ChemicalBook > CAS DataBase List > 6-Nitro-1,2,3,4-tetrahydroquinoline

6-Nitro-1,2,3,4-tetrahydroquinoline

Product Name: 6-Nitro-1,2,3,4-tetrahydroquinoline
CAS No.: 14026-45-0
Chemical Name: 6-Nitro-1,2,3,4-tetrahydroquinoline
Synonyms: Quinoline, 1,2,3,4-tetrahydro-6-nitro-
CBNumber: CB31117320
Molecular Formula: C9H10N2O2
Formula Weight: 178.19
MOL File: 14026-45-0.mol

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6-Nitro-1,2,3,4-tetrahydroquinoline Property

Melting point:: 161-162 °C(Solv: acetic acid, 50% (64-19-7))
Boiling point:: 341.4±31.0 °C(Predicted)
Density: 1.236±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
pka: 0.87±0.20(Predicted)
Appearance: Yellow to brown Solid
InChI: InChI=1S/C9H10N2O2/c12-11(13)8-3-4-9-7(6-8)2-1-5-10-9/h3-4,6,10H,1-2,5H2
InChIKey: ASVYHMUYLBMSKW-UHFFFAOYSA-N
SMILES: N1C2=C(C=C([N+]([O-])=O)C=C2)CCC1

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Safety

HS Code: 2933499090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: N497665
Product name: 6-nitro-1,2,3,4-tetrahydroquinoline
Packaging: 100mg
Price: $65
Updated: 2021/12/16

TRC

Product number: N497665
Product name: 6-nitro-1,2,3,4-tetrahydroquinoline
Packaging: 500mg
Price: $240
Updated: 2021/12/16

Apolloscientific

Product number: OR951068
Product name: 6-Nitro-1,2,3,4-tetrahydroquinoline
Purity: 96%
Packaging: 250mg
Price: $115
Updated: 2021/12/16

ChemScene

Product number: CS-0043686
Product name: 6-Nitro-1,2,3,4-tetrahydroquinoline
Purity: 98.61%
Packaging: 1g
Price: $117
Updated: 2021/12/16

AK Scientific

Product number: V3050
Product name: 6-Nitro-1,2,3,4-tetrahydroquinoline
Packaging: 250mg
Price: $124
Updated: 2021/12/16

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6-Nitro-1,2,3,4-tetrahydroquinoline Chemical Properties,Usage,Production

Synthesis

613-50-3

14026-45-0

General procedure for the synthesis of 6-nitro-1,2,3,4-tetrahydroquinoline from 6-nitroquinoline: in a 10 mL Schlenk tube, Fe(OTf)2 (0.005 mmol, 1.8 mg), 6-nitroquinoline (0.5 mmol, 72 mg), Hantzsch ester A (1.25 mmol, 318 mg) and 1.0 mL of CHCl3. The reaction mixture was stirred at 40 °C for 2 hours. After completion of the reaction, the reaction solution was concentrated under reduced pressure to remove the solvent. The crude product was purified by silica gel column chromatography to afford the target product 6-nitro-1,2,3,4-tetrahydroquinoline (63.8 mg, 96% yield).

References

[1] Tetrahedron Letters, 2004, vol. 45, # 16, p. 3215 - 3217
[2] ChemCatChem, 2017, vol. 9, # 13, p. 2496 - 2505
[3] Tetrahedron Letters, 2017, vol. 58, # 36, p. 3571 - 3573
[4] Chemical Communications, 2018, vol. 54, # 62, p. 8622 - 8625
[5] Chemical Science, 2017, vol. 8, # 12, p. 8164 - 8169

6-Nitro-1,2,3,4-tetrahydroquinoline Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 6-Nitro-1,2,3,4-tetrahydroquinoline manufacturers

Career Henan Chemical Co

Product: 6-Nitro-1,2,3,4-tetrahydroquinoline 14026-45-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2020-01-09

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Quinoline, 1,2,3,4-tetrahydro-6-nitro-

14026-45-0