3,3,4,4-diphenylsulfonetetracarboxylicdianhydride

Uses

Product Name: 3,3,4,4-diphenylsulfonetetracarboxylicdianhydride
CAS No.: 2540-99-0
Chemical Name: 3,3,4,4-diphenylsulfonetetracarboxylicdianhydride
Synonyms: DSDA;5,5'-Sulfonylbis(isobenzofuran-1,3-dione);SO2DPA;4,4'-SULFONYLDIPHTHALIC ANHYDRIDE;4,4'-Sulfonyldiphthalic dianhydride;5,5'-Sulfonylbis-1,3-isobenzofurandione;diphenylsulfonetetracarboxylicdianhydride;1,3-Isobenzofurandione, 5,5'-sulfonylbis-;5,5'-Sulfonylbis(isobenzofuran-1,3-dione);3,3',4,4'-Diphenylsulfonetetracarboxylic ,97%
CBNumber: CB2480514
Molecular Formula: C16H6O8S
Formula Weight: 358.28
MOL File: 2540-99-0.mol

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3,3,4,4-diphenylsulfonetetracarboxylicdianhydride Property

Melting point:: 283 °C
Boiling point:: 718.5±45.0 °C(Predicted)
Density: 1.755±0.06 g/cm3(Predicted)
vapor pressure: 0-0Pa at 20-50℃
storage temp.: Inert atmosphere,Room Temperature
form: Powder
InChI: InChI=1S/C16H6O8S/c17-13-9-3-1-7(5-11(9)15(19)23-13)25(21,22)8-2-4-10-12(6-8)16(20)24-14(10)18/h1-6H
InChIKey: ZHBXLZQQVCDGPA-UHFFFAOYSA-N
SMILES: S(C1C=CC2C(=O)OC(=O)C=2C=1)(C1C=CC2C(=O)OC(=O)C=2C=1)(=O)=O
CAS DataBase Reference: 2540-99-0
NIST Chemistry Reference: Bis-(3-phthalyl anhydride) sulfone(2540-99-0)
EPA Substance Registry System: 1,3-Isobenzofurandione, 5,5'-sulfonylbis- (2540-99-0)

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Safety

HS Code: 2917.39.7000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical

Product number: D4554
Product name: 5,5'-Sulfonylbis(isobenzofuran-1,3-dione)
Packaging: 25G
Price: $345
Updated: 2024/03/01

TCI Chemical

Product number: D4554
Product name: 3,3',4,4'-Diphenylsulfonetetracarboxylic Dianhydride (purified by sublimation)
Purity: >99.0%(HPLC)(T)
Packaging: 1g
Price: $95
Updated: 2021/12/16

TCI Chemical

Product number: D4554
Product name: 3,3',4,4'-Diphenylsulfonetetracarboxylic Dianhydride (purified by sublimation)
Purity: >99.0%(HPLC)(T)
Packaging: 5g
Price: $115
Updated: 2024/03/01

TRC

Product number: D492243
Product name: 3,3'',4,4''-Diphenylsulfonetetracarboxylicdianhydride
Packaging: 5g
Price: $130
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD62693
Product name: 3,3',4,4'-Diphenylsulfonetetracarboxylic Dianhydride
Packaging: 2g
Price: $140
Updated: 2021/12/16

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3,3,4,4-diphenylsulfonetetracarboxylicdianhydride Chemical Properties,Usage,Production

Uses

3,3',4,4'-Diphenylsulfonetetracarboxylic dianhydride is a novel class of human immunodeficiency virus type 1 integrase inhibitors.

Application

3,3',4,4'-Diphenylsulfonetetracarboxylic Dianhydride (DSDA) and 1,1-Bis[4-(4-aminophenoxy)phenyl]-1-phenylethane (BAPPE) can be used as raw materials for the synthesis of novel organosoluble polyimides and copolyimides. These polyimides and copolyimides have good mechanical properties and thermal stability.

Synthesis

4-Bromophthalic anhydride (purity 99.5%) 22.7g (0.10 mol), sodium sulfide 9 hydrate 13. 2g (0.055 mol) and γ-butyrolactone 200 g were allowed to react for 8 hours under reflux 200 ~ 205°C while stirring. 5ml of water was added to the reaction mixture 0.5g, boiled for 1 hour, this solution was analyzed by HPLC. The reaction rate of 4-Bromophthalic anhydride was 99.9%, yield of 4,4'-thiodiphthalic anhydride was 93%. γ-Butyrolactone from the reaction mixture was distilled off under reduced pressure, acetic acid 200g was added to the obtained residual substance solid, and the heating dissolution was carried out. This solution was cooled to room temperature, the precipitated crystals were filtered off and then under reduced pressure, and dried for 1 hour at 100°C. Purified 4,4'-Thiodiphthalic anhydride 23.5g (isolated yield 72%) was obtained. The purity was 99.6% from the analysis by HPLC.
Then, the resulting 4,4'-Thiodiphthalic anhydride 20.0g (0.061 mol), 12-tungstophosphoric acid (H3PW12O40 · 30H2O) 1.0g and acetic acid 250g were charged to four-necked flask made of glass equipped with reflux condenser, thermometer, dropping funnel and stirrer, dissolved by heating to 110°C. Cooled to 80°C, under stirring, the reaction temperature was maintained at 80°C and 9% peracetic acid· acetic acid solution 77.5g (0.091 mol) was added dropwise and takes 4 hours, further reacted for 2 hours. The reaction mixture was cooled to 15°C, the obtained crystals were then filtered, under reduced pressure, and dried for 3 hours at 100°C. 4,4'-Sulfonyldiphthalic anhydride 19.9g (isolation yield 91%) was obtained. This thing was analyzed by HPLC as hydrolysis, as a result purity was 98.9%.

