2-CHLORO-1-PIPERIDIN-1-YL-ETHANONE

Product Name: 2-CHLORO-1-PIPERIDIN-1-YL-ETHANONE
CAS No.: 1440-60-4
Chemical Name: 2-CHLORO-1-PIPERIDIN-1-YL-ETHANONE
Synonyms: LABOTEST-BB LT00000083;1-(CHLOROACETYL)PIPERIDINE;Pipridine, 1-chloroacetyl-;2-chloro-1-piperidino-ethanone;Piperidine, N-[2-chloroacetyl]-;2-CHLORO-1-PIPERIDINE ACETAMIDE;2-chloro-1-(1-piperidyl)ethanone;2-CHLORO-1-PIPERIDIN-1-YL-ETHANONE;2-Chloro-1-(1-piperidinyl)ethanone;2-Chloro-1-piperidine-1-yl-ethanone
CBNumber: CB3209820
Molecular Formula: C7H12ClNO
Formula Weight: 161.63
MOL File: 1440-60-4.mol

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2-CHLORO-1-PIPERIDIN-1-YL-ETHANONE Property

Boiling point:: 85°C/0.08mm
storage temp.: Storage temp. 2-8°C
form: liquid
color: Yellow
CAS DataBase Reference: 1440-60-4(CAS DataBase Reference)

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Safety

HS Code: 29333990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC

Product number: C380353
Product name: 2-Chloro-1-piperidin-1-yl-ethanone
Packaging: 500mg
Price: $65
Updated: 2021/12/16

TRC

Product number: C380353
Product name: 2-Chloro-1-piperidin-1-yl-ethanone
Packaging: 100mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC133246
Product name: 1-(Chloroacetyl)piperidine
Packaging: 500mg
Price: $60
Updated: 2021/12/16

Matrix Scientific

Product number: 138408
Product name: 1-(Chloroacetyl)piperidine
Purity: 95%+
Packaging: 5g
Price: $323
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC133246
Product name: 1-(Chloroacetyl)piperidine
Packaging: 5G
Price: $358
Updated: 2021/12/16

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2-CHLORO-1-PIPERIDIN-1-YL-ETHANONE Chemical Properties,Usage,Production

Synthesis

110-89-4

79-04-9

1440-60-4

GENERAL METHOD: Chloroacetyl chloride (3.70 mL, 46.45 mmol) was slowly added dropwise to a solution of hexahydropyridine (4.50 mL, 51.45 mmol) and triethylamine (7.90 mL, 56.68 mmol) in methylene chloride (80 mL) at 0°C. The reaction temperature was kept constant for 6 hours. After the dropwise addition was completed by keeping the reaction temperature at 0 °C, the reaction mixture was gradually warmed up to room temperature and stirred for 6 hours. After completion of the reaction, the reaction mixture was diluted with dichloromethane, washed with saturated sodium bicarbonate solution and brine sequentially, the organic phase was dried with anhydrous magnesium sulfate and filtered. The filtrate was concentrated under reduced pressure to give 2-chloro-1-(piperidin-1-yl)ethanone (7.55 g, 99% yield) as a light yellow liquid.

References

[1] Canadian Journal of Chemistry, 2004, vol. 82, # 5, p. 622 - 630
[2] Molecules, 2015, vol. 20, # 11, p. 19984 - 20013
[3] Synthetic Communications, 1998, vol. 28, # 22, p. 4257 - 4272
[4] Patent: WO2012/52843, 2012, A1. Location in patent: Page/Page column 73-74
[5] Chemistry - A European Journal, 2012, vol. 18, # 29, p. 8978 - 8986

2-CHLORO-1-PIPERIDIN-1-YL-ETHANONE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-CHLORO-1-PIPERIDIN-1-YL-ETHANONE Suppliers

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1440-60-4, 2-CHLORO-1-PIPERIDIN-1-YL-ETHANONERelated Search:

ETHYL 1-(2-CHLOROACETYL)-4-PIPERIDINECARBOXYLATE 2-CHLORO-1-PIPERIDIN-1-YL-ETHANONE N-CHLOROACETYLISONIPECOTIC ACID ETHYL 1-(2-CHLORO-2,2-DIFLUOROACETYL)-4-PIPERIDINECARBOXYLATE ETHYL 1-(CHLOROACETYL)PIPERIDINE-2-CARBOXYLATE 1-(4-BENZYL-PIPERIDIN-1-YL)-2-CHLORO-ETHANONE 1-(CHLOROACETYL)-4-METHYLPIPERIDINE 2-Chloro-1-(2,6-dimethyl-piperidin-1-yl)-ethanone 2-CHLORO-2,2-DIFLUORO-1-(4-HYDROXYPIPERIDINO)-1-ETHANONE 4-Piperidinecarboxamide, 1-(chloroacetyl)- (9CI) Piperidine, 1-(chloroacetyl)-3,5-dimethyl- (9CI) 1-(2-chloropropanoyl)piperidine 1-(chloroacetyl)-2-methylpiperidine 1-(2-CHLORO-ACETYL)-PIPERIDINE-3-CARBOXYLIC ACID ETHYL ESTER 2-CHLORO-1-(2-(2-[3,5-DI(TRIFLUOROMETHYL)ANILINO]ETHYL)PIPERIDINO)ETHAN-1-ONE 2,3,3-TRICHLORO-1-(4-[3-(4-CHLOROPHENYL)-1,2,4-OXADIAZOL-5-YL]PIPERIDINO)PROP-2-EN-1-ONE 2-CHLORO-3,3,3-TRIFLUORO-1-PIPERIDINO-1-PROPANONE 2-CHLORO-1-(3-METHYL-PIPERIDIN-1-YL)-ETHANONE

2-Chloro-1-piperidine-1-yl-ethanone

2-Chloro-1-(1-piperidinyl)ethanone

2-CHLORO-1-PIPERIDIN-1-YL-ETHANONE

2-CHLORO-1-PIPERIDINE ACETAMIDE

1-(CHLOROACETYL)PIPERIDINE

Piperidine, N-[2-chloroacetyl]-

LABOTEST-BB LT00000083

Piperidine, 1-(chloroacetyl)- (6CI,7CI,8CI,9CI)

2-CHLORO-1-PIPERIDIN-1-YL-ETHANONE >98%

2-Chloro-1-(piperidin-1-yl)ethan-1-one, 1-(2-Chloroethanoyl)piperidine

2-chloro-1-(1-piperidyl)ethanone

2-chloro-1-piperidino-ethanone

JR-8642, 1-(Chloroacetyl)piperidine, 97%

2-chloro-1-(piperidin-1-yl)ethan-1-one

Pipridine, 1-chloroacetyl-

Ethanone, 2-chloro-1-(1-piperidinyl)-

1440-60-4

Piperidine

ACETYLHALIDE