Ethyl 3-bromo-5-nitrobenzoate
- Product Name
- Ethyl 3-bromo-5-nitrobenzoate
- CAS No.
- 690260-94-7
- Chemical Name
- Ethyl 3-bromo-5-nitrobenzoate
- Synonyms
- Ethyl 3-bromo-5-nitrobenzoate;Ethyl3-bromo-5-nitrobenzoate98%;Ethyl 3-bromo-5-nitrobenzoate 98%;Benzoic acid, 3-bromo-5-nitro-, ethyl ester;Ethyl 3-bromo-5-nitrobenzoate ISO 9001：2015 REACH
- CBNumber
- CB2958233
- Molecular Formula
- C9H8BrNO4
- Formula Weight
- 274.07
- MOL File
- 690260-94-7.mol
Ethyl 3-bromo-5-nitrobenzoate Property
- storage temp.
- Sealed in dry,Room Temperature
- form
- solid
- color
- Yellow
Safety
- Hazard Codes
- Xi
- Hazard Note
- Irritant
- HS Code
- 2916399090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- E900800
- Product name
- Ethyl3-bromo-5-nitrobenzoate
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 449080
- Product name
- Ethyl 3-bromo-5-nitrobenzoate
- Packaging
- 100mg
- Price
- $305
- Updated
- 2021/12/16
- Product number
- OR3749
- Product name
- Ethyl3-bromo-5-nitrobenzoate
- Purity
- 98%
- Packaging
- 1g
- Price
- $37
- Updated
- 2021/12/16
- Product number
- 4654-9-Z0
- Product name
- Ethyl 3-bromo-5-nitrobenzoate
- Purity
- 98%
- Packaging
- 1g
- Price
- $40
- Updated
- 2021/12/16
- Product number
- 076086
- Product name
- Ethyl 3-bromo-5-nitrobenzoate
- Purity
- 95+%
- Packaging
- 1g
- Price
- $116
- Updated
- 2021/12/16
Ethyl 3-bromo-5-nitrobenzoate Chemical Properties,Usage,Production
Synthesis
64-17-5
6307-83-1
690260-94-7
Add 3-bromo-5-nitrobenzoic acid (25 g, 101.6 mmol) and anhydrous ethanol (200 mL) to a 500 mL round bottom flask. With stirring at 0 °C, sulfoxide chloride (15 mL) was added slowly and dropwise. The reaction mixture was warmed to 80 °C with continuous stirring for 4 hours. Upon completion of the reaction, the reaction was quenched by the addition of 50 mL of water. The reaction mixture was extracted with dichloromethane (3 x 50 mL), the organic layers were combined and concentrated under reduced pressure. The concentrated residue was purified by silica gel column chromatography with ethyl acetate/petroleum ether as eluent (gradient elution, 1:20 to 1:10). Ethyl 3-bromo-5-nitrobenzoate 27.5 g (99% yield) was obtained as a white solid.
References
[1] Patent: WO2017/184623, 2017, A1. Location in patent: Page/Page column 127
[2] Bioorganic and Medicinal Chemistry Letters, 2011, vol. 21, # 13, p. 3992 - 3996
Ethyl 3-bromo-5-nitrobenzoate Preparation Products And Raw materials
Raw materials
Preparation Products
Ethyl 3-bromo-5-nitrobenzoate Suppliers
- Tel
- --
- Fax
- --
- sales@apolloscientific.co.uk
- Country
- United Kingdom
- ProdList
- 6084
- Advantage
- 88
View Lastest Price from Ethyl 3-bromo-5-nitrobenzoate manufacturers
- Product
- Ethyl 3-bromo-5-nitrobenzoate 690260-94-7
- Price
- US $101.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-28