5-CHLORO-2,3-DIPHENYL-1H-INDOLE
- Product Name
- 5-CHLORO-2,3-DIPHENYL-1H-INDOLE
- CAS No.
- 52598-02-4
- Chemical Name
- 5-CHLORO-2,3-DIPHENYL-1H-INDOLE
- Synonyms
- 5-Chloro-2,3-diphenylindole;5-CHLORO-2,3-DIPHENYL-1H-INDOLE;1H-Indole, 5-chloro-2,3-diphenyl-
- CBNumber
- CB2717584
- Molecular Formula
- C20H14ClN
- Formula Weight
- 303.78
- MOL File
- Mol file
5-CHLORO-2,3-DIPHENYL-1H-INDOLE Property
- Melting point:
- 130-131 °C(Solv: ethanol (64-17-5))
- Boiling point:
- 478.1±33.0 °C(Predicted)
- Density
- 1.243±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 15.63±0.30(Predicted)
- Appearance
- Light brown to brown Solid
- InChI
- InChI=1S/C20H14ClN/c21-16-11-12-18-17(13-16)19(14-7-3-1-4-8-14)20(22-18)15-9-5-2-6-10-15/h1-13,22H
- InChIKey
- BAEWCDBRAIDXMN-UHFFFAOYSA-N
- SMILES
- N1C2=C(C=C(Cl)C=C2)C(C2=CC=CC=C2)=C1C1=CC=CC=C1
N-Bromosuccinimide Price
- Product number
- C370173
- Product name
- 5-Chloro-2,3-diphenyl-1H-indole
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- C370173
- Product name
- 5-Chloro-2,3-diphenyl-1H-indole
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 094095
- Product name
- 5-Chloro-2,3-diphenyl-1H-indole
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $265
- Updated
- 2021/12/16
- Product number
- J97701
- Product name
- 5-Chloro-2,3-diphenyl-1H-indole
- Packaging
- 10g
- Price
- $450
- Updated
- 2021/12/16
- Product number
- 094095
- Product name
- 5-Chloro-2,3-diphenyl-1H-indole
- Purity
- 95+%
- Packaging
- 1g
- Price
- $588
- Updated
- 2021/12/16
5-CHLORO-2,3-DIPHENYL-1H-INDOLE Chemical Properties,Usage,Production
Synthesis
106-47-8
501-65-5
52598-02-4
4-Chloroaniline (76.5 mg, 0.6 mmol) and diphenylacetylene (71.3 mg, 0.4 mmol) were used as raw materials, and Cp*Rh(H2O)3(OTf)2 (11.8 mg, 5 mol%) was added to the reaction vials as a catalyst, acetic anhydride (59.0 μL, 0.6 mmol) as acylate, and 2.0 mL of tertiary amyl alcohol as the solvent. The reaction system was stirred at 100 °C for 24 h under oxygen atmosphere (1 atm). After completion of the reaction, NaOH (48 mg, 1.2 mmol) and methanol (2 mL) were added to the reaction mixture and stirring was continued for 2 hours. Subsequently, purification by column chromatography afforded the target compound 5-chloro-2,3-diphenyl-1H-indole (3ja) as a white solid in 90% yield.
References
[1] Chemical Communications, 2014, vol. 50, # 33, p. 4331 - 4334
[2] Patent: CN105218426, 2016, A. Location in patent: Paragraph 0039; 0040
5-CHLORO-2,3-DIPHENYL-1H-INDOLE Preparation Products And Raw materials
Raw materials
Preparation Products
5-CHLORO-2,3-DIPHENYL-1H-INDOLE Suppliers
- Tel
- 22-58627059 13920586291
- Fax
- 022-58620305
- zdcomcon@126.com
- Country
- China
- ProdList
- 3829
- Advantage
- 50
- Tel
- 021-54306202 13764082696
- info@hanhongsci.com
- Country
- China
- ProdList
- 42934
- Advantage
- 64
- Tel
- +86 21 61551611
- Fax
- +86 21 50676805
- Country
- China
- ProdList
- 9891
- Advantage
- 58
- Tel
- 021-60343070
- Fax
- 021-35122006
- Country
- China
- ProdList
- 12740
- Advantage
- 55
- Tel
- 400-164-7117 13681763483
- Fax
- +86-21-61629029
- product02@bidepharm.com
- Country
- China
- ProdList
- 39966
- Advantage
- 60
- Tel
- +86-0579-86846643 18072368515
- Fax
- +86-0579-86846643
- sales@honsentech.com.cn
- Country
- China
- ProdList
- 124
- Advantage
- 55
- Tel
- 0371-0371-55629727 13323845623
- Fax
- 037155629727
- 2885676761@qq.com
- Country
- China
- ProdList
- 10110
- Advantage
- 58
- Tel
- 571-89925085
- Fax
- 0086-571-89925065
- sales@amadischem.com
- Country
- China
- ProdList
- 131957
- Advantage
- 58
- Tel
- 0371-55900031 18137872243
- Fax
- QQ：2853979815
- 2853979815@qq.com
- Country
- China
- ProdList
- 9975
- Advantage
- 55
- Tel
- 025-66061636 18013972705
- Fax
- (3)02557626880
- qqyang@aikonchem.com
- Country
- China
- ProdList
- 15814
- Advantage
- 58
View Lastest Price from 5-CHLORO-2,3-DIPHENYL-1H-INDOLE manufacturers
- Product
- 5-CHLORO-2,3-DIPHENYL-1H-INDOLE 52598-02-4
- Price
- US $0.01/KG
- Min. Order
- 1KG
- Purity
- 98%; 99%
- Supply Ability
- 500g;1kg； 25kg
- Release date
- 2020-01-09