10-Bromodecanol
- Product Name
- 10-Bromodecanol
- CAS No.
- 53463-68-6
- Chemical Name
- 10-Bromodecanol
- Synonyms
- 10-BROMODECAN-1-OL;10-BROMODECANOL;10-Bromo-1-decan;10-bromo-1-decano;10-BROMO-1-DECANOL;1-bromo-10-decanol;1-Decanol, 10-bromo-;10-Bromo-1-decanol,95%;10-Bromo-1-decanol >10-BROMO-1-DECANOL 85+%
- CBNumber
- CB2490678
- Molecular Formula
- C10H21BrO
- Formula Weight
- 237.18
- MOL File
- 53463-68-6.mol
10-Bromodecanol Property
- Boiling point:
- 165-169 °C/10 mmHg (lit.)
- Density
- 1.19 g/mL at 25 °C (lit.)
- refractive index
- n20/D 1.476(lit.)
- Flash point:
- >230 °F
- storage temp.
- Inert atmosphere,Store in freezer, under -20°C
- solubility
- Chloroform (Sparingly)
- form
- Liquid
- pka
- 15.20±0.10(Predicted)
- color
- Clear yellow
- Water Solubility
- It is miscible with water.
- BRN
- 1738593
- Stability:
- Moisture Sensitive
- InChIKey
- LGZMUUBPTDRQQM-UHFFFAOYSA-N
- CAS DataBase Reference
- 53463-68-6(CAS DataBase Reference)
- EPA Substance Registry System
- 1-Decanol, 10-bromo- (53463-68-6)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 310891
- Product name
- 10-Bromo-1-decanol
- Purity
- technical grade, 90%
- Packaging
- 5g
- Price
- $105.45
- Updated
- 2025/07/31
- Product number
- B1730
- Product name
- 10-Bromo-1-decanol
- Purity
- >85.0%(GC)
- Packaging
- 5g
- Price
- $95
- Updated
- 2025/07/31
- Product number
- B1730
- Product name
- 10-Bromo-1-decanol
- Purity
- >85.0%(GC)
- Packaging
- 25g
- Price
- $290
- Updated
- 2025/07/31
- Product number
- B688690
- Product name
- 10-Bromo-1-decanol
- Packaging
- 10g
- Price
- $130
- Updated
- 2021/12/16
- Product number
- B688690
- Product name
- 10-Bromo-1-decanol
- Packaging
- 25g
- Price
- $225
- Updated
- 2021/12/16
10-Bromodecanol Chemical Properties,Usage,Production
Chemical Properties
Clear yellow liquid
Uses
10-Bromo-1-decanol is used as an important raw material and intermediate used in organic Synthesis, pharmaceuticals, agrochemicals and dyestuff. It was also used in the synthesis of (11Z,13Z)-11,13-hexadecadienal, the female sex pheromone of the navel orangeworm (Amyelois transitella).
Uses
10-Bromodecanol can be used to synthesize rotaxane dendrimers. It can also be used to synthesize J2326, a molecule that induces neurite outgrowth in neuronal cells.
Definition
ChEBI: 10-Bromo-1-decanol is a primary alcohol.
Synthesis
112-47-0
53463-68-6
General procedure for the synthesis of 10-bromo-1-decanol from 1,10-decanediol: 1,10-decanediol (10 g, 57.47 mmol) was dissolved in toluene (600 mL) and transferred to a 1 L two-necked, round-bottomed flask fitted with a Dean-Stark separator. 48% hydrobromic acid (7.15 mL, 63.21 mmol) was slowly added to the reaction system and subsequently heated to reflux for 16 hours. After completion of the reaction, it was cooled to room temperature and the reaction mixture was washed sequentially with 1 N hydrochloric acid, 2 M aqueous sodium hydroxide, deionized water and saturated saline. The organic phase was separated, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography (eluent: 15% ethyl acetate/hexane) to afford 10-bromo-1-decanol as a colorless transparent oil (12.7 g, 93% yield). Thin layer chromatography (TLC) Rf = 0.45 (unfolding agent: 20% ethyl acetate/hexane); 1H NMR (500 MHz, CDCl3): δ 3.63 (t, J = 5.8 Hz, 2H), 3.39 (t, J = 6.8 Hz, 2H), 1.85 (m, 2H), 1.56 (m, 2H), 1.42 (m, 2H), 1.38- 1.27 (m, 10H); 13C NMR (125 MHz, CDCl3): δ 62.9, 33.9, 32.7, 32.6, 29.3, 29.2, 29.2, 28.6, 28.0, 25.6; infrared spectra (neat sample): νmax 2927, 2856, 1738, 1593, 1449, 1367, 1241 cm-1; high-resolution mass spectrum (ESI): calculated value C10H22BrO [M + H]+ 237.0854, measured value 237.0845.
References
[1] Tetrahedron, 2015, vol. 71, # 7, p. 1058 - 1067
[2] Bioorganic and Medicinal Chemistry, 2010, vol. 18, # 3, p. 1083 - 1092
[3] ACS Medicinal Chemistry Letters, 2010, vol. 1, # 6, p. 273 - 276
[4] Bioorganic and Medicinal Chemistry, 2011, vol. 19, # 1, p. 567 - 579
[5] Patent: EP1818336, 2007, A1. Location in patent: Page/Page column 7
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View Lastest Price from 10-Bromodecanol manufacturers
- Product
- 10-Bromodecanol 53463-68-6
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20 mt
- Release date
- 2024-11-22
- Product
- 10-Bromodecanol 53463-68-6
- Price
- US $40.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 5000kg/week
- Release date
- 2024-05-30
- Product
- 10-Bromodecanol 53463-68-6
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-10-14