ChemicalBook > CAS DataBase List > 1-(3-bromopropyl)-4-chlorobenzene

1-(3-bromopropyl)-4-chlorobenzene

Product Name
1-(3-bromopropyl)-4-chlorobenzene
CAS No.
64473-35-4
Chemical Name
1-(3-bromopropyl)-4-chlorobenzene
Synonyms
3-(4-Chlorophenyl)propyl bromide;3-(4-Chlorophenyl)-1-bromopropane;1-Chloro-4-(3-bromopropyl)benzene;1-(3-bromopropyl)-4-chlorobenzene;Benzene, 1-(3-bromopropyl)-4-chloro-
CBNumber
CB31481775
Molecular Formula
C9H10BrCl
Formula Weight
233.53
MOL File
64473-35-4.mol
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1-(3-bromopropyl)-4-chlorobenzene Property

Boiling point:
92 °C(Press: 0.3 Torr)
Density 
1.424
storage temp. 
Sealed in dry,Room Temperature
Appearance
light yellow liquid
InChI
InChI=1S/C9H10BrCl/c10-7-1-2-8-3-5-9(11)6-4-8/h3-6H,1-2,7H2
InChIKey
OVXYDNVSUOXGQG-UHFFFAOYSA-N
SMILES
C1(CCCBr)=CC=C(Cl)C=C1
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC
Product number
B689788
Product name
1-(3-Bromopropyl)-4-chlorobenzene
Packaging
250mg
Price
$105
Updated
2021/12/16
Matrix Scientific
Product number
097778
Product name
1-(3-Bromopropyl)-4-chlorobenzene
Purity
95+%
Packaging
1g
Price
$227
Updated
2021/12/16
AK Scientific
Product number
V7097
Product name
1-(3-Bromopropyl)-4-chlorobenzene
Packaging
1g
Price
$151
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0356481
Product name
1-(3-BROMOPROPYL)-4-CHLOROBENZENE
Purity
95.00%
Packaging
5MG
Price
$504.74
Updated
2021/12/16
Matrix Scientific
Product number
097778
Product name
1-(3-Bromopropyl)-4-chlorobenzene
Purity
95+%
Packaging
5g
Price
$706
Updated
2021/12/16
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1-(3-bromopropyl)-4-chlorobenzene Chemical Properties,Usage,Production

Synthesis

6282-88-8

64473-35-4

1. Preparation of 1-(3-bromopropyl)-4-chlorobenzene a. Triphenylphosphine (7.42 g, 28.3 mmol) was dissolved in dichloromethane (200 mL) and cooled at 0 °C. b. A solution of bromine (1.46 mL, 28.3 mmol) in dichloromethane (40 mL) was slowly added to the above cooled solution over 30 min. c. A dichloromethane (20 mL) solution of 3-(4-chlorophenyl)propan-1-ol (4.6 g, 27 mmol) was added. d. Gradually warm the reaction mixture to room temperature with continuous stirring for 24 hours. e. The reaction mixture was transferred to a partition funnel and washed sequentially with saturated sodium bicarbonate solution, water and brine. f. The organic layer was dried with anhydrous sodium sulfate and subsequently concentrated. g. The residue was purified by silica gel column chromatography (silica gel size: 230-400 mesh, 350 g; eluent: 7.5% ethyl acetate/hexane) to afford 6.15 g (97% yield) of the target product 1-(3-bromopropyl)-4-chlorobenzene as a clear, colorless oil. h. Product characterization data: - NMR hydrogen spectrum (400 MHz, CDCl3) δ 2.16 (2H, m), 2.77 (2H, t), 3.41 (2H, t), 7.15 (2H, d), 7.27 (2H, d). h. Product characterization data. - HPLC retention time: 5.1 min (Method A).

References

[1] Patent: WO2011/126567, 2011, A1. Location in patent: Page/Page column 164
[2] Patent: US6407298, 2002, B1. Location in patent: Page column 5
[3] Patent: WO2010/146111, 2010, A1. Location in patent: Page/Page column 114
[4] Journal of Medicinal Chemistry, 2002, vol. 45, # 16, p. 3549 - 3557
[5] Bioorganic and Medicinal Chemistry Letters, 2006, vol. 16, # 18, p. 4752 - 4756

1-(3-bromopropyl)-4-chlorobenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1-(3-bromopropyl)-4-chlorobenzene manufacturers

Career Henan Chemical Co
Product
1-(3-bromopropyl)-4-chlorobenzene 64473-35-4
Price
US $1.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1KG, 5KG, 50KG
Release date
2020-01-14

64473-35-4, 1-(3-bromopropyl)-4-chlorobenzeneRelated Search:

3-BROMOCHLOROBENZENE

  • 1-Chloro-4-(3-bromopropyl)benzene
  • 3-(4-Chlorophenyl)-1-bromopropane
  • 3-(4-Chlorophenyl)propyl bromide
  • 1-(3-bromopropyl)-4-chlorobenzene
  • Benzene, 1-(3-bromopropyl)-4-chloro-
  • 64473-35-4