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1-ADAMANTANECARBOXAMIDE

Product Name
1-ADAMANTANECARBOXAMIDE
CAS No.
5511-18-2
Chemical Name
1-ADAMANTANECARBOXAMIDE
Synonyms
OTAVA-BB BB5030040657;SALOR-INT L496057-1EA;LABOTEST-BB LT00007835;1-Adamantyl-carboxamide;1-ADAMANTANECARBOXAMIDE; Adamantane Impurity 14;ADAMANTANE-1-CARBOXAMIDE;1-Adamantanecarboxamide,98%;1-Adamantanecarboxamide >8-Quinolinol sulfate hydrate
CBNumber
CB3100671
Molecular Formula
C11H17NO
Formula Weight
179.26
MOL File
5511-18-2.mol
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1-ADAMANTANECARBOXAMIDE Property

Melting point:
188-190 °C(lit.)
Boiling point:
311.8°C (rough estimate)
Density 
1.0020 (rough estimate)
refractive index 
1.5065 (estimate)
storage temp. 
Sealed in dry,Room Temperature
solubility 
Chloroform, Dichloromethane, Methanol
form 
Solid
pka
16.85±0.20(Predicted)
color 
White
BRN 
2047887
CAS DataBase Reference
5511-18-2(CAS DataBase Reference)
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Safety

Safety Statements 
24/25
WGK Germany 
3
RTECS 
AU4452000
HazardClass 
IRRITANT
HS Code 
29242990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
390607
Product name
1-Adamantanecarboxamide
Purity
97%
Packaging
1g
Price
$106
Updated
2023/01/07
TCI Chemical
Product number
A2078
Product name
1-Adamantanecarboxamide
Purity
>97.0%(GC)
Packaging
1g
Price
$28
Updated
2024/03/01
TCI Chemical
Product number
A2078
Product name
1-Adamantanecarboxamide
Purity
>97.0%(GC)
Packaging
5g
Price
$133
Updated
2022/04/27
TRC
Product number
A207900
Product name
1-Adamantanecarboxamide
Packaging
1g
Price
$155
Updated
2021/12/16
TRC
Product number
A207900
Product name
1-Adamantanecarboxamide
Packaging
10g
Price
$1230
Updated
2021/12/16
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1-ADAMANTANECARBOXAMIDE Chemical Properties,Usage,Production

Chemical Properties

White Solid

Uses

Reproduction of Sindbis virus strains sensitive and resistant to 1-adamantanecarboxamide

Synthesis

2094-72-6

5511-18-2

GENERAL STEPS: To a stirred mixture of 1-adamantanecarboxylic acid (11, 36.05 g, 200 mmol) and DMF (5 drops) in CH2Cl2 (360 mL) was added thionyl chloride (26.17 g, 220 mmol) in batches under cooling conditions in an ice-water bath. The resulting mixture was refluxed until the release of HCl gas ceased (usually takes 2 hours). Subsequently, the solvent and excess thionyl chloride were removed using a rotary evaporator and the crude product, adamantanoyl chloride (12), was dissolved in THF (100 mL). This solution was slowly added dropwise to concentrated ammonia (400 mL) cooled and stirred in an ice water bath. After the dropwise addition was completed, the white slurry formed was continued to be stirred at room temperature for 2 hours. The white precipitate was collected by vacuum filtration, washed with cold hexane, and dried under vacuum to give 1-adamantanecarboxamide (13). The product was a white solid with a yield of 34.06 g (95% yield) and a melting point of 177-179 °C (literature value: 185.5-191.7 °C [48]).1H-NMR (DMSO-d6, 400 MHz) δ: 6.89 (brs, 1H), 6.62 (brs, 1H), 1.93 (s, 3H), 1.73-1.74 (m , 6H), 1.60-1.68 (m, 6H).

References

[1] Molecules, 2018, vol. 23, # 2,
[2] Chemistry - A European Journal, 2016, vol. 22, # 15, p. 5156 - 5159
[3] Synthetic Communications, 1988, vol. 18, # 11, p. 1179 - 1186
[4] Journal of Organic Chemistry, 1981, vol. 46, # 20, p. 3988 - 3991
[5] Chemische Berichte, 1960, vol. 93, p. 226 - 230

1-ADAMANTANECARBOXAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-ADAMANTANECARBOXAMIDE Suppliers

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View Lastest Price from 1-ADAMANTANECARBOXAMIDE manufacturers

Career Henan Chemical Co
Product
1-ADAMANTANECARBOXAMIDE 5511-18-2
Price
US $1.00/kg
Min. Order
1g
Purity
99%
Supply Ability
100KG
Release date
2018-12-21

5511-18-2, 1-ADAMANTANECARBOXAMIDERelated Search:

1-ADAMANTANECARBOXAMIDE ADAMANTANE-1-CARBOHYDRAZIDE Adamantane (1-ADAMANTANECARBONYL-D-ARG0,HYP3,BETA-(2-THIENYL)-ALA5,8,D-PHE7)-BRADYKININ N-Antipyrinyl-1-adamantanecarboxamide AURORA 401 N-(5-nitro-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-1-adamantanecarboxamide N-[4-(1-pyrrolidinylsulfonyl)phenyl]-3-(1H-1,2,4-triazol-1-yl)-1-adamantanecarboxamide N-(5-bromo-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-1-adamantanecarboxamide TOSLAB 865133 4-[(1-ADAMANTYLCARBONYL)AMINO]BENZOIC ACID TIMTEC-BB SBB007551 AURORA 402 2-[(ADAMANTANE-1-CARBONYL)-AMINO]-3-(1H-INDOL-3-YL)-PROPIONIC ACID N-(2-HYDROXYETHYL)-1-ADAMANTANECARBOXAMIDE N-HYDROXYADAMANTANE-1-CARBOXAMIDE TIMTEC-BB SBB006373 TIMTEC-BB SBB001230

  • 2-Carbamoyladamantane, Tricyclo[3.3.1.1~3,7~]decane-1-carboxamide
  • Tricyclo(3.3.1.1(sup 3,7))decane-1-carboxamide (9CI)
  • SALOR-INT L496057-1EA
  • OTAVA-BB BB5030040657
  • 1-Adamantyl-carboxamide
  • tricyclo(3.3.1.1(sup3,7))decane-1-carboxamide
  • Tricyclo(3.3.1.1<sup>3,7</sup>)decane-1-carboxamide
  • LABOTEST-BB LT00007835
  • 1-ADAMANTANECARBOXAMIDE
  • Tricyclo[3.3.1.13,7]decane-1-carboxamide
  • ADAMANTANE-1-CARBOXAMIDE
  • 1-Adamantanecarboxamide,98%
  • ADAMANTANE-1-CARBOXYLIC ACID AMIDE
  • Adamantane-1-carboxamide, 97+%
  • 1-Adamantanecarboxamide &gt
  • Adamantane Impurity 14
  • 8-Quinolinol sulfate hydrate
  • 5511-18-2
  • Building Blocks
  • Amides
  • Carbonyl Compounds
  • Organic Building Blocks
  • Building Blocks
  • Carbonyl Compounds
  • Chemical Synthesis
  • Organic Building Blocks
  • Intermediates & Fine Chemicals
  • Pharmaceuticals
  • Amides
  • Carbonyl Compounds
  • Organic Building Blocks
  • Adamantane derivatives
  • Adamantanes