5-chloro-4-iodo-2-nitroaniline

Product Name: 5-chloro-4-iodo-2-nitroaniline
CAS No.: 335349-57-0
Chemical Name: 5-chloro-4-iodo-2-nitroaniline
Synonyms: 5-chloro-4-iodo-2-nitroaniline;5-Chloro-4-iodo-2-nitrophenylamine;5-chloro-4-iodo-2-nitrobenzenaMine;Benzenamine, 5-chloro-4-iodo-2-nitro-
CBNumber: CB32545942
Molecular Formula: C6H4ClIN2O2
Formula Weight: 298.47
MOL File: 335349-57-0.mol

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5-chloro-4-iodo-2-nitroaniline Property

Boiling point:: 389.7±42.0 °C(Predicted)
Density: 2.169
storage temp.: 2-8°C(protect from light)
pka: -2.43±0.25(Predicted)
Appearance: Light yellow to yellow Solid

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Safety

HS Code: 2921420090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

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N-Bromosuccinimide Price

TRC

Product number: C380638
Product name: 5-Chloro-4-iodo-2-nitro-phenylamine
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: C380638
Product name: 5-Chloro-4-iodo-2-nitro-phenylamine
Packaging: 100mg
Price: $60
Updated: 2021/12/16

TRC

Product number: C380638
Product name: 5-Chloro-4-iodo-2-nitro-phenylamine
Packaging: 500mg
Price: $200
Updated: 2021/12/16

ChemScene

Product number: CS-0060133
Product name: 5-Chloro-4-iodo-2-nitroaniline
Purity: 97.01%
Packaging: 5g
Price: $105
Updated: 2021/12/16

ChemScene

Product number: CS-0060133
Product name: 5-Chloro-4-iodo-2-nitroaniline
Purity: 97.01%
Packaging: 1g
Price: $33
Updated: 2021/12/16

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5-chloro-4-iodo-2-nitroaniline Chemical Properties,Usage,Production

Synthesis

1635-61-6

335349-57-0

The general procedure for the synthesis of 5-chloro-4-iodo-2-nitroaniline from 2-nitro-5-chloroaniline was as follows: first, a 50 mL round-bottomed flask was prepared and purged with nitrogen to maintain an inert atmosphere. To the flask was added 5-chloro-2-nitroaniline (10 g, 57.95 mmol, 1.00 eq.), acetic acid (100 mL) and N-iodosuccinimide (NIS, 13 g, 57.78 mmol, 1.00 eq.). The reaction mixture was stirred in an oil bath at 50 °C for 3 hours. Upon completion of the reaction, the mixture was poured into 300 mL of water and the resulting solid was collected by filtration. Subsequently, the solid was washed with 200 mL of saturated sodium bicarbonate solution and three times 200 mL of water. Ultimately, 17 g (88% yield) of 5-chloro-4-iodo-2-nitroaniline was obtained as a yellow solid.

References

[1] Synlett, 2008, # 10, p. 1467 - 1470
[2] Bioorganic and Medicinal Chemistry Letters, 2007, vol. 17, # 24, p. 6811 - 6815
[3] MedChemComm, 2013, vol. 4, # 7, p. 1118 - 1123
[4] Patent: US2013/281392, 2013, A1. Location in patent: Paragraph 0148; 0150; 0151
[5] Patent: CN106496037, 2017, A. Location in patent: Paragraph 0026-0028

5-chloro-4-iodo-2-nitroaniline Preparation Products And Raw materials

Raw materials

Preparation Products

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5-chloro-4-iodo-2-nitroaniline Suppliers

China 36 India 1 United States 7 Global 44

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View Lastest Price from 5-chloro-4-iodo-2-nitroaniline manufacturers

Hebei Chuanghai Biotechnology Co., Ltd

Product: 5-chloro-4-iodo-2-nitroaniline 335349-57-0
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 10 mt
Release date: 2024-11-07

Henan Bao Enluo International TradeCo.，LTD

Product: 5-chloro-4-iodo-2-nitroaniline 335349-57-0
Price: US $50.00/kg
Min. Order: 1kg
Purity: 99.9%
Supply Ability: 10000MT
Release date: 2023-08-17

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335349-57-0

C6H4ClIN2O2