ChemicalBook > CAS DataBase List > 5-BROMO-4-METHYL-PYRIDINE-2,3-DIAMINE

5-BROMO-4-METHYL-PYRIDINE-2,3-DIAMINE

Product Name
5-BROMO-4-METHYL-PYRIDINE-2,3-DIAMINE
CAS No.
41230-93-7
Chemical Name
5-BROMO-4-METHYL-PYRIDINE-2,3-DIAMINE
Synonyms
5-broMo-4-Methylpyridine-2;5-Bromo-2,3-Diamino-4-Picoline;2,3-diamino-5-bromo-4-methylpyridine;5-bromo-4-methyl-2,3-Pyridinediamine;5-Bromo-2,3-diamino-4-methylpyridine;2,3-Diamine-4-methyl-5-bromopyridine;5-BROMO-4-METHYL-PYRIDINE-2,3-DIAMINE;2,3-Pyridinediamine, 5-bromo-4-methyl-;5-Bromo-2,3-diamino-4-methylpyridine 97%;5-BROMO-4-METHYL-PYRIDINE-2,3-DIAMINE ISO 9001：2015 REACH
CBNumber
CB3129140
Molecular Formula
C6H8BrN3
Formula Weight
202.05
MOL File
41230-93-7.mol
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5-BROMO-4-METHYL-PYRIDINE-2,3-DIAMINE Property

Melting point:
161-162℃
Boiling point:
331.2±37.0 °C(Predicted)
Density 
1.688±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
5.16±0.50(Predicted)
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B405208
Product name
5-Bromo-4-methylpyridine-2,3-diamine
Packaging
10mg
Price
$45
Updated
2021/12/16
TRC
Product number
B405208
Product name
5-Bromo-4-methylpyridine-2,3-diamine
Packaging
50mg
Price
$60
Updated
2021/12/16
Frontier Specialty Chemicals
Product number
CAPOB13672
Product name
5-Bromo-4-methylpyridine-2,3-diamine
Packaging
1g
Price
$75
Updated
2021/12/16
AK Scientific
Product number
W6169
Product name
5-Bromo-4-methylpyridine-2,3-diamine
Packaging
5g
Price
$232
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0037045
Product name
5-BROMO-4-METHYLPYRIDINE-2,3-DIAMINE
Purity
95.00%
Packaging
250MG
Price
$233.1
Updated
2021/12/16
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5-BROMO-4-METHYL-PYRIDINE-2,3-DIAMINE Chemical Properties,Usage,Production

Synthesis

100367-40-6

41230-93-7

5-Bromo-4-methyl-3-nitropyridin-2-amine (700.0 mg, 3.02 mmol) was added with iron powder (1680.0 mg, 30.20 mmol) and concentrated hydrochloric acid (50.0 μL) in a solvent mixture of ethanol (2.8 mL) and water (0.7 mL). The reaction suspension was stirred at 100 °C for 30 min. Upon completion of the reaction, the mixture was cooled to room temperature and filtered through diatomaceous earth to remove insoluble impurities. The filtrate was concentrated by distillation under reduced pressure and the resulting residue was purified by silica gel column chromatography (eluent: methanol/dichloromethane = 1:40). The grades containing the target product were collected and the solvent was removed by evaporation to give 5-bromo-4-methylpyridine-2,3-diamine as a brown solid (550.0 mg, 90% yield). The product was analyzed by LCMS ESI (+): m/z 202 ([M + H]+), 204 ([M + H + 2]+). 1H-NMR (300 MHz, DMSO-d6) data: δ 7.37 (s, 1H), 5.49 (s, 2H), 4.74 (s, 2H), 2.12 (s, 3H).

References

[1] Patent: US2014/315888, 2014, A1. Location in patent: Paragraph 0842-0844
[2] Journal of Medicinal Chemistry, 2018, vol. 61, # 7, p. 2949 - 2961
[3] Journal of Medicinal Chemistry, 2010, vol. 53, # 22, p. 7958 - 7966
[4] Journal of the American Chemical Society, 1957, vol. 79, p. 6421,6423,6424
[5] Bioorganic and Medicinal Chemistry Letters, 1996, vol. 6, # 22, p. 2749 - 2754

5-BROMO-4-METHYL-PYRIDINE-2,3-DIAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-BROMO-4-METHYL-PYRIDINE-2,3-DIAMINE manufacturers

Dideu Industries Group Limited
Product
5-BROMO-4-METHYL-PYRIDINE-2,3-DIAMINE 41230-93-7
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-08-27
Career Henan Chemical Co
Product
5-BROMO-4-METHYL-PYRIDINE-2,3-DIAMINE 41230-93-7
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
1ton
Release date
2019-07-11

41230-93-7, 5-BROMO-4-METHYL-PYRIDINE-2,3-DIAMINERelated Search:

Picoxystrobin 2,3-Diamino-5-methylpyridine 2,3-diaMino-5-chloropyrazine 2-amino-5-iodo-3-pyridinylamine 6-FLUORO-3,4-PYRIDINEDIAMINE 2,3-Diamino-5-trifluoromethylpyridine 4-METHYL-PYRIDINE-2,3-DIAMINE

  • 5-bromo-4-methyl-2,3-Pyridinediamine
  • 2,3-diamino-5-bromo-4-methylpyridine
  • 5-BROMO-4-METHYL-PYRIDINE-2,3-DIAMINE
  • 5-Bromo-2,3-diamino-4-methylpyridine 97%
  • 5-Bromo-2,3-diamino-4-methylpyridine
  • 5-broMo-4-Methylpyridine-2
  • 2,3-Diamine-4-methyl-5-bromopyridine
  • 2,3-Pyridinediamine, 5-bromo-4-methyl-
  • 5-BROMO-4-METHYL-PYRIDINE-2,3-DIAMINE ISO 9001：2015 REACH
  • 5-Bromo-2,3-Diamino-4-Picoline
  • 41230-93-7
  • Heterocycle-Pyridine series