ChemicalBook > CAS DataBase List > ETHYL 3,4-DIMETHOXYPHENYLACETATE

ETHYL 3,4-DIMETHOXYPHENYLACETATE

Product Name
ETHYL 3,4-DIMETHOXYPHENYLACETATE
CAS No.
18066-68-7
Chemical Name
ETHYL 3,4-DIMETHOXYPHENYLACETATE
Synonyms
ethyl homoveratrate;Ethyl dimethoxyphenylacetate;HOMOVERATRIC ACID ETHYL ESTER;ETHYL 3,4-DIMETHOXYPHENYLACETATE;ETHYL 2-(3,4-DIMETHOXYPHENYL)ACETATE;Ethyl 3,4-dimethoxyphenylacetate, 98+%;3,4-dimethoxy-benzeneaceticaciethylester;3,4-Dimethoxybenzeneacetic acid ethyl ester;2-(3,4-dimethoxyphenyl)acetic acid ethyl ester;Benzeneacetic acid, 3,4-dimethoxy-, ethyl ester
CBNumber
CB3233807
Molecular Formula
C12H16O4
Formula Weight
224.25
MOL File
18066-68-7.mol
More
Less

ETHYL 3,4-DIMETHOXYPHENYLACETATE Property

Boiling point:
191 °C
Density 
1.084±0.06 g/cm3(Predicted)
refractive index 
1.5180
Flash point:
159-160°C/4mm
storage temp. 
Sealed in dry,Room Temperature
form 
liquid
color 
Brown
BRN 
2697968
CAS DataBase Reference
18066-68-7(CAS DataBase Reference)
EPA Substance Registry System
Benzeneacetic acid, 3,4-dimethoxy-, ethyl ester (18066-68-7)
More
Less

Safety

TSCA 
Yes
HS Code 
2915390090
More
Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

More
Less

N-Bromosuccinimide Price

Sigma-Aldrich
Product number
PH011221
Product name
ethyl (3,4-dimethoxyphenyl)acetate
Purity
AldrichCPR
Packaging
500mg
Price
$172
Updated
2023/06/20
TRC
Product number
B125020
Product name
Ethyl2-(3,4-Dimethoxyphenyl)acetate
Packaging
2.5g
Price
$75
Updated
2021/12/16
SynQuest Laboratories
Product number
2623-1-X2
Product name
Ethyl 3,4-dimethoxyphenylacetate
Purity
98%
Packaging
25g
Price
$120
Updated
2021/12/16
AK Scientific
Product number
E006
Product name
Ethyl2-(3,4-dimethoxyphenyl)acetate
Packaging
5g
Price
$15
Updated
2021/12/16
Matrix Scientific
Product number
119718
Product name
Ethyl 2-(3,4-dimethoxyphenyl)acetate
Purity
98%
Packaging
10g
Price
$46
Updated
2021/12/16
More
Less

ETHYL 3,4-DIMETHOXYPHENYLACETATE Chemical Properties,Usage,Production

Synthesis

93-40-3

64-17-5

18066-68-7

In a typical reaction, 3,4-dimethoxyphenylacetic acid (332 g, 0.6 mol), ethanol (1.5-2 mol), and AMA 2:3 were mixed in a provided reaction glass tube equipped with a screw cap and magnetic stirrer until a wet mixture was formed. The reaction mixture was placed in a microwave reactor (Anton Parr Monowave 300) and irradiated at 80°C for 8 min or 120°C for 20 min. Upon completion of the reaction, the mixture was cooled, diluted with dichloromethane (41 mL), filtered by gravity and the filtrate was washed with dichloromethane. Subsequently, the filtrate was washed with saturated sodium carbonate solution and water. The organic layer was separated, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give ethyl 3,4-dimethoxyphenylacetate.

