N-[3-(Bromomethyl)benzyl]carbamic acid tert-butyl ester

Product Name: N-[3-(Bromomethyl)benzyl]carbamic acid tert-butyl ester
CAS No.: 220364-34-1
Chemical Name: N-[3-(Bromomethyl)benzyl]carbamic acid tert-butyl ester
Synonyms: tert-Butyl 3-(bromomethyl);3-(Boc-aMinoMethyl)benzylbroMide;tert-Butyl 3-(broMoMethyl)benzylcarbaMate;1-[3-(Bromomethyl)phenyl]-N-Boc-methanamine;3-(tert-Butoxycarbonylaminomethyl)benzyl bromide;[3-(Bromomethyl)benzyl]carbamic acid tert-butyl ester;tert-butyl N-[[3-(bromomethyl)phenyl]methyl]carbamate;N-[3-(Bromomethyl)benzyl]carbamic acid tert-butyl ester;Carbamic acid, N-[[3-(bromomethyl)phenyl]methyl]-, 1,1-dimethylethyl ester
CBNumber: CB32554317
Molecular Formula: C13H18BrNO2
Formula Weight: 300.19
MOL File: 220364-34-1.mol

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N-[3-(Bromomethyl)benzyl]carbamic acid tert-butyl ester Property

Boiling point:: 390.9±30.0 °C(Predicted)
Density: 1.304
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 12.11±0.46(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Matrix Scientific

Product number: 119702
Product name: tert-Butyl 3-(bromomethyl)benzylcarbamate
Purity: 95+%
Packaging: 250mg
Price: $303
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0369905
Product name: TERT-BUTYL-3-(BROMOMETHYL)BENZYLCARBAMATE
Purity: 95.00%
Packaging: 5MG
Price: $498.25
Updated: 2021/12/16

AK Scientific

Product number: Z4426
Product name: tert-Butyl3-(bromomethyl)benzylcarbamate
Packaging: 5g
Price: $1337
Updated: 2021/12/16

Crysdot

Product number: CD12095167
Product name: tert-Butyl3-(bromomethyl)benzylcarbamate
Purity: 98%
Packaging: 1g
Price: $294
Updated: 2021/12/16

Abosyn

Product number: 10-2493
Product name: tert-butyl3-(bromomethyl)benzylcarbamate
Purity: 95%-98%
Packaging: 1g
Price: $756
Updated: 2021/12/16

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N-[3-(Bromomethyl)benzyl]carbamic acid tert-butyl ester Chemical Properties,Usage,Production

Synthesis

226070-69-5

220364-34-1

General procedure for the synthesis of tert-butyl 3-(bromomethyl)benzylcarbamate from tert-butyl (3-hydroxymethyl-benzyl)-carboxylate: Boc-aminomethylbenzyl alcohol (237 mg), triphenylphosphine (485 mg), and carbon tetrabromide (491 mg) were dissolved in dichloromethane (10 mL) and the reaction was stirred at room temperature overnight. After completion of the reaction, the reaction solution was concentrated. The crude product was purified by silica gel column chromatography to afford the target product tert-butyl 3-(bromomethyl)benzylcarbamate (200 mg, 67% yield).

References

[1] Patent: US2006/173183, 2006, A1. Location in patent: Page/Page column 113
[2] Patent: WO2005/18557, 2005, A2. Location in patent: Page/Page column 282-283
[3] Patent: WO2005/18557, 2005, A2. Location in patent: Page/Page column 282-283
[4] Patent: EP1452521, 2004, A1. Location in patent: Page 55

N-[3-(Bromomethyl)benzyl]carbamic acid tert-butyl ester Preparation Products And Raw materials

Raw materials

Preparation Products

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N-[3-(Bromomethyl)benzyl]carbamic acid tert-butyl ester Suppliers

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220364-34-1, N-[3-(Bromomethyl)benzyl]carbamic acid tert-butyl esterRelated Search:

[3-(Bromomethyl)benzyl]carbamic acid tert-butyl ester

N-[3-(Bromomethyl)benzyl]carbamic acid tert-butyl ester

tert-Butyl 3-(broMoMethyl)benzylcarbaMate

3-(Boc-aMinoMethyl)benzylbroMide

tert-Butyl 3-(bromomethyl)

tert-butyl N-[[3-(bromomethyl)phenyl]methyl]carbamate

3-(tert-Butoxycarbonylaminomethyl)benzyl bromide

Carbamic acid, N-[[3-(bromomethyl)phenyl]methyl]-, 1,1-dimethylethyl ester

1-[3-(Bromomethyl)phenyl]-N-Boc-methanamine

220364-34-1