ChemicalBook > CAS DataBase List > 3-(9H-Carbazol-9-yl)phenylboronic acid

3-(9H-Carbazol-9-yl)phenylboronic acid

Product Name
3-(9H-Carbazol-9-yl)phenylboronic acid
CAS No.
864377-33-3
Chemical Name
3-(9H-Carbazol-9-yl)phenylboronic acid
Synonyms
3-NBAPC;-9-yL;PF23A;(3-(9H-CarbazoL;3-(9-Carbazolyl)benzeneboronic acid;3-(9H-Carbazol-9-yl)phenylboronic acid;3-(9H-Carbazol-9-yl)phenylboromic acid;3-(9-Carbazolyl)benzeneboronicacid,98%;3-(9H-carbazole-9-yl)phenylboronic acid;3-(9H-Carbazol-9-yl)benzeneboronic Acid
CBNumber
CB32548099
Molecular Formula
C18H14BNO2
Formula Weight
287.12
MOL File
864377-33-3.mol
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3-(9H-Carbazol-9-yl)phenylboronic acid Property

Boiling point:
472.6±51.0 °C(Predicted)
Density 
1.20
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
form 
Powder
pka
8.30±0.10(Predicted)
color 
Off-white
InChI
InChI=1S/C18H14BNO2/c21-19(22)13-6-5-7-14(12-13)20-17-10-3-1-8-15(17)16-9-2-4-11-18(16)20/h1-12,21-22H
InChIKey
IDQUIFLAFFZYEX-UHFFFAOYSA-N
SMILES
B(C1=CC=CC(N2C3=C(C=CC=C3)C3=C2C=CC=C3)=C1)(O)O
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Safety

HS Code 
2933998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TCI Chemical
Product number
C2967
Product name
3-(9H-Carbazol-9-yl)phenylboronic Acid (contains varying amounts of Anhydride)
Packaging
1g
Price
$37
Updated
2025/07/31
TCI Chemical
Product number
C2967
Product name
3-(9H-Carbazol-9-yl)phenylboronic Acid (contains varying amounts of Anhydride)
Packaging
5g
Price
$109
Updated
2025/07/31
TRC
Product number
C176073
Product name
3-(9H-Carbazol-9-yl)phenylboronicacid
Packaging
100mg
Price
$45
Updated
2021/12/16
TRC
Product number
C176073
Product name
3-(9H-Carbazol-9-yl)phenylboronicacid
Packaging
250mg
Price
$55
Updated
2021/12/16
TRC
Product number
C176073
Product name
3-(9H-Carbazol-9-yl)phenylboronicacid
Packaging
500mg
Price
$65
Updated
2021/12/16
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3-(9H-Carbazol-9-yl)phenylboronic acid Chemical Properties,Usage,Production

Chemical Properties

off-white solid

Uses

suzuki reaction

Synthesis

185112-61-2

121-43-7

864377-33-3

General procedure for the synthesis of 3-(9H-carbazol-9-yl)phenylboronic acid from 9-(3-bromophenyl)-9H-carbazole and trimethyl borate: (2) Dissolve 4.00 g of 9-(3-bromophenyl)-9H-carbazole in dry 50 mL of THF, and cool to -78 °C. 6mL (2.4M) of n-butyllithium solution was slowly added and reacted for 1 hour. Subsequently, 1.8 mL of trimethyl borate was added and the reaction continued for 2 hours. The reaction mixture was warmed to room temperature and stirred overnight. After cooling to 0°C, 40 mL of 2.0 M HCl was added for hydrolysis. The reaction mixture was extracted with dichloromethane and the solvent was evaporated to give 2.96 g of 3-(9H-carbazol-9-yl)phenylboronic acid in 83% yield.

References

[1] Patent: CN103588770, 2016, B. Location in patent: Paragraph 0047
[2] Patent: CN107686484, 2018, A. Location in patent: Paragraph 0129-0132
[3] Patent: WO2013/12298, 2013, A1. Location in patent: Paragraph 103-104

3-(9H-Carbazol-9-yl)phenylboronic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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3-(9H-Carbazol-9-yl)phenylboronic acid Suppliers

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View Lastest Price from 3-(9H-Carbazol-9-yl)phenylboronic acid manufacturers

Shanghai Daken Advanced Materials Co.,Ltd
Product
3-(9H-Carbazol-9-yl)phenylboronic acid 864377-33-3
Price
US $0.00/KG
Min. Order
1KG
Purity
98.00%
Supply Ability
150KG /month
Release date
2021-11-17
Henan Fengda Chemical Co., Ltd
Product
3-(9H-Carbazol-9-yl)phenylboronic acid 864377-33-3
Price
US $50.00-1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-22
LY Global chemicals co.,ltd .
Product
3-(9H-Carbazol-9-yl)phenylboronic acid 864377-33-3
Price
US $0.00-0.00/kg
Min. Order
1kg
Purity
98%Min
Supply Ability
1000kg
Release date
2023-03-12

864377-33-3, 3-(9H-Carbazol-9-yl)phenylboronic acidRelated Search:

4-(9H-Carbozol-9-yl)phenylboronic acid Calcium formate (9-(4-BROMOPHENYL))-9H-CARBAZOLE

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