4-Chloro-3,5-dinitrobenzoic acid

Product Name: 4-Chloro-3,5-dinitrobenzoic acid
CAS No.: 118-97-8
Chemical Name: 4-Chloro-3,5-dinitrobenzoic acid
Synonyms: 4-Chloro-3;AKOS 212-81;4-C-3,5-DNBA;CBI-BB ZERO/005300;TIMTEC-BB SBB003176;RARECHEM AL BO 0221;LABOTEST-BB LT00117948;4-chloro-3,5-dinitrobenzoate;4-chloro-3,5-dinitro-benzoicaci;4-CHLORO-3,5-DINITROBENZOIC ACID
CBNumber: CB6753319
Molecular Formula: C7H3ClN2O6
Formula Weight: 246.56
MOL File: 118-97-8.mol

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4-Chloro-3,5-dinitrobenzoic acid Property

Melting point:: 159-162 °C (lit.)
Boiling point:: 315°C
Density: 1.9543 (rough estimate)
refractive index: 1.6500 (estimate)
Flash point:: 186°C
storage temp.: Sealed in dry,2-8°C
solubility: soluble in Methanol
form: powder to crystal
pka: 2?+-.0.10(Predicted)
color: Light orange to Yellow to Green
BRN: 668253
CAS DataBase Reference: 118-97-8(CAS DataBase Reference)
EPA Substance Registry System: Benzoic acid, 4-chloro-3,5-dinitro- (118-97-8)

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Safety

Hazard Codes: Xi,E
Risk Statements: 38-36/37/38-36/38-2
Safety Statements: 28-24/25-22-35-26
WGK Germany: 3
Hazard Note: Irritant
TSCA: Yes
HS Code: 29163990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: C38907
Product name: 4-Chloro-3,5-dinitrobenzoic acid
Purity: 97%
Packaging: 25g
Price: $65
Updated: 2023/06/20

Sigma-Aldrich

Product number: C38907
Product name: 4-Chloro-3,5-dinitrobenzoic acid
Purity: 97%
Packaging: 100g
Price: $210
Updated: 2023/06/20

TCI Chemical

Product number: C0607
Product name: 4-Chloro-3,5-dinitrobenzoic Acid
Purity: >98.0%(T)
Packaging: 25g
Price: $74
Updated: 2024/03/01

TCI Chemical

Product number: C0607
Product name: 4-Chloro-3,5-dinitrobenzoic Acid
Purity: >98.0%(T)
Packaging: 250g
Price: $471
Updated: 2024/03/01

Alfa Aesar

Product number: A12373
Product name: 4-Chloro-3,5-dinitrobenzoic acid, 99%
Packaging: 25g
Price: $50.65
Updated: 2024/03/01

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4-Chloro-3,5-dinitrobenzoic acid Chemical Properties,Usage,Production

Chemical Properties

yellow crystals

Uses

4-Chloro-3,5-dinitrobenzoic-15N2 Acid is an intermediate in synthesizing Lodoxamide-15N2,d2 (L469367), a labelled form of Lodoxamide. It is an antiallergic drug that acts as a mast cell stabilizer. It is effective in the treatment of allergic conjunctivitis and in decreasing vascular permeability.

Hazard

irritant

Synthesis

The synthesis of 4-Chloro-3,5-dinitrobenzoic acid is as follows:
4-chloro-benzoic acid (20 g, 0.128 mol) was dissolved in H₂SO₄ (d = 1.835 g/mL, 300 mL) at80 C, and KNO₃ (66 g, 0.65 mol) was added. The reaction mixture was heated to 125 C using ahigh-pressure flask and kept for 2 h, after which the reaction was cooled to rt and poured onto ice.The yield of 4-Chloro-3,5-dinitrobenzoic acid was 28 g (89%) .

Purification Methods

Crystallise the acid from EtOH/ H2O, EtOH or *C6H6. The 1:1 naphthalene complex (by fusing various ratios of ingredients and recrystallising from EtOH) has m 122o. [Beilstein 9 H 416, 9 III 1953, 9 IV 1360.]

4-Chloro-3,5-dinitrobenzoic acid Preparation Products And Raw materials

Raw materials

4-Chlorobenzoic acid Nitric acid Sulfuric acid

Preparation Products

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4-Chloro-3,5-dinitrobenzoic acid Suppliers

Americas 1 Austria 1 Canada 2 China 167 Europe 3 Germany 8 India 17 Japan 6 Russia 1 Slovakia 1 South Korea 1 Switzerland 3 Ukraine 1 United Kingdom 11 United States 36 Global 259

Nantong Lianyi Chemical CO.,LTD.