3,3,4,4-diphenylsulfonetetracarboxylicdianhydride Preparation Products And Raw materials

Raw materials

Sodium sulfide nonahydrate Acetic anhydride Acetone Hydrogen peroxide Phosphotungstic acid 44-hydrate Phthalic anhydride Hydrochloric acid Government regulation Acetic acid Sodium hydroxide PETROLEUM ETHER Gamma Butyrolactone

Preparation Products

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3,3,4,4-diphenylsulfonetetracarboxylicdianhydride Suppliers

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View Lastest Price from 3,3,4,4-diphenylsulfonetetracarboxylicdianhydride manufacturers

Hebei Weibang Biotechnology Co., Ltd

Product: 3,3',4,4'-DIPHENYLSULFONETETRACARBOXYLIC DIANHYDRIDE 2540-99-0
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 500000kg
Release date: 2024-10-30

Hebei Yanxi Chemical Co., Ltd.

Product: 3,3',4,4'-DIPHENYLSULFONETETRACARBOXYLIC DIANHYDRIDE 2540-99-0
Price: US $0.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 20 tons
Release date: 2023-03-09

CHINATECH(TIANJIN) CHEMICAL CO.,LTD.

Product: 3,3,4,4-diphenylsulfonetetracarboxylicdianhydride (DSDA) 2540-99-0
Price: US $0.00/Kg/Drum
Min. Order: 1KG
Purity: ≥99%
Supply Ability: 100KG
Release date: 2021-12-15

2540-99-0, 3,3,4,4-diphenylsulfonetetracarboxylicdianhydrideRelated Search:

4-Benzenesulfonylbenzoic acid 3,3,4,4-diphenylsulfonetetracarboxylicdianhydride Methyl 4-Mercaptobenzoate Phthalic anhydride 4,4'-Dimethyldiphenylsulfoxide DI-P-TOLYL SULFONE 4-(METHYLTHIO)BENZOIC ACID 4-(PHENYLTHIO)BENZALDEHYDE 4-(Methylthio)benzaldehyde 4-Mercaptobenzoic acid 3-Methylthioanisole 4-METHYLDIPHENYL SULFIDE 3-(Methylsulfonyl)benzaldehyde 4,4'-SULFONYLBIS-BENZOIC ACID 3-(Methylthio)benzoic acid 3-(METHYLSULFONYL)BENZOIC ACID 4-(Methylthio)benzyl alcohol 4-Methylsulphonylbenzoic acid

3,3',4,4'-DIPHENYLSULFONETETRACARBOXYLIC DIANHYDRIDE

DSDA

4,4'-SULFONYLDIPHTHALIC ANHYDRIDE

5,5'-Sulfonylbis-1,3-isobenzofurandione

4,4'-Sulfonyldiphthalic dianhydride

diphenylsulfonetetracarboxylicdianhydride

3,3,4,4''-DIPHENYLSULFONETETRACARBOXYLIC DIANHYDRIDE 96+%

4,4'-Sulfonylbis(benzene-1,2-dicarboxylic acid)1,2:1',2'-dianhydride

4,4'-Sulfonylbisphthalic 1,2:1',2'-dianhydride

4,4'-Sulfonylbisphthalic acid-1,2:1',2'-dianhydride

SO2DPA

5-(1,3-diketoisobenzofuran-5-yl)sulfonylisobenzofuran-1,3-quinone

5-[(1,3-dioxo-2-benzofuran-5-yl)sulfonyl]-2-benzofuran-1,3-dione

3,3',4,4'-Diphenylsulfonetetracarboxylic ,97%

3,3',4,4'-Diphenylsulfonetetracarboxylic Dianhydride (purified by sublimation)

5,5'-Sulfonylbis(isobenzofuran-1,3-dione)

diphenylsulfone-3,3',4,4'-tetracarboxylic dianhydride

3,3',4,4'-Diphenylsulfonetetracarboxylic Dianhydride (purified by sublimation) &gt

3,3',4,4'-DiphenylsulfonetetracarboxylicDianhydride&gt

1,3-Isobenzofurandione, 5,5'-sulfonylbis-

3,3,4,4-diphenylsulfonetetracarboxylicdianhydride (DSDA)

g3,3',4,4'-Diphenylsulfonetetracarboxylic dianhydride

3,3',4,4'-diphenylsulfonetetracarboxylic acid dianhydride DSDA

3,3',4,4'-Diphenylsulfonetetracarboxylic Dianhydride

5,5'-Sulfonylbis(isobenzofuran-1,3-dione)

3,3,4,4-Diphenyl sulfone tetracarboxylic dianhydride (s- DSDA)

2540-99-0

C16H6O8S

00000

Reagent for High-Performance Polymer Research

Diphenyl Sulfones (for High-Performance Polymer Research)

Aromatic Tetracarboxylic Dianhydrides (for High-Performance Polymer Research)

Diphenyl Sulfones (for High-Performance Polymer Research)

Functional Materials

Reagent for High-Performance Polymer Research