList: 15493
Advantage: 58

Suzhou Nuoouman Biological Technology Co., Ltd.

Tel: 15026866316
Email: 180642609@qq.com
Country: China
ProdList: 4967
Advantage: 58

3A Chemicals

Tel: 400-668-9898
Fax: 010-51582189
Email: service@3achem.com
Country: China
ProdList: 20557
Advantage: 58

Shanghai Jizhi Biochemical Technology Co. Ltd.

Tel: 4009004166/18616739031 18616739031
Email: 3007523370@qq.com
Country: China
ProdList: 52687
Advantage: 58

Shanghai Thunder Biological Technology Co., Ltd.

Tel: 18621609968
Email: 1162686636@qq.com
Country: China
ProdList: 879
Advantage: 58

Aishilun biotechnology (Shanghai) co., LTD

Tel: 021-50676523 18019098996
Email: info@acelybio.com
Country: China
ProdList: 3960
Advantage: 58

Henan Alpha Chemical Co., Ltd.

Tel: 0371-55055611 18137792234
Fax: QQ：3002694073
Email: 3002694073@qq.com
Country: China
ProdList: 9987
Advantage: 58

Henan Alfa Chemical Co., Ltd

Tel: +8615838112936
Email: alfa10@alfachem.cn
Country: China
ProdList: 12921
Advantage: 58

Accela ChemBio Co.,Ltd.

Tel: 021-50795510 4000665055
Email: sales@accelachem.com
Country: China
ProdList: 10467
Advantage: 58

Jiangsu Hongmin Pharmaceutical Co., Ltd.

Tel: 18221292452
Email: fannieliu@glschina.com
Country: China
ProdList: 6798
Advantage: 58

Wuhan Chemwish Technology Co., Ltd

Tel: 027-67849912
Email: sales@chemwish.com
Country: CHINA
ProdList: 10821
Advantage: 58

Changzhou Kechem Bio-Scientific Co., LTD.

Tel: 0519-68985668 13685222090
Fax: qq735434464
Email: sales@kechem.cn
Country: China
ProdList: 26028
Advantage: 58

Energy Chemical

Tel: 021-58432009 400-005-6266
Fax: 021-58436166
Email: marketing@energy-chemical.com
Country: China
ProdList: 44918
Advantage: 58

Shanghai Sunway Pharmaceutical Technology Co.,Ltd.

Tel: 021-51816796-820 13611835272
Fax: 021-5161 3951
Email: sales2@sunwaypharm.com
Country: China
ProdList: 44119
Advantage: 58

Hubei Co-prosperity Medicine Technonlogy Co., Ltd

Tel: 2383948258 19172820304
Email: 2383948258@qq.com
Country: China
ProdList: 12987
Advantage: 58

Beijing Jin Ming Biotechnology Co., Ltd.

Tel: 010-60605840 15801484223;
Email: psaitong@jm-bio.com
Country: China
ProdList: 29757
Advantage: 58

Shanghai Haohong Pharmaceutical Co., Ltd.

Tel: 400-8210725 4008210725
Email: malulu@leyan.com
Country: China
ProdList: 40000
Advantage: 58

Bide Pharmatech Ltd.

Tel: 400-1647117 13681763483
Email: product02@bidepharm.com
Country: China
ProdList: 59936
Advantage: 58

Bide Pharmatech Ltd.

Tel: 400-6005915
Email: sales@picasso-e.com
Country: China
ProdList: 39653
Advantage: 58

Shanghai Zhixia Chemical Technology Co., LTD

Tel: 15216847143 18321145570
Email: 1458509898@qq.com
Country: China
ProdList: 499
Advantage: 58

Shanghai Lingfu Pharmaceutical Research Co. LTD

Tel: +86(21)5895 0110 19945755304
Email: sales@chemany.com
Country: China
ProdList: 9984
Advantage: 58

Suzhou Meishi Biotechnology Co., Ltd.

Tel: 1173954148q
Email: meishipharma@126.com
Country: China
ProdList: 20033
Advantage: 58

Beijing Solarbio Science & Tecnology Co., Ltd.

Tel: 010-50973130 17801761073
Email: Gsiyu@solarbio.com
Country: China
ProdList: 50751
Advantage: 58

Shanghai Huasige Pharmaceutical Technology Co., LTD

Tel: 13611612777
Email: 3627377363@qq.com
Country: China
ProdList: 4015
Advantage: 58

ATK CHEMICAL COMPANY LIMITED

Tel: +undefined-21-51877795
Fax: +86 21 5161 9052/ 5187 7796
Email: ivan@atkchemical.com
Country: China
ProdList: 33024
Advantage: 60

DAYANG CHEM (HANGZHOU) CO.,LTD

Tel: +86-88938639 +86-17705817739
Email: info@dycnchem.com
Country: China
ProdList: 53899
Advantage: 58

Sichuan Biosynce Pharmatech Co., Ltd.

Tel: +8619950309693
Email: diane@biosynce.com
Country: China
ProdList: 4871
Advantage: 58

Kindchem(Nanjing)Co.,Ltd

Tel: +86-025-025-85281586 +8618651653755
Fax: 025-68661290
Email: sales@kindchem.cn
Country: China
ProdList: 1226
Advantage: 58

Shanghai Sunway Pharmaceutical Technology Co., Ltd

Tel: --
Fax: --
Email: sales@sunwaypharm.com
Country: China
ProdList: 6536
Advantage: 58

Shanghai Hao Zhun Biological Technology Co., Ltd.

Tel: --
Fax: --
Email: info@zzsrm.com
Country: CHINA
ProdList: 6650
Advantage: 58

90390-46-8, (3-AMINO-5-NITROPHENYL)METHANOLRelated Search:

3,5-Dinitrobenzoic acid 3,5-DINITROBENZYL ALCOHOL ETHYL 3,5-DINITROBENZOATE 3,5-Dinitro-4-methylbenzoic acid 4-DIMETHYLAMINO-3,5-DINITROBENZOIC ACID 3,5-Dinitro-2-methylbenzoic acid 2-Chloro-3,5-dinitrobenzoic acid 4-AMINO-3,5-DINITROBENZOIC ACID 3,5-Dinitrosalicylic acid Methyl 3,5-dinitrobenzoate 4-Chloro-3,5-dinitrobenzoic acid 3-Amino-5-nitrobenzoic acid 3,5-DINITRO-4-HYDROXYBENZOIC ACID 2,4-DICHLORO-3,5-DINITROBENZOIC ACID Methyl 3,5-dinitrosalicylate 3,5-DINITRO-2-HYDROXYBENZOIC ACID SODIUM METHYL 4-CHLORO-3,5-DINITROBENZOATE 3,5-DINITRO-2-METHYLBENZYL ALCOHOL

3-(Hydroxymethyl)-5-nitroaniline

3-Amino-5-nitrobenzenemethanol

(3-AMINO-5-NITROPHENYL)METHANOL

(3-AMINO-5-NITROPHENYL)METHANO

Benzenemethanol, 3-amino-5-nitro-

90390-46-8