7-broMoquinolin-3-aMine

Product Name: 7-broMoquinolin-3-aMine
CAS No.: 1266322-58-0
Chemical Name: 7-broMoquinolin-3-aMine
Synonyms: 7-broMoquinolin-3-aMine;3-Amino-7-bromoquinoline;3-Quinolinamine, 7-bromo-
CBNumber: CB32582897
Molecular Formula: C9H7BrN2
Formula Weight: 223.07
MOL File: 1266322-58-0.mol

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7-broMoquinolin-3-aMine Property

storage temp.: 2-8°C(protect from light)
Appearance: White to light brown Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Warning
Hazard statements: H315Causes skin irritation
Precautionary statements: P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: B998985
Product name: 7-bromoquinolin-3-amine
Packaging: 100mg
Price: $265
Updated: 2021/12/16

AK Scientific

Product number: 5261AA
Product name: 7-Bromoquinolin-3-amine
Packaging: 1g
Price: $475
Updated: 2021/12/16

AK Scientific

Product number: 5261AA
Product name: 7-Bromoquinolin-3-amine
Packaging: 250mg
Price: $219
Updated: 2021/12/16

Alichem

Product number: 1266322580
Product name: 7-Bromoquinolin-3-amine
Packaging: 1g
Price: $589.36
Updated: 2021/12/16

Alichem

Product number: 1266322580
Product name: 7-Bromoquinolin-3-amine
Packaging: 5g
Price: $1633.66
Updated: 2021/12/16

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7-broMoquinolin-3-aMine Chemical Properties,Usage,Production

Synthesis

1375108-38-5

1266322-58-0

b) Synthesis of 7-bromoquinolin-3-amine: 2-(7-bromoquinolin-3-yl)isoindoline-1,3-dione (10 g, 28.3 mmol) was suspended in ethanol (200 mL), hydrazine (1.777 mL, 56.6 mmol) was added, followed by heating and refluxing for 1 hour. After completion of the reaction, the mixture was allowed to cool to room temperature and the precipitate was collected and washed with a small amount of ethanol. The filtrate was concentrated to dryness to give a gray solid. The resulting solid was dissolved in warm ethanol and adsorbed on silica gel. Purification by silica gel column chromatography (eluent: 50-100% ethyl acetate/hexane gradient) afforded the target compound 7-bromoquinolin-3-amine (3.5 g, 56% yield).1H NMR (400 MHz, DMSO-d6) δ ppm: 5.83 (s, 2H), 7.14 (d, J = 2.53 Hz, 1H), 7.49 (dd, J = 8.84, 2.02Hz, 1H), 7.54-7.65 (m, 1H), 7.94 (d, J = 1.77Hz, 1H), 8.46 (d, J = 2.78Hz, 1H).

References

[1] Patent: WO2017/32840, 2017, A1. Location in patent: Page/Page column 265; 266
[2] Patent: WO2013/28447, 2013, A1. Location in patent: Page/Page column 117
[3] Patent: WO2013/52716, 2013, A1. Location in patent: Page/Page column 63
[4] Patent: WO2013/177253, 2013, A2. Location in patent: Page/Page column 64
[5] Patent: WO2014/8223, 2014, A2. Location in patent: Page/Page column 71-72

7-broMoquinolin-3-aMine Preparation Products And Raw materials

Raw materials

Preparation Products

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7-broMoquinolin-3-aMine Suppliers

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View Lastest Price from 7-broMoquinolin-3-aMine manufacturers

Career Henan Chemical Co

Product: 7-broMoquinolin-3-aMine 1266322-58-0
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 200g
Release date: 2020-02-01

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1266322-58-0