ChemicalBook > CAS DataBase List > 2-AMINO-(4'-NITRO)ACETOPHENONE HYDROCHLORIDE

2-AMINO-(4'-NITRO)ACETOPHENONE HYDROCHLORIDE

Product Name: 2-AMINO-(4'-NITRO)ACETOPHENONE HYDROCHLORIDE
CAS No.: 5425-81-0
Chemical Name: 2-AMINO-(4'-NITRO)ACETOPHENONE HYDROCHLORIDE
Synonyms: AURORA 23208;OTAVA-BB BB7110952478;2-AMino-4'-nitroacetophenone HCl;2-AMino-p-nitro-acetophenone HCl;2-AMINO-P-NITRO-ACETOPHENONE HYDROCHLORIDE;2-AMINO-(4'-NITRO)ACETOPHENONE HYDROCHLORIDE;2-AMINO-1-(4-NITRO-PHENYL)-ETHANONE HYDROCHLORIDE;2-Amino-1-(4-nitrophenyl)ethanone hydrochloride (1:1);Ethanone, 2-amino-1-(4-nitrophenyl)-, hydrochloride (1:1);2-Amino-(4′-nitro)acetophenone hydrochloride, CAS 5425-81-0
CBNumber: CB3146488
Molecular Formula: C8H9ClN2O3
Formula Weight: 216.62
MOL File: 5425-81-0.mol

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2-AMINO-(4'-NITRO)ACETOPHENONE HYDROCHLORIDE Property

Melting point:: >211°C (dec)
storage temp.: Sealed in dry,Room Temperature
solubility: DMSO (Slightly), Methanol (Slightly)
form: Solid
color: White to Off-White
CAS DataBase Reference: 5425-81-0(CAS DataBase Reference)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Warning

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: PH011994
Product name: 2-amino-1-(4-nitrophenyl)ethanone hydrochloride
Purity: AldrichCPR
Packaging: 100mg
Price: $134
Updated: 2023/06/20

TRC

Product number: A578998
Product name: 2-amino-1-(4-nitrophenyl)ethanone hydrochloride
Packaging: 500mg
Price: $245
Updated: 2021/12/16

TRC

Product number: A578998
Product name: 2-amino-1-(4-nitrophenyl)ethanone hydrochloride
Packaging: 50mg
Price: $50
Updated: 2021/12/16

TRC

Product number: A578998
Product name: 2-amino-1-(4-nitrophenyl)ethanone hydrochloride
Packaging: 100mg
Price: $75
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4654-5-59
Product name: 4-Nitrophenacylamine hydrochloride hydrate
Packaging: 250mg
Price: $84
Updated: 2021/12/16

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2-AMINO-(4'-NITRO)ACETOPHENONE HYDROCHLORIDE Chemical Properties,Usage,Production

Synthesis

99-81-0

5425-81-0

Example 2: Synthesis of 2-amino-1-(4-nitrophenyl)ethanone hydrochloride 2-Bromo-4'-nitroacetophenone (25 g) prepared in Example 1 was dissolved in dichloromethane (250 mL), hexamethylenetetramine (20.1 g) was added, and the reaction was stirred for 1 hour at room temperature. After the reaction was completed, the solid crude product (30 g) was collected by filtration. The crude product was dissolved in a mixture of ethanol (162 mL) and concentrated hydrochloric acid (40 mL) and the reaction was continued with stirring for about 3 hours. After the reaction mixture was left to stand for about 48 hours, the solid product was precipitated, filtered, washed with water and dried to give the target compound 2-amino-1-(4-nitrophenyl)ethanone hydrochloride (refer to the method described in US4812470). Yield: 11.8 g (72% yield); 1H NMR (DMSO-d6, 300MHz): δ 8.3 (broad peak, 3H), 8.38 (double peak, 2H), 8.27 (double peak, 2H), 4.68 (single peak, 2H).

References

[1] Patent: WO2011/55289, 2011, A2. Location in patent: Page/Page column 36
[2] Patent: WO2012/29032, 2012, A2. Location in patent: Example 2
[3] European Journal of Medicinal Chemistry, 2012, vol. 54, p. 324 - 342
[4] European Journal of Medicinal Chemistry, 2014, vol. 79, p. 203 - 215
[5] Journal of Medicinal Chemistry, 1982, vol. 25, # 9, p. 1045 - 1050

2-AMINO-(4'-NITRO)ACETOPHENONE HYDROCHLORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-AMINO-(4'-NITRO)ACETOPHENONE HYDROCHLORIDE manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: 2-amino-(4'-nitro)acetophenone hydrochloride 5425-81-0
Price: US $1.10-9.90/KG
Min. Order: 1KG
Purity: 99% min
Supply Ability: 100kg
Release date: 2025-08-18

5425-81-0, 2-AMINO-(4'-NITRO)ACETOPHENONE HYDROCHLORIDERelated Search:

OTAVA-BB BB7110952478

2-AMINO-P-NITRO-ACETOPHENONE HYDROCHLORIDE

2-AMINO-1-(4-NITRO-PHENYL)-ETHANONE HYDROCHLORIDE

2-AMINO-(4'-NITRO)ACETOPHENONE HYDROCHLORIDE

AURORA 23208

Ethanone, 2-amino-1-(4-nitrophenyl)-, hydrochloride (1:1)

2-AMino-p-nitro-acetophenone HCl

2-AMino-4'-nitroacetophenone HCl

2-Amino-1-(4-nitrophenyl)ethanone hydrochloride (1:1)

2-Amino-(4′-nitro)acetophenone hydrochloride, CAS 5425-81-0

5425-81-0

5428-81-0

Aromatic Acetophenones & Derivatives (substituted)