4-(4-OXOCYCLOHEXYL)BENZONITRILE

Product Name: 4-(4-OXOCYCLOHEXYL)BENZONITRILE
CAS No.: 73204-07-6
Chemical Name: 4-(4-OXOCYCLOHEXYL)BENZONITRILE
Synonyms: 4-(p-Cyanophenyl)cyclohexanone;4-(4-OXOCYCLOHEXY)BENZONITRILE;4-(4-OXOCYCLOHEXYL)BENZONITRILE;4-(4-CYANOPHENYL) CYCLOHEXANONE;4-(4'-cyanophenyl)cyclohexanone;Benzonitrile, 4-(4-oxocyclohexyl)-;4-(4-hydroxycyclohexyl) benzonitrile
CBNumber: CB2442682
Molecular Formula: C13H13NO
Formula Weight: 199.25
MOL File: 73204-07-6.mol

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4-(4-OXOCYCLOHEXYL)BENZONITRILE Property

Boiling point:: 367.3±42.0 °C(Predicted)
Density: 1.12±0.1 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid

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Safety

HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: O990080
Product name: 4-(4-Oxocyclohexyl)benzonitrile
Packaging: 10mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC149461
Product name: 4-(4-Cyanophenyl)cyclohexanone
Packaging: 500mg
Price: $80
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC149461
Product name: 4-(4-Cyanophenyl)cyclohexanone
Packaging: 1g
Price: $141
Updated: 2021/12/16

AK Scientific

Product number: J51500
Product name: 4-(4-Cyanophenyl)cyclohexanone
Packaging: 10g
Price: $240
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC149461
Product name: 4-(4-Cyanophenyl)cyclohexanone
Packaging: 2g
Price: $245
Updated: 2021/12/16

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4-(4-OXOCYCLOHEXYL)BENZONITRILE Chemical Properties,Usage,Production

Chemical Properties

white crystalline

Synthesis

73204-06-5

73204-07-6

The general procedure for the synthesis of 4-(4'-benzonitrile)cyclohexanone from 4-benzamide-cyclohexanone is as follows: to a 50 ml solution of dichloromethane containing 4.8 g (22.1 mmol) of 4-(4-oxocyclohexyl)benzamide, 3.0 ml (24.3 mmol) of pivaloyl chloride and 2.14 ml (26.5 mmol) of pyridine were sequentially added at room temperature. . The reaction mixture was stirred overnight. After completion of the reaction, the reaction solution was diluted with 50 ml of dichloromethane and washed three times with water. The organic phase was separated and dried over anhydrous magnesium sulfate and subsequently concentrated. Purification by fast column chromatography (silica gel as stationary phase and petroleum ether/ethyl acetate 1:1→1:4 as eluent) gave 700 mg (16% yield) of the target product. The structure of the product was confirmed by 1H NMR (CDCl3): δ 7.61 (d, 2H), 7.36 (d, 2H), 3.09 (m, 1H), 2.51 (m, 4H), 2.25 (m, 2H), 1.96 (m, 2H).

References

[1] Patent: WO2010/97410, 2010, A1. Location in patent: Page/Page column 128-129
[2] Patent: US2012/40942, 2012, A1. Location in patent: Page/Page column 59-60

4-(4-OXOCYCLOHEXYL)BENZONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(4-OXOCYCLOHEXYL)BENZONITRILE Suppliers

China 80 Europe 1 Germany 1 India 1 United Kingdom 2 United States 8 Global 93

3B Pharmachem (Wuhan) International Co.,Ltd.

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Shanghai Topbiochem Technology Co., Ltd

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View Lastest Price from 4-(4-OXOCYCLOHEXYL)BENZONITRILE manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 4-(4-OXOCYCLOHEXYL)BENZONITRILE 73204-07-6
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1ton
Release date: 2022-09-28

Henan Fengda Chemical Co., Ltd

Product: 4-(4-Oxocyclohexyl)benzonitrile 73204-07-6
Price: US $8.00-0.60/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-01-14

LY Global chemicals co.,ltd .

Product: 4-(4-OXOCYCLOHEXYL)BENZONITRILE 73204-07-6
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98.0%
Supply Ability: 1000kg
Release date: 2023-04-05

73204-07-6, 4-(4-OXOCYCLOHEXYL)BENZONITRILERelated Search:

Cyclohexanone, 4-(4-chlorophenyl)- 4-[P-(BENZYLOXY)PHENYL]CYCLOHEXANONE 4-(4-fluorophenyl)cyclohexanone 4-(4-Nitrophenyl)cyclohexanone 4-Methyl-4-phenylcyclohexanone 4-(4-BROMOPHENYL)CYCLOHEXANONE 4-(3'-fluorophenyl)-cyclohexanone 4-(4-Fluorophenyl)-4-hydroxycyclohexanone 4-(4-Methylphenyl)cyclohexanone 4-CYANO-4-(3-METHOXYPHENYL)CYCLOHEXANONE 4-CYANO-4-(3,4-DIMETHOXYPHENYL)CYCLOHEXANONE 4-(3-METHOXYPHENYL)CYCLOHEXANONE 1-[3-(CYCLOPENTYLOXY)-4-METHOXYPHENYL]-4-OXOCYCLOHEXANE-1-CARBONITRILE 4-(4-OXOCYCLOHEXYL)BENZONITRILE Cyclohexanone 4-Phenylcyclohexanone BENZONITRILE, 4-CYCLOHEXYL- 4-(2,4-dioxocyclohexyl)benzenecarbonitrile

4-(p-Cyanophenyl)cyclohexanone

4-(4-hydroxycyclohexyl) benzonitrile

4-(4-OXOCYCLOHEXY)BENZONITRILE

4-(4-CYANOPHENYL) CYCLOHEXANONE

4-(4-OXOCYCLOHEXYL)BENZONITRILE

Benzonitrile, 4-(4-oxocyclohexyl)-

4-(4'-cyanophenyl)cyclohexanone

73204-07-6

Liqiud crystal intermediates