4-methyl-5-nitro-1H-indole

Product Name: 4-methyl-5-nitro-1H-indole
CAS No.: 165250-69-1
Chemical Name: 4-methyl-5-nitro-1H-indole
Synonyms: 4-Methyl-5-nitroindole;4-methyl-5-nitro-1H-indole;1H-Indole, 4-Methyl-5-nitro-
CBNumber: CB31871910
Molecular Formula: C9H8N2O2
Formula Weight: 176.17
MOL File: 165250-69-1.mol

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4-methyl-5-nitro-1H-indole Property

Boiling point:: 359.9±22.0 °C(Predicted)
Density: 1.355±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 15.61±0.30(Predicted)
Appearance: Yellow to green Solid
InChI: InChI=1S/C9H8N2O2/c1-6-7-4-5-10-8(7)2-3-9(6)11(12)13/h2-5,10H,1H3
InChIKey: XRJNLFAXLSBIDS-UHFFFAOYSA-N
SMILES: N1C2=C(C(C)=C([N+]([O-])=O)C=C2)C=C1

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: M341828
Product name: 4-Methyl-5-nitro-1H-indole
Packaging: 100mg
Price: $90
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H54-1-5S
Product name: 4-Methyl-5-nitro-1H-indole
Packaging: 250mg
Price: $320
Updated: 2021/12/16

Matrix Scientific

Product number: 118985
Product name: 4-Methyl-5-nitro-1H-indole
Purity: 95+%
Packaging: 250mg
Price: $468
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0386137
Product name: 4-METHYL-5-NITRO-1H-INDOLE
Purity: 95.00%
Packaging: 5MG
Price: $501.34
Updated: 2021/12/16

Apolloscientific

Product number: OR301286
Product name: 4-Methyl-5-nitro-1H-indole
Packaging: 1g
Price: $696
Updated: 2021/12/16

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4-methyl-5-nitro-1H-indole Chemical Properties,Usage,Production

Synthesis

6146-52-7

165250-69-1

General procedure for the synthesis of 4-methyl-5-nitro-1H-indole using 5-nitroindole as starting material: to an anhydrous THF solution (20 mL) of 5-nitroindole (purchased from Aldrich, 0.82 g, 5.1 mmol) was slowly added methylmagnesium bromide (5.0 mL, 15 mmol), and the reaction was stirred continuously for 1 hr at 25 °C. Subsequently, the reaction was quenched by addition of THF solution of tetrachloro-1,4-benzoquinone (1.2 g, 4.9 mmol). The reaction mixture was concentrated under reduced pressure to give a dark colored solid. This solid was purified by column chromatography (eluent: 30% ethyl acetate/hexane) to give the final target product 4-methyl-5-nitro-1H-indole (0.72 g, 4.1 mmol, 80% yield).

References

[1] Patent: US5677321, 1997, A

4-methyl-5-nitro-1H-indole Preparation Products And Raw materials

Raw materials

Preparation Products

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4-methyl-5-nitro-1H-indole Suppliers

China 66 India 4 Switzerland 1 United Kingdom 1 United States 6 Global 78

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