ChemicalBook > CAS DataBase List > α,β-1-Methyl-D-ribofuranoside

α,β-1-Methyl-D-ribofuranoside

Product Name
α,β-1-Methyl-D-ribofuranoside
CAS No.
13039-63-9
Chemical Name
α,β-1-Methyl-D-ribofuranoside
Synonyms
(2R,3S,4R)-2-(Hydroxymethyl)-5-methoxytetrahydrofuran-3,4-diol;Methyl D-ribofuranoside(α and β mixture);AzacitidineImpurity46;α,β-1-Methyl-D-ribofuranoside;α,β-1-Methyl-D-ribofuranoside;(2R,3S,4R)-2-(Hydroxymethyl)-5-methoxytetrahydrofuran-3,4-diol(α and β mixture)
CBNumber
CB32603556
Molecular Formula
C6H12O5
Formula Weight
164.16
MOL File
13039-63-9.mol
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α,β-1-Methyl-D-ribofuranoside Property

storage temp. 
Sealed in dry,Room Temperature
Stability:
Hygroscopic
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific
Product number
5558AA
Product name
(2R,3S,4R)-2-(Hydroxymethyl)-5-methoxytetrahydrofuran-3,4-diol
Packaging
5g
Price
$492
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CRB0005204
Product name
(2R,3S,4R)-2-(HYDROXYMETHYL)-5-METHOXYTETRAHYDROFURAN-3,4-DIOL
Purity
95.00%
Packaging
5MG
Price
$497.57
Updated
2021/12/16
Ambeed
Product number
A134503
Product name
MethylD-ribofuranoside(αandβmixture)
Purity
97%
Packaging
250mg
Price
$113
Updated
2021/12/16
Chemenu
Product number
CM196174
Product name
(2R,3S,4R)-2-(hydroxymethyl)-5-methoxytetrahydrofuran-3,4-diol
Purity
95%
Packaging
1g
Price
$122
Updated
2021/12/16
Arctom
Product number
SY111642
Product name
(2R,3S,4R)-2-(Hydroxymethyl)-5-methoxytetrahydrofuran-3,4-diol
Purity
≥95%
Packaging
5g
Price
$320
Updated
2021/12/16
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α,β-1-Methyl-D-ribofuranoside Chemical Properties,Usage,Production

Uses

Methyl D-Ribofuranoside is used in the preparation of antiviral nucleosides and derivatives thereof.

Synthesis

67-56-1

532-20-7

1824-96-0

General procedure for the synthesis of methyl α-D-xylofuranoside from methanol and 2-furancarboxylic acid (CAS:532-20-7): D-ribose (500 g, 3.33 mol) was dissolved in 1.5 L of anhydrous methanol containing 0.5% (v/v) hydrochloric acid, and the reaction system was placed in a round-bottomed flask fitted with a drying tube of calcium carbonate, and the reaction was stirred for 48 h at room temperature. Upon completion of the reaction, the pH of the reaction mixture was adjusted to 7 using Dowex (OH type) ion exchange resin to neutralize the acidity. Subsequently, the resin was removed by filtration, the filtrate was concentrated under reduced pressure to remove the solvent, and the resulting residue was dried under vacuum overnight to afford methyl α-D-xylofuranoside (550 g, 98% yield).

References

[1] European Journal of Organic Chemistry, 2006, # 14, p. 3152 - 3168
[2] Angewandte Chemie - International Edition, 2017, vol. 56, # 39, p. 11963 - 11965
[3] Angew. Chem., 2017, vol. 129, # 39, p. 12125 - 12127,3
[4] Tetrahedron, 1992, vol. 48, # 41, p. 9033 - 9072
[5] Patent: WO2005/27962, 2005, A1. Location in patent: Page/Page column 69-70

α,β-1-Methyl-D-ribofuranoside Preparation Products And Raw materials

Raw materials

Preparation Products

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α,β-1-Methyl-D-ribofuranoside Suppliers

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13039-63-9, α,β-1-Methyl-D-ribofuranosideRelated Search:


  • α,β-1-Methyl-D-ribofuranoside
  • (2R,3S,4R)-2-(Hydroxymethyl)-5-methoxytetrahydrofuran-3,4-diol
  • Methyl D-ribofuranoside(α and β mixture)
  • (2R,3S,4R)-2-(Hydroxymethyl)-5-methoxytetrahydrofuran-3,4-diol(α and β mixture)
  • AzacitidineImpurity46
  • α,β-1-Methyl-D-ribofuranoside
  • 13039-63-9