2-BROMO-1-BENZOFURAN
- Product Name
- 2-BROMO-1-BENZOFURAN
- CAS No.
- 54008-77-4
- Chemical Name
- 2-BROMO-1-BENZOFURAN
- Synonyms
- 2-BROMOBENZOFURAN;Benzofuran, 2-broMo-;2-Bromobenzo[b]furan;2-BROMO-1-BENZOFURAN;2-bromobenzofuran-D5;2-Bromo-1-benzofurane;2-Bromobenzo[b]furan 90%;2-Bromo-1-benzofuran, 90+%;2-Bromo-1-benzofuran:2-bromobenzofuran
- CBNumber
- CB2721954
- Molecular Formula
- C8H5BrO
- Formula Weight
- 197.03
- MOL File
- 54008-77-4.mol
2-BROMO-1-BENZOFURAN Property
- Melting point:
- 247-247.5 °C
- Boiling point:
- 234℃
- Density
- 1.608
- Flash point:
- 95℃
- storage temp.
- Sealed in dry,Store in freezer, under -20°C
- Appearance
- Colorless to light yellow Liquid
- InChI
- InChI=1S/C8H5BrO/c9-8-5-6-3-1-2-4-7(6)10-8/h1-5H
- InChIKey
- RNEOFIVNTNLSEH-UHFFFAOYSA-N
- SMILES
- O1C2=CC=CC=C2C=C1Br
Safety
- HS Code
- 2932990090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B678388
- Product name
- 2-Bromo-1-benzofuran
- Packaging
- 500mg
- Price
- $130
- Updated
- 2021/12/16
- Product number
- 2H10-9-12
- Product name
- 2-Bromobenzo[b]furan
- Purity
- 90%
- Packaging
- 1g
- Price
- $191
- Updated
- 2021/12/16
- Product number
- HCH0018529
- Product name
- 2-BROMO-1-BENZOFURAN
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $193.26
- Updated
- 2021/12/16
- Product number
- FB42238
- Product name
- 2-Bromobenzofuran
- Packaging
- 2g
- Price
- $240
- Updated
- 2021/12/16
- Product number
- FB42238
- Product name
- 2-Bromobenzofuran
- Packaging
- 250mg
- Price
- $60
- Updated
- 2021/12/16
2-BROMO-1-BENZOFURAN Chemical Properties,Usage,Production
Synthesis
91703-34-3
54008-77-4
2-(2,2-dibromovinyl)phenol (2.8 g, 10 mmol) was dissolved in tetrahydrofuran (30 mL) under nitrogen protection. Subsequently, cuprous iodide (I) (0.1 g, 0.5 mmol) and potassium phosphate (4.2 g, 20 mmol) were added. The reaction mixture was stirred at 80°C for 12 hours. After completion of the reaction, the mixture was poured into water (200 mL) and extracted with ethyl acetate (200 mL). The organic phases were combined, dried over anhydrous sodium sulfate and filtered. The filtrate was concentrated and purified by column chromatography (silica gel, eluent ethyl acetate/petroleum ether=1:20) to afford the target product 2-bromobenzofuran (1.8 g, 92% yield).
References
[1] Tetrahedron, 2011, vol. 67, # 33, p. 5913 - 5919
[2] Chemical Communications, 2011, vol. 47, # 37, p. 10476 - 10478
[3] Organic and Biomolecular Chemistry, 2013, vol. 11, # 24, p. 4095 - 4101
[4] Organic and Biomolecular Chemistry, 2012, vol. 10, # 21, p. 4172 - 4178
[5] Chemistry - A European Journal, 2015, vol. 21, # 4, p. 1482 - 1487
2-BROMO-1-BENZOFURAN Preparation Products And Raw materials
Raw materials
Preparation Products
2-BROMO-1-BENZOFURAN Suppliers
- Tel
- --
- Fax
- --
- contact@ambinter.com
- Country
- France
- ProdList
- 1648
- Advantage
- 60
View Lastest Price from 2-BROMO-1-BENZOFURAN manufacturers
- Product
- 2-BROMO-1-BENZOFURAN 54008-77-4
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1ton
- Release date
- 2022-09-27
- Product
- 2-BROMO-1-BENZOFURAN 54008-77-4
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99.0%
- Supply Ability
- 100kg
- Release date
- 2020-01-07