1-ADAMANTANECARBOXAMIDE

Product Name: 1-ADAMANTANECARBOXAMIDE
CAS No.: 5511-18-2
Chemical Name: 1-ADAMANTANECARBOXAMIDE
Synonyms: OTAVA-BB BB5030040657;SALOR-INT L496057-1EA;LABOTEST-BB LT00007835;1-Adamantyl-carboxamide;1-ADAMANTANECARBOXAMIDE; Adamantane Impurity 14;ADAMANTANE-1-CARBOXAMIDE;1-Adamantanecarboxamide,98%;1-Adamantanecarboxamide >8-Quinolinol sulfate hydrate
CBNumber: CB3100671
Molecular Formula: C11H17NO
Formula Weight: 179.26
MOL File: 5511-18-2.mol

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1-ADAMANTANECARBOXAMIDE Property

Melting point:: 188-190 °C(lit.)
Boiling point:: 311.8°C (rough estimate)
Density: 1.0020 (rough estimate)
refractive index: 1.5065 (estimate)
storage temp.: Sealed in dry,Room Temperature
solubility: Chloroform, Dichloromethane, Methanol
form: Solid
pka: 16.85±0.20(Predicted)
color: White
BRN: 2047887
CAS DataBase Reference: 5511-18-2(CAS DataBase Reference)

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Safety

Safety Statements: 24/25
WGK Germany: 3
RTECS: AU4452000
HazardClass: IRRITANT
HS Code: 29242990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 390607
Product name: 1-Adamantanecarboxamide
Purity: 97%
Packaging: 1g
Price: $106
Updated: 2023/01/07

TCI Chemical

Product number: A2078
Product name: 1-Adamantanecarboxamide
Purity: >97.0%(GC)
Packaging: 1g
Price: $28
Updated: 2024/03/01

TCI Chemical

Product number: A2078
Product name: 1-Adamantanecarboxamide
Purity: >97.0%(GC)
Packaging: 5g
Price: $133
Updated: 2022/04/27

TRC

Product number: A207900
Product name: 1-Adamantanecarboxamide
Packaging: 1g
Price: $155
Updated: 2021/12/16

TRC

Product number: A207900
Product name: 1-Adamantanecarboxamide
Packaging: 10g
Price: $1230
Updated: 2021/12/16

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1-ADAMANTANECARBOXAMIDE Chemical Properties,Usage,Production

Chemical Properties

White Solid

Uses

Reproduction of Sindbis virus strains sensitive and resistant to 1-adamantanecarboxamide

Synthesis

2094-72-6

5511-18-2

GENERAL STEPS: To a stirred mixture of 1-adamantanecarboxylic acid (11, 36.05 g, 200 mmol) and DMF (5 drops) in CH2Cl2 (360 mL) was added thionyl chloride (26.17 g, 220 mmol) in batches under cooling conditions in an ice-water bath. The resulting mixture was refluxed until the release of HCl gas ceased (usually takes 2 hours). Subsequently, the solvent and excess thionyl chloride were removed using a rotary evaporator and the crude product, adamantanoyl chloride (12), was dissolved in THF (100 mL). This solution was slowly added dropwise to concentrated ammonia (400 mL) cooled and stirred in an ice water bath. After the dropwise addition was completed, the white slurry formed was continued to be stirred at room temperature for 2 hours. The white precipitate was collected by vacuum filtration, washed with cold hexane, and dried under vacuum to give 1-adamantanecarboxamide (13). The product was a white solid with a yield of 34.06 g (95% yield) and a melting point of 177-179 °C (literature value: 185.5-191.7 °C [48]).1H-NMR (DMSO-d6, 400 MHz) δ: 6.89 (brs, 1H), 6.62 (brs, 1H), 1.93 (s, 3H), 1.73-1.74 (m , 6H), 1.60-1.68 (m, 6H).

References

[1] Molecules, 2018, vol. 23, # 2,
[2] Chemistry - A European Journal, 2016, vol. 22, # 15, p. 5156 - 5159
[3] Synthetic Communications, 1988, vol. 18, # 11, p. 1179 - 1186
[4] Journal of Organic Chemistry, 1981, vol. 46, # 20, p. 3988 - 3991
[5] Chemische Berichte, 1960, vol. 93, p. 226 - 230

1-ADAMANTANECARBOXAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-ADAMANTANECARBOXAMIDE Suppliers

Americas 1 Belgium 3 Canada 2 China 94 Europe 1 France 1 Germany 7 India 6 Japan 5 Latvia 1 Russia 1 Slovakia 2 South Korea 1 Switzerland 2 The Netherlands 2 Ukraine 2 United Kingdom 12 United States 35 Global 178

J & K SCIENTIFIC LTD.

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INTATRADE GmbH

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Shanghai Hanhong Scientific Co.,Ltd.

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Chemsky（shanghai）International Co.,Ltd.

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View Lastest Price from 1-ADAMANTANECARBOXAMIDE manufacturers

Career Henan Chemical Co

Product: 1-ADAMANTANECARBOXAMIDE 5511-18-2
Price: US $1.00/kg
Min. Order: 1g
Purity: 99%
Supply Ability: 100KG
Release date: 2018-12-21

5511-18-2, 1-ADAMANTANECARBOXAMIDERelated Search:

1-ADAMANTANECARBOXAMIDE ADAMANTANE-1-CARBOHYDRAZIDE Adamantane (1-ADAMANTANECARBONYL-D-ARG0,HYP3,BETA-(2-THIENYL)-ALA5,8,D-PHE7)-BRADYKININ N-Antipyrinyl-1-adamantanecarboxamide AURORA 401 N-(5-nitro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-1-adamantanecarboxamide N-[4-(1-pyrrolidinylsulfonyl)phenyl]-3-(1H-1,2,4-triazol-1-yl)-1-adamantanecarboxamide N-(5-bromo-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-1-adamantanecarboxamide TOSLAB 865133 4-[(1-ADAMANTYLCARBONYL)AMINO]BENZOIC ACID TIMTEC-BB SBB007551 AURORA 402 2-[(ADAMANTANE-1-CARBONYL)-AMINO]-3-(1H-INDOL-3-YL)-PROPIONIC ACID N-(2-HYDROXYETHYL)-1-ADAMANTANECARBOXAMIDE N-HYDROXYADAMANTANE-1-CARBOXAMIDE TIMTEC-BB SBB006373 TIMTEC-BB SBB001230

2-Carbamoyladamantane, Tricyclo[3.3.1.1~3,7~]decane-1-carboxamide

Tricyclo(3.3.1.1(sup 3,7))decane-1-carboxamide (9CI)

SALOR-INT L496057-1EA

OTAVA-BB BB5030040657

1-Adamantyl-carboxamide

tricyclo(3.3.1.1(sup3,7))decane-1-carboxamide

Tricyclo(3.3.1.1<sup>3,7</sup>)decane-1-carboxamide

LABOTEST-BB LT00007835

1-ADAMANTANECARBOXAMIDE

Tricyclo[3.3.1.13,7]decane-1-carboxamide

ADAMANTANE-1-CARBOXAMIDE

1-Adamantanecarboxamide,98%

ADAMANTANE-1-CARBOXYLIC ACID AMIDE

Adamantane-1-carboxamide, 97+%

1-Adamantanecarboxamide &gt

Adamantane Impurity 14

8-Quinolinol sulfate hydrate

5511-18-2

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