4-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE
- Product Name
- 4-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE
- CAS No.
- 320-43-4
- Chemical Name
- 4-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE
- Synonyms
- 4-Chloro-2-(trifluoromethyl)benzald;2-TRIFLUOROMETHYL-4-CHLOROBENZALDEHYDE;4-Chloro-2-fluoro-7-methoxyacetophenone;2-(Trifluoromthyl)-4-Chlorobenzaldehyde;4-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE;Benzaldehyde, 4-chloro-2-(trifluoromethyl)-;4-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE, 97%+
- CBNumber
- CB2418832
- Molecular Formula
- C8H4ClF3O
- Formula Weight
- 208.57
- MOL File
- 320-43-4.mol
4-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE Property
- Boiling point:
- 218.5±40.0 °C(Predicted)
- Density
- 1.423±0.06 g/cm3(Predicted)
- refractive index
- 1.4960
- storage temp.
- 2-8°C, stored under nitrogen
- form
- liquid
- color
- Clear, colourless
- Sensitive
- Air Sensitive
- CAS DataBase Reference
- 320-43-4(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- C432915
- Product name
- 4-Chloro-2-(trifluoromethyl)benzaldehyde
- Packaging
- 250mg
- Price
- $55
- Updated
- 2021/12/16
- Product number
- C432915
- Product name
- 4-Chloro-2-(trifluoromethyl)benzaldehyde
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 2815-7-24
- Product name
- 4-Chloro-2-(trifluoromethyl)benzaldehyde
- Purity
- 97%
- Packaging
- 5G
- Price
- $23
- Updated
- 2021/12/16
- Product number
- 2815-7-24
- Product name
- 4-Chloro-2-(trifluoromethyl)benzaldehyde
- Purity
- 97%
- Packaging
- 25g
- Price
- $93
- Updated
- 2021/12/16
- Product number
- J94823
- Product name
- 4-Chloro-2-(trifluoromethyl)benzaldehyde
- Packaging
- 100g
- Price
- $240
- Updated
- 2021/12/16
4-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE Chemical Properties,Usage,Production
Synthesis
320-41-2
320-43-4
The general procedure for the synthesis of 4-chloro-2-trifluoromethylbenzaldehyde using 2-trifluoromethyl-4-chlorobenzonitrile as a starting material was as follows: 2-trifluoromethyl-4-chlorobenzonitrile (appropriate amount) was added to a mixed solution of formic acid (96%, 15 mL) and water (3 mL). Nickel-aluminum alloy (1260 mg) was then added. The reaction mixture was heated and reacted at 100 °C overnight. Upon completion of the reaction, the reaction mixture was diluted with ethyl acetate and filtered through diatomaceous earth to remove solid impurities. The filtrate was sequentially extracted with 1N sodium hydroxide solution and saturated aqueous sodium chloride solution. The organic phase was dried with anhydrous sodium sulfate, filtered and concentrated to give 4-chloro-2-trifluoromethylbenzaldehyde (555 mg, 87% yield). The product was characterized by 1HNMR (400 MHz, MeOH-d4): δ 10.29 (m, 1H), 8.10 (d, 1H, J = 8.4 Hz), 7.91 (d, 1H, J = 1.6 Hz), 7.85 (dd, 1H, J = 8.4,1.6 Hz).
References
[1] Patent: WO2006/44454, 2006, A1. Location in patent: Page/Page column 63
4-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE manufacturers
- Product
- 4-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE 320-43-4
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20 mt
- Release date
- 2024-11-25
- Product
- 4-CHLORO-2-(TRIFLUOROMETHYL)BENZALDEHYDE 320-43-4
- Price
- US $3.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2020-01-31