References

[1] Bioorganic and Medicinal Chemistry, 2007, vol. 15, # 4, p. 1586 - 1605
[2] Journal of Organic Chemistry, 2003, vol. 68, # 3, p. 1165 - 1167
[3] Synthetic Communications, 2014, vol. 44, # 16, p. 2386 - 2392
[4] Journal of Organic Chemistry, 2010, vol. 75, # 19, p. 6549 - 6562
[5] Tetrahedron, 1997, vol. 53, # 30, p. 10555 - 10564

ETHYL 3,4-DIMETHOXYPHENYLACETATE Preparation Products And Raw materials

Raw materials

Preparation Products

More
Less

ETHYL 3,4-DIMETHOXYPHENYLACETATE Suppliers

Belgium 1 China 43 Germany 2 India 3 Ukraine 1 United Kingdom 9 United States 15 Global 74
GLR Innovations
Tel
+91 9891111994
Email
info@glrgroup.in
Country
India
ProdList
4535
Advantage
58
A.J Chemicals
Tel
--
Fax
--
Email
sales@ajchem.in
Country
India
ProdList
6100
Advantage
58
CHEMSWORTH
Tel
--
Fax
--
Email
info@chemsworth.com
Country
India
ProdList
6700
Advantage
30
More
Less

View Lastest Price from ETHYL 3,4-DIMETHOXYPHENYLACETATE manufacturers

Career Henan Chemica Co
Product
ETHYL 3,4-DIMETHOXYPHENYLACETATE 18066-68-7
Price
US $1.00/KG
Min. Order
1KG
Purity
MIn98%HPLC/LC
Supply Ability
100KGS
Release date
2020-10-29

18066-68-7, ETHYL 3,4-DIMETHOXYPHENYLACETATERelated Search:

ETHYL 3,4-DIMETHOXYPHENYLACETATE propyl 4-diethylcarbamoylmethoxy-3-methoxyphenylacetate (3,4-Dimethoxyphenyl)acetic acid ETHYL 3,4-ETHYLENEDIOXYBENZOYLFORMATE ETHYL 3,4,5-TRIMETHOXYBENZOYLFORMATE ethyl 3,4-dimethoxyphenylglyoxylate 6,7-DIMETHOXY-1,2,3,4-TETRAHYDRO-ISOQUINOLINE-1-CARBOXYLIC ACID ETHYL ESTER (4,5-DIMETHOXY-2-NITRO-PHENYL)-ACETIC ACID ETHYL ESTER 2-ACETYL-6,7-DIMETHOXY-1,2,3,4-TETRAHYDRO-ISOQUINOLINE-1-CARBOXYLIC ACID ETHYL ESTER DIETHYL 3,4,5-TRIMETHOXYPHENYL MALONATE ETHYL 2,5-DIMETHOXYPHENYLACETATE RARECHEM AK ML 0195 MANDELIC ACID, 3,4-DIMETHOXY-alpha-ISOPROPENYL-, 1-METHYL-4-PIPERIDYL ESTER AKOS AU36-M280 AKOS AU36-M469 AKOS AU36-M283 AKOS AU36-M281 RARECHEM AK ML 0170

  • 3,4-dimethoxy-benzeneaceticaciethylester
  • Acetic acid, (3,4-dimethoxyphenyl)-, ethyl ester
  • Benzeneacetic acid, 3,4-dimethoxy-, ethyl ester
  • Ethyl dimethoxyphenylacetate
  • ETHYL 3,4-DIMETHOXYPHENYLACETATE
  • ETHYL 2-(3,4-DIMETHOXYPHENYL)ACETATE
  • HOMOVERATRIC ACID ETHYL ESTER
  • 3,4-Dimethoxyphenylacetic acid ethyl ester~Ethyl homoveratrate
  • ethyl homoveratrate
  • Ethyl 3,4-dimethoxyphenylacetate, 98+%
  • 3,4-Dimethoxybenzeneacetic acid ethyl ester
  • 2-(3,4-dimethoxyphenyl)acetic acid ethyl ester
  • 18066-68-7
  • Catechol Derivatives
  • Aromatic Esters