1H-INDAZOLE-4-CARBALDEHYDE
- Product Name
- 1H-INDAZOLE-4-CARBALDEHYDE
- CAS No.
- 669050-70-8
- Chemical Name
- 1H-INDAZOLE-4-CARBALDEHYDE
- Synonyms
- 4-Formylindazole;4-Formyl-1H-indazole;1H-indazole-4-carbald;1H-INDAZOLE-4-CARBALDEHYDE;1H-Indazole-4-carbaldehyd...;1H-Indazole-4-carboxaldehyde;1H-Indazole-4-carboxaldehyde (9CI);1H-Indazole-4-carboxaldehyde (9CI, ACI)
- CBNumber
- CB2395487
- Molecular Formula
- C8H6N2O
- Formula Weight
- 146.15
- MOL File
- 669050-70-8.mol
1H-INDAZOLE-4-CARBALDEHYDE Property
- Boiling point:
- 358.3±15.0 °C(Predicted)
- Density
- 1.368±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 12.49±0.40(Predicted)
- form
- Crystalline Powder
- color
- White
Safety
- Risk Statements
- 36/37/38
- Safety Statements
- 26-36/37/39
- HS Code
- 29339980
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- I628085
- Product name
- 1H-Indazole-4-carbaldehyde
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- W7760
- Product name
- 1H-Indazole-4-carbaldehyde
- Packaging
- 250mg
- Price
- $117
- Updated
- 2021/12/16
- Product number
- F11365
- Product name
- 4-Formylindazole
- Purity
- 95%
- Packaging
- 1g
- Price
- $120
- Updated
- 2021/12/16
- Product number
- 4H15-1-0F
- Product name
- 1H-Indazole-4-carboxaldehyde
- Packaging
- 1g
- Price
- $275
- Updated
- 2021/12/16
- Product number
- F11365
- Product name
- 4-Formylindazole
- Purity
- 95%
- Packaging
- 500mg
- Price
- $80
- Updated
- 2021/12/16
1H-INDAZOLE-4-CARBALDEHYDE Chemical Properties,Usage,Production
Synthesis
709608-85-5
669050-70-8
Synthesis of 1H-indazole-1,4-carboxaldehyde (12i): 4-(Hydroxymethyl)-1H-indazole (54 mg, 0.36 mmol) was dissolved in 3 mL of tetrahydrofuran (THF) followed by addition of Dess-Martin periodinane (247 mg, 0.58 mmol). The reaction mixture was stirred overnight at room temperature and quenched with 2.0 M sodium thiosulfate (Na2S2O3) solution upon completion of the reaction. The reaction mixture was extracted with ethyl acetate, the organic layers were combined, washed sequentially with saturated sodium bicarbonate (NaHCO3) solution and brine, and dried over anhydrous magnesium sulfate (MgSO4). The solvent was removed by concentration under reduced pressure and the residue was purified by column chromatography (75% ethyl acetate/hexane) to afford 1-hydro-indazole-4-carbaldehyde (37 mg, 70% yield) as a white solid. Determination by mass spectrometry (electrospray ionization): expected value of M+H = 147.1, measured value = 147.2.
References
[1] Patent: WO2007/51062, 2007, A2. Location in patent: Page/Page column 127-128
1H-INDAZOLE-4-CARBALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
1H-INDAZOLE-4-CARBALDEHYDE Suppliers
- Tel
- --
- Fax
- --
- sales@apolloscientific.co.uk
- Country
- United Kingdom
- ProdList
- 6084
- Advantage
- 88
View Lastest Price from 1H-INDAZOLE-4-CARBALDEHYDE manufacturers
- Product
- 1H-INDAZOLE-4-CARBALDEHYDE 669050-70-8
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2019-12-31