ChemicalBook > CAS DataBase List > 5-FLUORO-6-METHOXY-3-PYRIDINECARBOXYLIC ACID

5-FLUORO-6-METHOXY-3-PYRIDINECARBOXYLIC ACID

Product Name: 5-FLUORO-6-METHOXY-3-PYRIDINECARBOXYLIC ACID
CAS No.: 953780-42-2
Chemical Name: 5-FLUORO-6-METHOXY-3-PYRIDINECARBOXYLIC ACID
Synonyms: 5-fluoro-6-methoxynicotinic acid;3-Fluoro-2-methoxy-5-pyridinecarboxylic acid;5-FLUORO-6-METHOXY-3-PYRIDINECARBOXYLIC ACID;5-Fluoro-6-methoxypyridine-3-carboxylic acid;3-Pyridinecarboxylic acid, 5-fluoro-6-methoxy-
CBNumber: CB32455274
Molecular Formula: C7H6FNO3
Formula Weight: 171.13
MOL File: 953780-42-2.mol

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5-FLUORO-6-METHOXY-3-PYRIDINECARBOXYLIC ACID Property

Boiling point:: 275.9±35.0 °C(Predicted)
Density: 1.386±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
pka: 3.40±0.10(Predicted)
Appearance: Off-white to light brown Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: F402545
Product name: 5-Fluoro-6-methoxynicotinicAcid
Packaging: 500mg
Price: $350
Updated: 2021/12/16

AK Scientific

Product number: Z5403
Product name: 5-Fluoro-6-methoxynicotinicacid
Packaging: 250mg
Price: $104
Updated: 2021/12/16

Matrix Scientific

Product number: 126647
Product name: 5-Fluoro-6-methoxynicotinicacid
Purity: >95%
Packaging: 1g
Price: $810
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0361408
Product name: 5-FLUORO-6-METHOXYNICOTINIC ACID
Purity: 95.00%
Packaging: 5MG
Price: $497.26
Updated: 2021/12/16

Chemenu

Product number: CM177630
Product name: 5-Fluoro-6-methoxynicotinicacid
Purity: 95%
Packaging: 10g
Price: $585
Updated: 2021/12/16

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5-FLUORO-6-METHOXY-3-PYRIDINECARBOXYLIC ACID Chemical Properties,Usage,Production

Synthesis

953780-40-0

953780-42-2

General procedure for the synthesis of 5-fluoro-6-methoxynicotinic acid from 5-fluoro-6-methoxynicotinic acid methyl ester: 5-fluoro-6-methoxynicotinic acid methyl ester (3.5 g, 18.9 mmol) and potassium hydroxide (4.2 g, 61.5 mmol) were dissolved in methanol (70 ml), and the reaction was stirred at room temperature for 5 hours. After completion of the reaction, methanol was removed by concentration under reduced pressure, the residue was dissolved in water and the aqueous solution was washed with ether. Subsequently, the aqueous phase was acidified to pH=1 with dilute hydrochloric acid and extracted with ether. The organic layers were combined, washed with saturated brine, dried with anhydrous sodium sulfate, and finally concentrated under reduced pressure to give 5-fluoro-6-methoxynicotinic acid (3.2 g, 98% yield) as a white solid.

References

[1] Patent: WO2007/120729, 2007, A2. Location in patent: Page/Page column 57
[2] Patent: WO2016/51193, 2016, A1. Location in patent: Paragraph 00667; 00674; 00675

5-FLUORO-6-METHOXY-3-PYRIDINECARBOXYLIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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953780-42-2, 5-FLUORO-6-METHOXY-3-PYRIDINECARBOXYLIC ACIDRelated Search:

5-FLUORO-6-METHOXY-3-PYRIDINECARBOXYLIC ACID

3-Fluoro-2-methoxy-5-pyridinecarboxylic acid

5-fluoro-6-methoxynicotinic acid

5-Fluoro-6-methoxypyridine-3-carboxylic acid

3-Pyridinecarboxylic acid, 5-fluoro-6-methoxy-

953780-42-2