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N-(2-AMINOETHYL)METHANESULFONAMIDE

Product Name
N-(2-AMINOETHYL)METHANESULFONAMIDE
CAS No.
202197-61-3
Chemical Name
N-(2-AMINOETHYL)METHANESULFONAMIDE
Synonyms
N-(2-AMINOETHYL)METHANESULFONAMIDE;Methanesulfonamide, N-(2-aminoethyl)-, hydrochloride (1:1)
CBNumber
CB31491703
Molecular Formula
C3H11ClN2O2S
Formula Weight
174.64
MOL File
202197-61-3.mol
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N-(2-AMINOETHYL)METHANESULFONAMIDE Property

storage temp. 
Storage temp. 2-8°C
Appearance
White to off-white Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific
Product number
4112DA
Product name
N-(2-Aminoethyl)methanesulfonamidehydrochloride
Packaging
1g
Price
$392
Updated
2021/12/16
ChemBridge Corporation
Product number
BB-4029868
Product name
N-(2-aminoethyl)methanesulfonamidehydrochloride
Purity
95%
Packaging
5G
Price
$460
Updated
2021/12/16
Crysdot
Product number
CD13018843
Product name
N-(2-Aminoethyl)methanesulfonamidehydrochloride
Purity
95+%
Packaging
5g
Price
$540
Updated
2021/12/16
AstaTech
Product number
AR2420
Product name
N-(2-AMINOETHYL)METHANESULFONAMIDEHCL
Purity
95%
Packaging
5/ G
Price
$704
Updated
2021/12/16
ChemBridge Corporation
Product number
BB-4029868
Product name
N-(2-aminoethyl)methanesulfonamidehydrochloride
Purity
95%
Packaging
10g
Price
$745
Updated
2021/12/16
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N-(2-AMINOETHYL)METHANESULFONAMIDE Chemical Properties,Usage,Production

Synthesis

1190044-23-5

202197-61-3

N-(2-Aminoethyl)methane sulfonamide hydrochloride was synthesized from tert-butyl {2-[(methylsulfonyl)amino]ethyl}carbamate (4.44 g) by the method of Example 17. The steps were as follows: the raw material was dissolved in a solvent mixture of ethyl acetate (40 mL) and THF (20 mL), and a 4M HCl-ethyl acetate solution (23 mL) was slowly added at room temperature. The reaction mixture was stirred at room temperature for 23 hours. Upon completion of the reaction, the solvent was removed by concentration under reduced pressure, and the resulting residue was washed with ethyl acetate to give the final N-(2-aminoethyl)methane sulfonamide hydrochloride (3.02 g, 93% yield) as white crystals. The product was characterized by 1H NMR (300 MHz, DMSO-d6) with chemical shifts of δ 2.90 (2H, t, J = 6.4 Hz), 2.96 (3H, s), 3.20 (2H, t, J = 6.2 Hz), 7.35 (1H, br.s.), 8.06 (3H, s).

References

[1] Patent: EP2261213, 2010, A1. Location in patent: Page/Page column 44
[2] Patent: EP2484678, 2012, A1. Location in patent: Page/Page column 19
[3] Patent: US2012/208833, 2012, A1. Location in patent: Page/Page column 13
[4] Patent: WO2018/39621, 2018, A1. Location in patent: Paragraph 00364-00365

N-(2-AMINOETHYL)METHANESULFONAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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N-(2-AMINOETHYL)METHANESULFONAMIDE Suppliers

China 12 Ukraine 2 United States 1 Global 15
Enamine
Tel
--
Fax
--
Email
enamine@enamine.net
Country
Ukraine
ProdList
6216
Advantage
67
UkrOrgSynthesis Ltd.
Tel
--
Fax
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Email
y.barysheva@ukrorgsynth.com
Country
Ukraine
ProdList
6230
Advantage
38

202197-61-3, N-(2-AMINOETHYL)METHANESULFONAMIDERelated Search:

N-(2-Aminoethyl)-N-benzylglycine Bis(trifluoroacetate) A-3 HYDROCHLORIDE N-(2-AMINO-PHENYL)-4-FLUORO-BENZENESULFONAMIDE N-(2-aminoethyl)-N-methylmethanesulfonamide hydrochloride N-(2-AMINOETHYL)MALEIMIDE TRIFLUOROACETA N-(2-aminoethyl)-4-methyl-benzenesulfonamide

  • N-(2-AMINOETHYL)METHANESULFONAMIDE
  • Methanesulfonamide, N-(2-aminoethyl)-, hydrochloride (1:1)
  • 202197-61-3
  • C3H10N2O2S