ChemicalBook > CAS DataBase List > 3-Iodo-4-hydroxybenzaldehyde

3-Iodo-4-hydroxybenzaldehyde

Product Name
3-Iodo-4-hydroxybenzaldehyde
CAS No.
60032-63-5
Chemical Name
3-Iodo-4-hydroxybenzaldehyde
Synonyms
AKOS B029221;4-Formyl-2-iodophenol;4-Hyroxy-3-iodobenzaldehyde;4-HYDRO-3-IODO-BENZALDEHYDE;3-IODO-4-HYDROXYBENZALDEHYDE;4-HYDROXY-3-IODOBENZALDEHYDE;Benzaldehyde, 4-hydroxy-3-iodo-
CBNumber
CB2670579
Molecular Formula
C7H5IO2
Formula Weight
248.02
MOL File
60032-63-5.mol
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3-Iodo-4-hydroxybenzaldehyde Property

Melting point:
128-130°C
Boiling point:
257.8±25.0 °C(Predicted)
Density 
2.039±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
solubility 
DMSO (Slightly), Methanol (Slightly)
form 
Solid
pka
6.33±0.18(Predicted)
color 
White to Pale Beige
InChI
InChI=1S/C7H5IO2/c8-6-3-5(4-9)1-2-7(6)10/h1-4,10H
InChIKey
KNQVIRRXVOTGGT-UHFFFAOYSA-N
SMILES
C(=O)C1=CC=C(O)C(I)=C1
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
I707250
Product name
3-Iodo-4-hydroxybenzaldehyde
Packaging
5g
Price
$1265
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0012587
Product name
3-IODO-4-HYDROXYBENZALDEHYDE
Purity
95.00%
Packaging
500MG
Price
$808.5
Updated
2021/12/16
Matrix Scientific
Product number
181582
Product name
4-Hydroxy-3-iodobenzaldehyde
Purity
95%
Packaging
10g
Price
$990
Updated
2021/12/16
Matrix Scientific
Product number
181582
Product name
4-Hydroxy-3-iodobenzaldehyde
Purity
95%
Packaging
25g
Price
$1650
Updated
2021/12/16
AK Scientific
Product number
X5653
Product name
4-Hydroxy-3-iodobenzaldehyde
Packaging
25g
Price
$2548
Updated
2021/12/16
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3-Iodo-4-hydroxybenzaldehyde Chemical Properties,Usage,Production

Chemical Properties

White Solid

Uses

3-Iodo-4-hydroxybenzaldehyde (cas# 60032-63-5) is a compound useful in organic synthesis.

Synthesis

123-08-0

60032-63-5

General procedure for the synthesis of 4-hydroxy-3-iodobenzaldehyde from 4-hydroxybenzaldehyde: To a stirred solution of 4-hydroxybenzaldehyde (2.0 g, 16.39 mmol) in acetic acid (30 mL) was added N-iodosuccinimide (4.5 g, 19.67 mmol). The reaction mixture was stirred at room temperature for 16 hours and then filtered. The filtrate was poured into water (100 mL) and ethyl acetate (50 mL) was added. The aqueous phase was separated and then extracted with ethyl acetate (3 x 50 mL). The organic phases were combined, washed with water (2 × 20 mL), dried over anhydrous sodium sulfate, filtered and concentrated in vacuo to give the title compound (2.0 g, 50% yield) as a white solid, which was ready to be used without further purification.LCMS (ES-) m/z 247.1 ([M-H]-) with a retention time of 1.44 min (Method 9).

References

[1] Organic Preparations and Procedures International, 2002, vol. 34, # 6, p. 647 - 651
[2] Journal of the Brazilian Chemical Society, 2010, vol. 21, # 1, p. 3 - 6
[3] Journal of Organic Chemistry, 2002, vol. 67, # 24, p. 8622 - 8624
[4] Synthesis, 2010, # 9, p. 1467 - 1472
[5] Bioorganic and Medicinal Chemistry Letters, 2011, vol. 21, # 2, p. 769 - 772

3-Iodo-4-hydroxybenzaldehyde Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Iodo-4-hydroxybenzaldehyde Suppliers

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View Lastest Price from 3-Iodo-4-hydroxybenzaldehyde manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
4-Hydroxy-3-iodobenzaldehyde 60032-63-5
Price
US $0.10-10.00/KG
Min. Order
0.10000000149011612KG
Purity
98%
Supply Ability
200TONS
Release date
2025-08-14
ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
Product
4-Hydroxy-3-iodobenzaldehyde 60032-63-5
Price
US $1.10-9.90/kg
Min. Order
1kg
Purity
99%min
Supply Ability
100kg
Release date
2025-08-14
Career Henan Chemical Co
Product
3-IODO-4-HYDROXYBENZALDEHYDE 60032-63-5
Price
US $1.00/g
Min. Order
1g
Purity
99%
Supply Ability
10000KGS
Release date
2020-01-09

60032-63-5, 3-Iodo-4-hydroxybenzaldehydeRelated Search:

Amiodarone hydrochloride 5-Iodovanillin Amiodarone METHYL 3-IODO-4-METHOXYBENZOATE 3-Iodo-4-methoxybenzoic acid 3,5-DIIODO-4-HYDROXYBENZALDEHYDE 3,5-DIIODO-4-HYDROXYBENZOIC ACID 4-HYDROXY-3-IODO-5-NITROBENZOIC ACID 3-Iodo-4,5-dimethoxybenzaldehyde 4-HYDROXY-3-IODOBENZOIC ACID 3-Iodo-2-hydroxybenzaldehyde 5-IODO-2-HYDROXYBENZALDEHYDE 3-Iodobenzaldehyde 3-(3,5-DIIODO-4-HYDROXYBENZOYL)-INDOLE METHYL 3,5-DIIODO-4-METHOXYBENZOATE 3,5-DIIODO-4-HYDROXYBENZHYDRAZIDE 4-(4'-HYDROXY-3'-IODOPHENOXY)-3,5-DIIODO-BENZOIC ACID 5-IODOVANILLIC ACID

  • 4-Formyl-2-iodophenol
  • 4-Hyroxy-3-iodobenzaldehyde
  • 3-IODO-4-HYDROXYBENZALDEHYDE
  • 4-HYDRO-3-IODO-BENZALDEHYDE
  • 4-HYDROXY-3-IODOBENZALDEHYDE
  • AKOS B029221
  • Benzaldehyde, 4-hydroxy-3-iodo-
  • 60032-63-5
  • Aromatics
  • Aromatic Aldehydes & Derivatives (substituted)