Tel: 0513-81188185 13861935768
Email: ourui@lyhgchem.com
Country: China
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Shangqiu Ladybug Network Technology Co., LTD

Tel: 0370-2059268 15672839268
Fax: 03702782809
Email: 2352713635@qq.com
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J & K SCIENTIFIC LTD.

Tel: 010-82848833 400-666-7788
Fax: 86-10-82849933
Email: jkinfo@jkchemical.com
Country: China
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Meryer (Shanghai) Chemical Technology Co., Ltd.

Tel: 4006608290; 18621169109
Fax: 86-21-61259102
Email: market03@meryer.com
Country: China
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future industrial shanghai co., ltd

Tel: 400-0066400 13621662912
Fax: 021-55660885
Email: sales@jonln.com
Country: China
ProdList: 1998
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Alfa Aesar

Tel: 400-6106006
Fax: 021-67582001/03/05
Email: saleschina@alfa-asia.com
Country: China
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TAIYUAN RHF CO.,LTD.

Tel: +86 351 7031519
Fax: +86 351 7031519
Email: sales@RHFChem.com
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TCI (Shanghai) Development Co., Ltd.

Tel: 021-67121386
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Email: Sales-CN@TCIchemicals.com
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Energy Chemical

Tel: 021-021-58432009 400-005-6266
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Beijing Ouhe Technology Co., Ltd

Tel: 010-82967028 13552068683
Fax: +86-10-82967029
Email: 2355560935@qq.com
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View Lastest Price from 4-Chloro-3,5-dinitrobenzoic acid manufacturers

Asia Chem I and E (Jiangsu) Co Ltd

Product: 4-Chloro-3,5-dinitrobenzoic acid 118-97-8
Price: US $34.88/Kg/Drum
Min. Order: 25Kg/Drum
Purity: 99.00%HPLC
Supply Ability: 10tons/month
Release date: 2021-09-23

Henan Fengda Chemical Co., Ltd

Product: 4-Chloro-3,5-dinitrobenzoic acid 118-97-8
Price: US $100.00-1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2023-12-25

Hebei Mojin Biotechnology Co., Ltd

Product: 4-Chloro-3,5-dinitrobenzoic acid 118-97-8
Price: US $0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 50000KG/month
Release date: 2023-10-27

118-97-8, 4-Chloro-3,5-dinitrobenzoic acidRelated Search:

3,5-Dinitrobenzoic acid 2-Nitrochlorobenzene 2-Chlorobenzoic acid 4-Chloro-3-nitrobenzoic acid 4-Nitrobenzoic acid 1-Chloro-3-nitrobenzene 4-Nitrophenyl chloroformate Difluorochloromethane Ethyl chloroformate 4-CHLORO-2,6-DINITROBENZOIC ACID 2,4-DICHLORO-3,5-DINITROBENZOIC ACID 4-CHLORO-3,5-DINITRO-BENZOIC ACID ISOBUTYL ESTER 2-CHLORO-3,5-DINITROBENZOIC ACID,2-Chloro-3,5-dinitrobenzoic acid, 97% (dry wt.), may cont. up to ca 5% water 5-CHLORO-2,4-DINITROBENZOIC ACID 2-CHLORO-4,6-DINITROBENZOIC ACID 4-Chlorobenzoic acid 4-Chloro-3,5-dinitrobenzoic acid METHYL 4-CHLORO-3,5-DINITROBENZOATE

TIMTEC-BB SBB003176

CBI-BB ZERO/005300

4-chloro-3,5-dinitrobenzoate

4-chloro-3,5-dinitro-benzoicaci

RARECHEM AL BO 0221

LABOTEST-BB LT00117948

AKOS 212-81

3,5-DINITRO-4-CHLOROBENZOIC ACID

4-CHLORO-3,5-DINITROBENZOIC ACID

4-Chloro-3,5-dinitrobenzoic acid,99%

4-CHLORO-3,5-DINITROBENZOIC ACID FOR SYN

4-chloro -3,5-twoNitrobenzoic Acid

4-Chloro-3,5-dinitrobenzoic acid, 98%+

4-Chloro-3

4-C-3,5-DNBA

4-Chloro-3,5-dinitrobenzoic Acid &gt

Benzoic acid, 4-chloro-3,5-dinitro-

4-Chloro-3,5-dinitrobenzoic acid ISO 9001：2015 REACH

4-Chloro-3,5-dinitrobenzoic acid, 97%,

118-97-8

C7H3ClN2O6

ClC6H2NO22CO2H

C7H2ClN2O6

Organic Building Blocks

C7

Carboxylic Acids

Carbonyl Compounds

Building Blocks

Organic acids

C7

Carbonyl Compounds

Carboxylic Acids

1