N1-(4-Chlorophenyl)benzene-1,2-diamine

Product Name: N1-(4-Chlorophenyl)benzene-1,2-diamine
CAS No.: 68817-71-0
Chemical Name: N1-(4-Chlorophenyl)benzene-1,2-diamine
Synonyms: TIMTEC-BB SBB003366;2-(4-Chloroanilino)aniline;4'-Chloro-2-aminodiphenylamine;2-AMINO-4'-CHLORODIPHENYLAMINE;N1-(4-Chlorophenyl)-2-amino-aniline;N-(4-Chorophenyl)-1,2-benzenediamine;(2-aminophenyl)(4-chlorophenyl)amine;N-(4-CHLOROPHENYL)-1,2-BENZENEDIAMINE;N-(4-chlorophenyl)benzene-1,2-diamine;N-(4-Chlorophenyl)-1,2-benzenediamone
CBNumber: CB2467496
Molecular Formula: C12H11ClN2
Formula Weight: 218.68
MOL File: 68817-71-0.mol

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N1-(4-Chlorophenyl)benzene-1,2-diamine Property

Melting point:: 117-119 °C(lit.)
Boiling point:: 357.0±27.0 °C(Predicted)
Density: 1.288±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
pka: 4.90±0.10(Predicted)
Appearance: Brown to reddish brown Solid
InChI: InChI=1S/C12H11ClN2/c13-9-5-7-10(8-6-9)15-12-4-2-1-3-11(12)14/h1-8,15H,14H2
InChIKey: WEUBIWJPIRTWDF-UHFFFAOYSA-N
SMILES: C1(NC2=CC=C(Cl)C=C2)=CC=CC=C1N

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36
WGK Germany: 3
HS Code: 2921599090
Storage Class: 11 - Combustible Solids
Hazard Classifications: Eye Irrit. 2
Skin Irrit. 2
STOT SE 3

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 327522
Product name: N-(4-Chlorophenyl)-1,2-phenylenediamine
Purity: 97%
Packaging: 25g
Price: $275
Updated: 2025/07/31

TRC

Product number: C377770
Product name: N-(4-Chlorophenyl)-1,2-phenylenediamine
Packaging: 1g
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FN63116
Product name: N-(4-Chlorophenyl)-1,2-benzenediamone
Packaging: 2g
Price: $50
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FN63116
Product name: N-(4-Chlorophenyl)-1,2-benzenediamone
Packaging: 5G
Price: $100
Updated: 2021/12/16

AK Scientific

Product number: X6178
Product name: 2-Amino-4-Chlorodiphenylamine
Packaging: 5g
Price: $111
Updated: 2021/12/16

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N1-(4-Chlorophenyl)benzene-1,2-diamine Chemical Properties,Usage,Production

Uses

N-(4-Chlorophenyl)-1,2-phenylenediamine is a reagent in the synthesis of clofazimine analogs as antileishmanials and antiplasmodials.

Uses

N-(4-Chlorophenyl)-1,2-phenylenediamine (2-Amino-4′-chlorodiphenylamine) was used in preparation of N-(p-chloro)phenylbenzimidazolin-2-one and monoaminophenazine dyes.

Synthesis

To a mixture of EtOH (100 ml) and NH4C1 saturated solution (15 ml), N-(4-chlorophenyl)-2-nitrobenzenamine (5.0 g, 20.1 mmol) was added, followed by iron powder (4.0 g). The reaction mixture was heated at 70 °C for 2h. The solid was filtered, and the filtrate was extracted by EA (100 mL x 3) and dried over Na2S04. After the solvent was removed, the mixture was purified by Combi-flash (PE: EA = 5 : 1) to give N1-(4-Chlorophenyl)benzene-1,2-diamine (4.1 g, 93.2 percent) as a light yellow solid.

References

[1] Chinese Journal of Chemistry, 2013, vol. 31, # 12, p. 1473 - 1482
[2] Organic Process Research and Development, 2016, vol. 20, # 2, p. 452 - 464
[3] Patent: WO2012/151512, 2012, A2. Location in patent: Page/Page column 103-104
[4] ACS Medicinal Chemistry Letters, 2016, vol. 7, # 2, p. 145 - 150
[5] Patent: CN107445845, 2017, A. Location in patent: Paragraph 0047; 0048; 0049; 0050; 0051; 0052

N1-(4-Chlorophenyl)benzene-1,2-diamine Preparation Products And Raw materials

Raw materials

Preparation Products

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N1-(4-Chlorophenyl)benzene-1,2-diamine Suppliers

China 83 India 9 Switzerland 2 United Kingdom 5 United States 11 Global 110

Sinfachem Limited.

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Hangzhou J&H Chemical Co., Ltd.

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View Lastest Price from N1-(4-Chlorophenyl)benzene-1,2-diamine manufacturers

Honest Joy Holdings Limited

Product: 2-N-(4-chlorophenyl)benzene-1,2-diamine 68817-71-0
Price: US $0.00/KG
Min. Order: 1KG
Purity: 98.3%
Supply Ability: 100 tons
Release date: 2022-01-14

Career Henan Chemical Co

Product: 2-AMINO-4'-CHLORODIPHENYLAMINE 68817-71-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95%-99%
Supply Ability: 100KG
Release date: 2019-07-31

68817-71-0, N1-(4-Chlorophenyl)benzene-1,2-diamineRelated Search:

Clofazimine o-Phenylenediamine 4-CHLORODIPHENYLAMINE 4-amino-4'-chlorodiphenylamine-2-sulfonic acid 2-AMINO-4-CHLORODIPHENYLAMINE 2-AMINO-4-CHLORODIPHENYLAMINE 4-AMINO-4'-CHLORODIPHENYLAMINE-2-SULPHONIC ACID 5-AMINO-2-CHLORO-10H-ACRIDIN-9-ONE 2-chloro-11-(4-methyl-1-piperazinyl)-5H-dibenzo(b,e)(1,4)diazepine N-(4-CHLOROPHENYL)-2-NITROBENZENAMINE CLOFAZIMINE, [METHYL-3H] N1-(4-Chlorophenyl)benzene-1,2-diamine 1-(4-CHLOROPHENYL)-3-HYDROXY-1,2-DIHYDROQUINOXALIN-2-ONE

2-AMINO-4'-CHLORODIPHENYLAMINE

TIMTEC-BB SBB003366

N-(4-CHLOROPHENYL)-1,2-PHENYLENEDIAMINE

N-(4-chlorophenyl)benzene-1,2-diamine

N-(4-CHLOROPHENYL)-1,2-BENZENEDIAMINE

(2-aminophenyl)(4-chlorophenyl)amine(SALTDATA: FREE)

1,2-Benzenediamine, N-(4-chlorophenyl)-

N1-(4-Chlorophenyl)benzene-1,2-diaMine

N1-(4-Chlorophenyl)-2-amino-aniline

N-(4-chlorophenyl)-1,2-phenylinediamine

4'-Chloro-2-aminodiphenylamine

N-(4-Chlorophenyl)-1,2-benzenediamone

N - (4-chlorobenzene) - 1,2-phenylenediamine

1,2-Benzenediamine, N1-(4-chlorophenyl)-

N-(4-Chorophenyl)-1,2-benzenediamine

(2-aminophenyl)(4-chlorophenyl)amine

N1-(4-Chlorophenyl)-1,2-benzenediamine

2-(4-Chloroanilino)aniline

<i>N</i>-(4-Chlorophenyl)-1,2-phenylenediamine

68817-71-0

C12H11ClN2

ClC6H4NHC6H4NH2

Nitrogen Compounds

Organic Building Blocks

Polyamines

Building Blocks