ChemicalBook > CAS DataBase List > 3-CHLOROPHENETHYLALCOHOL

3-CHLOROPHENETHYLALCOHOL

Product Name: 3-CHLOROPHENETHYLALCOHOL
CAS No.: 5182-44-5
Chemical Name: 3-CHLOROPHENETHYLALCOHOL
Synonyms: 3-chlorobenzeneethanol;3-CHLOROPHENETHYLALCOHOL;2-(3-Chlorophenyl)ethanol;M-CHLOROPHENETHYL ALCOHOL;Benzeneethanol, 3-chloro-;3-ChlorophenylEthylalcohol;m-chlorophenethylic alcohol;Phenethyl alcohol, m-chloro-;3-Chlorophenethylalcohol,98%;3-CHLOROPHENETHYLALCOHOL 98%
CBNumber: CB2745246
Molecular Formula: C8H9ClO
Formula Weight: 156.61
MOL File: 5182-44-5.mol

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3-CHLOROPHENETHYLALCOHOL Property

Boiling point:: 135-137 °C/13 mmHg (lit.)
Density: 1.181 g/mL at 25 °C (lit.)
refractive index: n20/D 1.549(lit.)
Flash point:: >230 °F
storage temp.: Sealed in dry,Room Temperature
form: Liquid
pka: 14.76±0.10(Predicted)
Specific Gravity: 1.157
color: Clear colorless to very slightly yellow
BRN: 2042059
InChI: InChI=1S/C8H9ClO/c9-8-3-1-2-7(6-8)4-5-10/h1-3,6,10H,4-5H2
InChIKey: NDWAVJKRSASRPH-UHFFFAOYSA-N
SMILES: C1(CCO)=CC=CC(Cl)=C1

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Safety

Safety Statements: 23-24/25
WGK Germany: 3
HS Code: 29052900

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 193518
Product name: 3-Chlorophenethyl alcohol
Purity: 98%
Packaging: 1g
Price: $55
Updated: 2023/06/20

TCI Chemical

Product number: C2907
Product name: 2-(3-Chlorophenyl)ethanol
Purity: >98.0%(GC)
Packaging: 5g
Price: $88
Updated: 2025/07/31

TCI Chemical

Product number: C2907
Product name: 2-(3-Chlorophenyl)ethanol
Purity: >98.0%(GC)
Packaging: 25g
Price: $295
Updated: 2025/07/31

TRC

Product number: C596685
Product name: 2-(3-Chlorophenyl)ethanol
Packaging: 100mg
Price: $45
Updated: 2021/12/16

Matrix Scientific

Product number: 075279
Product name: 3-Chlorophenethyl alcohol
Purity: 95+%
Packaging: 1g
Price: $40
Updated: 2021/12/16

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3-CHLOROPHENETHYLALCOHOL Chemical Properties,Usage,Production

Chemical Properties

clear colorless to very slightly yellow liquid

General Description

3-Chlorophenethyl alcohol undergoes coupling reaction with dibutylamine.

Synthesis

1878-65-5

5182-44-5

Example 86A Synthesis of 2-(3-chlorophenyl)ethanol: To a solution of 2-(3-chlorophenyl)acetic acid (11.4 g, 66.7 mmol) dissolved in 150 mL of THF was added LiAlH4 (3.04 g, 80.0 mmol) in batches at 0 °C. The reaction mixture was gradually warmed up to room temperature and stirred continuously under nitrogen protection for 2 hours. Upon completion of the reaction, the reaction was quenched by slow dropwise addition of 2N NaOH solution (30 mL), followed by extraction with ethyl acetate (2 x 150 mL). The organic phases were combined, dried with anhydrous Na2SO4, filtered and concentrated under reduced pressure to give the crude product. The crude product was purified by column chromatography (silica gel as stationary phase, petroleum ether/ethyl acetate = 50:1 to 10:1 gradient elution) to give 4.96 g of the target product, 3-chlorophenethyl alcohol, as a colorless oil. The yield was 55%.

References

[1] Bioorganic and Medicinal Chemistry Letters, 2007, vol. 17, # 3, p. 756 - 760
[2] Patent: US2013/131036, 2013, A1. Location in patent: Paragraph 1585; 1586
[3] Patent: WO2013/62966, 2013, A2. Location in patent: Paragraph 112; 113
[4] Helvetica Chimica Acta, 1973, vol. 56, p. 2460 - 2479
[5] Journal of the American Chemical Society, 1978, vol. 100, p. 228 - 246

3-CHLOROPHENETHYLALCOHOL Preparation Products And Raw materials

Raw materials

Preparation Products

2-(3-CHLORO-PHENYL)-ETHANESULFONYL CHLORIDE

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View Lastest Price from 3-CHLOROPHENETHYLALCOHOL manufacturers

Career Henan Chemical Co

Product: 3-CHLOROPHENETHYLALCOHOL 5182-44-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2019-12-25

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