NSC54180
- Product Name
- NSC54180
- CAS No.
- 6623-35-4
- Chemical Name
- NSC54180
- Synonyms
- NSC54180;5-BroMo-2-hydroxy-4-Methyl-benzoic acid;Benzoic acid, 5-bromo-2-hydroxy-4-methyl-
- CBNumber
- CB31250933
- Molecular Formula
- C8H7BrO3
- Formula Weight
- 231.04
- MOL File
- 6623-35-4.mol
NSC54180 Property
- Melting point:
- 205-208 °C
- Boiling point:
- 359.2±42.0 °C(Predicted)
- Density
- 1.739±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 2.68±0.10(Predicted)
- Appearance
- White to off-white Solid
Safety
- HS Code
- 2916399090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B700745
- Product name
- 5-Bromo-2-hydroxy-4-methylbenzoicAcid
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- HCH0361356
- Product name
- 5-BROMO-2-HYDROXY-4-METHYLBENZOIC ACID
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $499.35
- Updated
- 2021/12/16
- Product number
- CD12045440
- Product name
- 5-Bromo-2-hydroxy-4-methylbenzoicacid
- Purity
- 97%
- Packaging
- 5g
- Price
- $1066
- Updated
- 2021/12/16
- Product number
- CD12045440
- Product name
- 5-Bromo-2-hydroxy-4-methylbenzoicacid
- Purity
- 97%
- Packaging
- 10g
- Price
- $1914
- Updated
- 2021/12/16
- Product number
- A414305
- Product name
- 5-Bromo-2-hydroxy-4-methylbenzoicacid
- Purity
- 97%
- Packaging
- 100mg
- Price
- $18
- Updated
- 2021/12/16
NSC54180 Chemical Properties,Usage,Production
Synthesis
50-85-1
6623-35-4
A) Synthesis of 5-bromo-2-hydroxy-4-methylbenzoic acid: 2-hydroxy-4-methylbenzoic acid (5.00 g) was dissolved in acetic acid (70.0 mL) and bromine (1.68 mL) was added slowly and dropwise. The reaction mixture was stirred at room temperature for 5.5 hours. Upon completion of the reaction, water was added to the mixture and the precipitate was collected by filtration. The precipitate was dried under reduced pressure to give the target compound 5-bromo-2-hydroxy-4-methylbenzoic acid (6.78 g). The result of mass spectrometry analysis: [M-H]? 229.0.
References
[1] Patent: WO2018/24224, 2018, A1. Location in patent: Page/Page column 80; 81
[2] Patent: US2018/127370, 2018, A1. Location in patent: Paragraph 0892
[3] Journal of the Chemical Society, 1914, vol. 105, p. 1891
[4] Journal fuer Praktische Chemie (Leipzig), 1915, vol. <2> 91, p. 388
[5] Patent: EP1391451, 2004, A1. Location in patent: Page 84
NSC54180 Preparation Products And Raw materials
Raw materials
Preparation Products
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