3-AMINO-1H-PYRROLE-2,4-DICARBOXYLIC ACID DIETHYL ESTER

Product Name: 3-AMINO-1H-PYRROLE-2,4-DICARBOXYLIC ACID DIETHYL ESTER
CAS No.: 853058-40-9
Chemical Name: 3-AMINO-1H-PYRROLE-2,4-DICARBOXYLIC ACID DIETHYL ESTER
Synonyms: Diethyl 3-amino-1H-2,4-pyrroledicarboxylate;DIETHYL 3-AMINO-1H-PYRROLE-2,4-DICARBOXYLATE;2,4-diethyl 3-amino-1H-pyrrole-2,4-dicarboxylate;3-AMINO-1H-PYRROLE-2,4-DICARBOXYLIC ACID DIETHYL ESTER;1H-Pyrrole-2,4-dicarboxylic acid, 3-amino-, 2,4-diethyl ester
CBNumber: CB32454161
Molecular Formula: C10H14N2O4
Formula Weight: 226.23
MOL File: 853058-40-9.mol

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3-AMINO-1H-PYRROLE-2,4-DICARBOXYLIC ACID DIETHYL ESTER Property

Boiling point:: 410.0±40.0 °C(Predicted)
Density: 1.265±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Store in freezer, under -20°C
pka: 14.35±0.50(Predicted)

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Safety

HazardClass: IRRITANT

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Matrix Scientific

Product number: 059892
Product name: Diethyl 3-amino-1H-pyrrole-2,4-dicarboxylate
Purity: >95%
Packaging: 250mg
Price: $116
Updated: 2021/12/16

Matrix Scientific

Product number: 059892
Product name: Diethyl 3-amino-1H-pyrrole-2,4-dicarboxylate
Purity: >95%
Packaging: 1g
Price: $342
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0377361
Product name: DIETHYL-3-AMINO-1H-PYRROLE-2,4-DICARBOXYLATE
Purity: 95.00%
Packaging: 5MG
Price: $496.86
Updated: 2021/12/16

AK Scientific

Product number: 0749AF
Product name: Diethyl3-amino-1H-pyrrole-2,4-dicarboxylate
Packaging: 5g
Price: $1101.2
Updated: 2021/12/16

Crysdot

Product number: CD11045525
Product name: Diethyl3-amino-1H-pyrrole-2,4-dicarboxylate
Purity: 95+%
Packaging: 250mg
Price: $80
Updated: 2021/12/16

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3-AMINO-1H-PYRROLE-2,4-DICARBOXYLIC ACID DIETHYL ESTER Chemical Properties,Usage,Production

Synthesis

144918-37-6

13433-00-6

853058-40-9

Diethyl 2-aminomalonate hydrochloride (20 g, 90 mmol) and ethyl 2-cyano-3-ethoxyacrylate (16 g, 94 mmol) were dissolved in ethanol (250 mL). Sodium ethoxide (21 g, 310 mmol) was added to the solution and the reaction mixture was heated to reflux for 14 hours. Upon completion of the reaction, the reaction solution was neutralized with acetic acid (20 mL) and subsequently concentrated. The concentrated mixture was partitioned between dichloromethane and water for liquid-liquid separation. The aqueous layer was extracted twice with dichloromethane. All organic layers were combined, washed with brine, dried over anhydrous sodium sulfate and concentrated. The resulting solid was ground overnight with a mixture of heptane and dichloromethane (10:1 v/v). The suspension was filtered to give 12.5 g of diethyl 3-amino-1H-pyrrole-2,4-dicarboxylate as a solid in 80% yield. The product was characterized by 1H NMR (400 MHz, DMSO-d6): δ 11.53 (s, 1H), 7.20 (d, J = 4.0 Hz, 1H), 5.57 (s, 2H), 4.27-4.11 (m, 4H), 1.32-1.19 (m, 6H).

References

[1] Patent: WO2011/25940, 2011, A1. Location in patent: Page/Page column 85

3-AMINO-1H-PYRROLE-2,4-DICARBOXYLIC ACID DIETHYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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3-AMINO-1H-PYRROLE-2,4-DICARBOXYLIC ACID DIETHYL ESTER Suppliers

China 45 India 1 United States 1 Global 47

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View Lastest Price from 3-AMINO-1H-PYRROLE-2,4-DICARBOXYLIC ACID DIETHYL ESTER manufacturers

Career Henan Chemical Co

Product: 3-AMINO-1H-PYRROLE-2,4-DICARBOXYLIC ACID DIETHYL ESTER 853058-40-9
Price: US $1.00/g
Min. Order: 1g
Purity: ≥98%
Supply Ability: g/kg/Ton
Release date: 2019-12-25

853058-40-9, 3-AMINO-1H-PYRROLE-2,4-DICARBOXYLIC ACID DIETHYL ESTERRelated Search:

METHYL 3-AMINO-4-FLUOROBENZENECARBOXYLATE 2,6-Dioxopiperidine-3-ammonium chloride 3-AMINO-2-PIPERIDINONE HYDROCHLORIDE 1H-Pyrrole-2,4-dicarboxylicacid,3-amino-,dimethylester(9CI) 3-AMINO-1H-PYRROLE-2,4-DICARBOXYLIC ACID DIETHYL ESTER 3-AMINO-PHENYL-1H-PYRROLE-2,4-DICARBOXYLIC ACID DIEHYL ESTER

3-AMINO-1H-PYRROLE-2,4-DICARBOXYLIC ACID DIETHYL ESTER

DIETHYL 3-AMINO-1H-PYRROLE-2,4-DICARBOXYLATE

2,4-diethyl 3-amino-1H-pyrrole-2,4-dicarboxylate

1H-Pyrrole-2,4-dicarboxylic acid, 3-amino-, 2,4-diethyl ester

Diethyl 3-amino-1H-2,4-pyrroledicarboxylate

853058-40-9