ChemicalBook > CAS DataBase List > 1-benzyl-4-piperidone oxime

1-benzyl-4-piperidone oxime

Product Name
1-benzyl-4-piperidone oxime
CAS No.
949-69-9
Chemical Name
1-benzyl-4-piperidone oxime
Synonyms
1-benzyl-4-piperidon;Cinitapride Impurity 5;Cinitapride Impurity 14;1-benzyl-4-piperidone oxime;1-Benzylpiperidine-4-oneoxime;1-Benzyl-piperidin-4-one oxime;N-benzyl-4-(N-hydroxyimino)piperidine;4-Piperidinone,1-(phenylMethyl)-, oxiMe;N-(1-Benzylpiperidin-4-ylidene)hydroxylamine;N-benzyl 4- (N-hydroxyimine) piperidine, oxime
CBNumber
CB2928072
Molecular Formula
C12H16N2O
Formula Weight
204.27
MOL File
949-69-9.mol
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1-benzyl-4-piperidone oxime Property

Melting point:
126-128 °C(Solv: chloroform (67-66-3); ligroine (8032-32-4))
Boiling point:
338.5±35.0 °C(Predicted)
Density 
1.12±0.1 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
12.14±0.20(Predicted)
Appearance
White to light yellow Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
L478938
Product name
1-BENZYL-4-PIPERIDINONE OXIME
Purity
AldrichCPR
Packaging
10MG
Price
$30.7
Updated
2025/07/31
TRC
Product number
B704078
Product name
1-benzyl-piperidin-4-oneoxime
Packaging
50mg
Price
$45
Updated
2021/12/16
AK Scientific
Product number
R147
Product name
1-Benzyl-piperidin-4-oneoxime
Packaging
10g
Price
$40
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB147939
Product name
1-Benzyl-piperidin-4-oneoxime
Packaging
100mg
Price
$55
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB147939
Product name
1-Benzyl-piperidin-4-oneoxime
Packaging
250mg
Price
$110
Updated
2021/12/16
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1-benzyl-4-piperidone oxime Chemical Properties,Usage,Production

Synthesis

3612-20-2

949-69-9

General procedure for the synthesis of (1-benzylpiperidin-4-) ketoxime from N-benzylpiperidone: N-benzylpiperidone (1.89 g, 10 mmol) was dissolved in 50 mL of anhydrous ethanol, potassium carbonate (2.76 g, 20 mmol) and hydroxylamine hydrochloride (1.04 g, 15 mmol) were added sequentially, and the reaction was stirred for 6 hours at room temperature. After completion of the reaction, the reaction mixture was concentrated and diluted by adding water. The aqueous phase was extracted with ethyl acetate, the organic phase was washed with saturated sodium chloride solution, dried over anhydrous sodium sulfate, and concentrated under reduced pressure to afford (1-benzylpiperidin-4-)ketoxime (2.04 g, 100% yield) as a white solid, and mass spectrometry analysis showed MS: 205.0 [M + H]+.

References

[1] Patent: US2017/44187, 2017, A1. Location in patent: Paragraph 0086; 0087
[2] European Journal of Medicinal Chemistry, 2010, vol. 45, # 7, p. 2827 - 2840
[3] Bioorganic and Medicinal Chemistry Letters, 2013, vol. 23, # 14, p. 4085 - 4090
[4] Tetrahedron, 1995, vol. 51, # 17, p. 5143 - 5156
[5] Journal of Medicinal Chemistry, 2013, vol. 56, # 22, p. 9089 - 9099

1-benzyl-4-piperidone oxime Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1-benzyl-4-piperidone oxime manufacturers

Henan Aochuang Chemical Co.,Ltd.
Product
1-benzyl-4-piperidone oxime 949-69-9
Price
US $0.00-0.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
1Ton
Release date
2022-09-16
Jinan Ande Pharmaceutical Co.,Ltd.
Product
1-benzyl-4-piperidone oxime 949-69-9
Price
US $0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
100
Release date
2021-12-23
Qiuxian Baitai New Material Co., LTD
Product
1-benzyl-4-piperidone oxime 949-69-9
Price
US $19.00/g
Min. Order
1KG
Purity
99%
Supply Ability
5ton/Month
Release date
2021-12-15

949-69-9, 1-benzyl-4-piperidone oxime Related Search:

Benzoic acid, 4-aMino-2-ethoxy-, Methyl ester Benzamide, 4-amino-N-[1-(3-cyclohexen-1-ylmethyl)-4-piperidinyl]-2-methoxy-5-nitro- 4-(4-amino-2-ethoxy-5-nitrobenzamido)-1-(cyclohex-3-en-1-ylmethyl)piperidine 1-oxide Benzoic acid, 4-amino-2-ethoxy- 4-(AcetylaMino)-2-ethoxy-5-nitrobenzoic Acid Methyl Ester Benzoic acid, 4-(acetylamino)-2-ethoxy- 4-AMino-2-ethoxy-5-nitrobenzoic Acid Methyl Ester Benzoic acid, 2-ethoxy-4-hydroxy-, methyl ester Benzamide, 4-amino-2-ethoxy-5-nitro-N-4-piperidinyl- 4-AMINO-2-ETHOXY-5-NITROBENZOIC ACID 1-benzyl-4-piperidone oxime 8-BENZYL-1AH,5AH-NORTROPAN-3-ONE OXIME 1-(4-CHLOROBENZYL)PIPERIDIN-4-ONE OXIME 1-(2-hydroxy-4-methylbenzoyl)piperidin-4-one oxime 1-(5-bromo-2-fluorobenzyl)piperidin-4-one oxime 1-(3,5-difluorobenzoyl)piperidin-4-one oxime 1-(2-chlorobenzoyl)piperidin-4-one oxime 1-(2,6-difluorobenzoyl)piperidin-4-one oxime

  • 1-benzyl-4-piperidone oxime
  • 1-Benzyl-piperidin-4-one oxime
  • 1-Benzylpiperidine-4-oneoxime
  • N-[1-(phenylmethyl)piperidin-4-ylidene]hydroxylamine
  • 1-benzyl-4-piperidon
  • 4-Piperidinone,1-(phenylMethyl)-, oxiMe
  • N-benzyl-4-(N-hydroxyimino)piperidine
  • N-(1-Benzylpiperidin-4-ylidene)hydroxylamine
  • Pharmaceutical Intermediates 1-Benzylpiperidin-4-One Oxime
  • Cinitapride Impurity 14
  • N-benzyl 4- (N-hydroxyimine) piperidine, oxime
  • Cinitapride Impurity 5
  • 949-69-9
  • Piperidine