1H-Pyrrolo[2,3-b]pyridine, 5-bromo-1-(phenylsulfonyl)-
- Product Name
- 1H-Pyrrolo[2,3-b]pyridine, 5-bromo-1-(phenylsulfonyl)-
- CAS No.
- 1001070-33-2
- Chemical Name
- 1H-Pyrrolo[2,3-b]pyridine, 5-bromo-1-(phenylsulfonyl)-
- Synonyms
- 5-Bromo-1-(phenylsulfonyl...;5-BroMo-1-(phenylsulfonyl)-7-azaindole;1-(phenylsulfonyl)-5-bromo-7-azaindole;1-(Phenylsulphonyl)-5-broMo-7-azaindole;1-(Benzenesulfonyl)-5-broMopyrrolo[2,3-b]pyridine;5-Bromo-1-(benzenesulfonyl)-1H-pyrrolo[2,3-b]pyridine;1H-Pyrrolo[2,3-b]pyridine, 5-bromo-1-(phenylsulfonyl)-
- CBNumber
- CB31871819
- Molecular Formula
- C13H9BrN2O2S
- Formula Weight
- 337.19
- MOL File
- 1001070-33-2.mol
1H-Pyrrolo[2,3-b]pyridine, 5-bromo-1-(phenylsulfonyl)- Property
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- White to off-white Solid
Safety
- WGK Germany
- 3
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H319Causes serious eye irritation
- Precautionary statements
-
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- ADE000931
- Product name
- 1-Benzenesulfonyl-5-bromo-1H-pyrrolo[2,3-b]pyridine
- Purity
- Aldrich
- Packaging
- 1g
- Price
- $761
- Updated
- 2023/06/20
- Product number
- B190033
- Product name
- 1-Benzenesulfonyl-5-bromo-1H-pyrrolo[2,3-b]pyridine
- Packaging
- 100mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- 8H69-9-12
- Product name
- 1-(Benzenesulfonyl)-5-bromopyrrolo[2,3-b]pyridine
- Packaging
- 1g
- Price
- $125
- Updated
- 2021/12/16
- Product number
- 026229
- Product name
- 1-Benzenesulfonyl-5-bromo-1H-pyrrolo[2,3-b]pyridine
- Packaging
- 250mg
- Price
- $321
- Updated
- 2021/12/16
- Product number
- HCH0039072
- Product name
- 1-BENZENESULFONYL-5-BROMO-1H-PYRROLO[2,3-B]PYRIDINE
- Purity
- 95.00%
- Packaging
- 100MG
- Price
- $837.38
- Updated
- 2021/12/16
1H-Pyrrolo[2,3-b]pyridine, 5-bromo-1-(phenylsulfonyl)- Chemical Properties,Usage,Production
Synthesis
754214-54-5
98-09-9
1001070-33-2
GENERAL STEPS: Sodium hydroxide (4.1 g, 102.8 mmol) was added to a dichloromethane solution containing tetrabutylammonium bromide (331 mg, 1.0 mmol) and 5-bromo-1H-pyrrolo[2,3-b]pyridine (6.7 g, 34.7 mmol). The mixture was stirred at 0 °C for 5 min. Subsequently, benzenesulfonyl chloride (5.7 mL, 44.5 mmol) was added slowly at 0 °C. The reaction mixture was continued to be stirred at 0 °C for 15 minutes, then gradually warmed to 25 °C and stirred continuously at this temperature for 12 hours. After completion of the reaction, the mixture was filtered and the filtrate was concentrated in vacuum and washed with hexane to afford 1-benzenesulfonyl-5-bromo-1H-pyrrolo[2,3-b]pyridine as a white solid (11.8 g, 100% yield). LC/MS analysis: m/e calculated value C13H10BrN2O2S [M+H]+ 338.20, measured values 337.1, 339.1 1H NMR (400 MHz, CDCl3) δ ppm: 6.56 (d, J = 4.0 Hz, 1H), 7.51 (m, 2H), 7.60 (m, 1H), 7.75 (d, J = 4.0 Hz, 1H), 7.98 (d, J = 2.1 Hz, 1H), 8.18 (m, 2H), 8.45 (d, J = 2.0 Hz. 1H).
References
[1] Patent: US2011/144105, 2011, A1. Location in patent: Page/Page column 16
1H-Pyrrolo[2,3-b]pyridine, 5-bromo-1-(phenylsulfonyl)- Preparation Products And Raw materials
Raw materials
Preparation Products
1H-Pyrrolo[2,3-b]pyridine, 5-bromo-1-(phenylsulfonyl)- Suppliers
- Tel
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- Fax
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- sales@ajchem.in
- Country
- India
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- 6100
- Advantage
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View Lastest Price from 1H-Pyrrolo[2,3-b]pyridine, 5-bromo-1-(phenylsulfonyl)- manufacturers
- Product
- 1-(Benzenesulfonyl)-5-broMopyrrolo[2,3-b]pyridine 1001070-33-2
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-06-27