2-IODOISOPROPYLBENZENE
- Product Name
- 2-IODOISOPROPYLBENZENE
- CAS No.
- 19099-54-8
- Chemical Name
- 2-IODOISOPROPYLBENZENE
- Synonyms
- Iodocumene;o-iodocumene;2-IODOCUMENE;2-Iodocumene>2-IODOISOPROPYLBENZENE;2-isopropyliodobenzene;2-Isopropylphenyl iodide;2-Iodo-1-isopropylbenzene;1-Isopropyl-2-iodobenzene;1-IODO-2-ISOPROPYLBENZENE
- CBNumber
- CB2746218
- Molecular Formula
- C9H11I
- Formula Weight
- 246.09
- MOL File
- 19099-54-8.mol
2-IODOISOPROPYLBENZENE Property
- Boiling point:
- 89 °C
- Density
- 1.54
- refractive index
- 1.5801
- Flash point:
- 110°C/20mm
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- solubility
- Chloroform (Slightly), Methanol (Slightly)
- form
- Oil
- color
- Clear Pale Red to Red
- Sensitive
- Light Sensitive
- BRN
- 2351872
- CAS DataBase Reference
- 19099-54-8(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi,N
- Risk Statements
- 36/37/38-50/53-41-37/38
- Safety Statements
- 26-36/37/39-61-60-39
- Hazard Note
- Irritant/Light Sensitive
- HS Code
- 29039990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- I0559
- Product name
- 2-Iodocumene
- Packaging
- 5G
- Price
- $39
- Updated
- 2025/07/31
- Product number
- I694525
- Product name
- 2-Iodocumene
- Packaging
- 1g
- Price
- $45
- Updated
- 2021/12/16
- Product number
- I694525
- Product name
- 2-Iodocumene
- Packaging
- 10g
- Price
- $110
- Updated
- 2021/12/16
- Product number
- 005746
- Product name
- 2-Iodoisopropylbenzene
- Purity
- 98%
- Packaging
- 25g
- Price
- $121
- Updated
- 2021/12/16
- Product number
- HCH0016467
- Product name
- 1-IODO-2-ISOPROPYLBENZENE
- Purity
- 95.00%
- Packaging
- 10G
- Price
- $134.4
- Updated
- 2021/12/16
2-IODOISOPROPYLBENZENE Chemical Properties,Usage,Production
Uses
2-Iodocumene acts as a reagent in the synthesis of aryliminoguanidines as NPFF1 and NPFF2 agonists.
Synthesis
643-28-7
19099-54-8
General procedure for the synthesis of 2-isopropyliodobenzene from 2-isopropylaniline: 2-isopropylaniline (27.04 g, 0.2 mol) was dissolved in 25% aqueous sulfuric acid solution (w/w, 160 mL), and diazotization reaction was carried out by slowly and dropwise addition of an aqueous solution of sodium nitrite (14 g) (26 mL) at -20 °C. The resulting diazonium salt solution was transferred to an aqueous solution (100 mL) of potassium iodide (100 g) and after 18 hours of reaction, sodium hydroxide (36 g) and water (125 mL) were added to neutralize the reaction system. The reaction mixture was extracted with hexane, the organic phases were combined and purified by silica gel column chromatography, and the target product, 2-isopropyliodobenzene, was obtained after concentration in a yield of 35.8 g, 73%. The product was identified by mass spectrometry: m/z 246 (M+). 1H NMR (CDCl3) δppm: 1.23 (d, 6H, J=6.84 Hz), 3.18 (septet, 1H, J=6.84 Hz), 6.86 (m, 1H), 7.28 (m, 2H), 7.82 (dd, 1H, J=1.24 and 7.92 Hz).
References
[1] Patent: US10113065, 2018, B1. Location in patent: Page/Page column 21
[2] Journal of the American Chemical Society, 1957, vol. 79, p. 1897,1900
[3] Bulletin of the Chemical Society of Japan, 1971, vol. 44, p. 266 - 270
[4] Journal of Organic Chemistry, 1997, vol. 62, # 16, p. 5651 - 5656
[5] Advanced Synthesis and Catalysis, 2008, vol. 350, # 14-15, p. 2179 - 2182
2-IODOISOPROPYLBENZENE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-IODOISOPROPYLBENZENE manufacturers
- Product
- 2-IODOISOPROPYLBENZENE 19099-54-8
- Price
- US $100.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-26
- Product
- 2-IODOISOPROPYLBENZENE 19099-54-8
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1kg;10kg;100kg
- Release date
- 2019-08-29