3,5-DIIODO-4-HYDROXYBENZALDEHYDE
- Product Name
- 3,5-DIIODO-4-HYDROXYBENZALDEHYDE
- CAS No.
- 1948-40-9
- Chemical Name
- 3,5-DIIODO-4-HYDROXYBENZALDEHYDE
- Synonyms
- NSC 72943;AKOS B028744;6-Fluoroacetophenone;Amiodarone Impurity 46;2,6-Diiodo-4-formylphenol;4-Hydroxy-3,5-diiodbenzaldehyd;Levothyroxine Sodium Impurity f;3,5-Diiodo-4-Hydroxybenzaldhyde;3,5-Diiodo-4-Hydroxybenzadehyde;3,5-DIIODO-4-HYDROXYBENZALDEHYDE
- CBNumber
- CB5406528
- Molecular Formula
- C7H4I2O2
- Formula Weight
- 373.91
- MOL File
- 1948-40-9.mol
3,5-DIIODO-4-HYDROXYBENZALDEHYDE Property
- Melting point:
- 202-203°C
- Boiling point:
- 284.1±40.0 °C(Predicted)
- Density
- 2.602±0.06 g/cm3(Predicted)
- storage temp.
- -20°C Freezer, Under Inert Atmosphere
- solubility
- Chloroform (Slightly, Sonicated), DMSO (Slightly)
- form
- Solid
- pka
- 4.89±0.23(Predicted)
- color
- White to Pale Yellow
- Water Solubility
- Insoluble in water. Sparingly soluble in chloroform and methanol.
- Sensitive
- Air & Light Sensitive
- BRN
- 1283414
- InChI
- InChI=1S/C7H4I2O2/c8-5-1-4(3-10)2-6(9)7(5)11/h1-3,11H
- InChIKey
- WHLUEIMENHLCMY-UHFFFAOYSA-N
- SMILES
- C(=O)C1=CC(I)=C(O)C(I)=C1
- CAS DataBase Reference
- 1948-40-9(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- H1539
- Product name
- 4-Hydroxy-3,5-diiodobenzaldehyde
- Purity
- >97.0%(T)
- Packaging
- 5g
- Price
- $62
- Updated
- 2025/07/31
- Product number
- H1539
- Product name
- 4-Hydroxy-3,5-diiodobenzaldehyde
- Purity
- >97.0%(T)
- Packaging
- 25g
- Price
- $182
- Updated
- 2025/07/31
- Product number
- D455080
- Product name
- 3,5-Diiodo-4-hydroxybenzaldehyde
- Packaging
- 500mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- D455080
- Product name
- 3,5-Diiodo-4-hydroxybenzaldehyde
- Packaging
- 5g
- Price
- $90
- Updated
- 2021/12/16
- Product number
- D455080
- Product name
- 3,5-Diiodo-4-hydroxybenzaldehyde
- Packaging
- 10g
- Price
- $110
- Updated
- 2021/12/16
3,5-DIIODO-4-HYDROXYBENZALDEHYDE Chemical Properties,Usage,Production
Chemical Properties
Pale Beige Solid
Uses
3,5-Diiodo-4-hydroxybenzaldehyde (cas# 1948-40-9) is a compound useful in organic synthesis.
Synthesis
3,5-Diiodo-4-hydroxybenzaldehyde was prepared as follows: in a 100 mL round bottom flask, 4-hydroxybenzaldehyde (1.0 g, 8.19 mmol), sodium periodate (1.75 g, 8.19 mmol), and NaCl (957 mg, 16.38 mmol) were dissolved in acetic acid (30 mL). H2O (3 mL) was added at room temperature. The reaction mixture was stirred at room temperature for 10 min, then potassium iodide (2.72 g, 16.4 mmol) was added and the reaction mixture was stirred at room temperature for 96 hours. The reaction mixture was diluted with EtOAc (25 mL) and 1 M aqueous sodium thiosulfate. The solution (25 mL) was added and the resulting mixture was stirred for 15 minutes. The solution was poured into 250 mLErlenmeyer and washed with EtOAc (50 mL) and 1 M aqueous sodium thiosulfate. solution (50mL) and the resulting solution was stirred for another 15 minutes. The organic layer was separated and the aqueous phase was further extracted with EtOAc (3 x 50 mL). The combined organic layers were washed with brine (100 mL), dried over Na2SO4, filtered and concentrated to dryness to afford 4-hydroxy-3,5-diiodobenzaldehyde (2.91 g, 95% yield) as a light yellow solid.
3,5-DIIODO-4-HYDROXYBENZALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3,5-DIIODO-4-HYDROXYBENZALDEHYDE manufacturers
- Product
- 3,5-DIIODO-4-HYDROXYBENZALDEHYDE 1948-40-9
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 2000
- Release date
- 2025-09-04
- Product
- 3,5-DIIODO-4-HYDROXYBENZALDEHYDE 1948-40-9
- Price
- US $840.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1-500kg
- Release date
- 2021-06-04
- Product
- 3,5-DIIODO-4-HYDROXYBENZALDEHYDE 1948-40-9
- Price
- US $0.10/KG
- Min. Order
- 1KG
- Purity
- 99.0%
- Supply Ability
- 1000 tons
- Release date
- 2020-04-24