6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one
- Product Name
- 6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one
- CAS No.
- 32263-70-0
- Chemical Name
- 6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one
- Synonyms
- 6-benzyloxytetralone;oxy)-3,4-dihydronaphthaL;6-Benzyloxy-3,4-dihydro-2H-naphthalen-1-one;6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one;6-(Benzyloxy)-3,4-dihydro-1(2H)-naphthalenone;6-phenylmethoxy-3,4-dihydro-2H-naphthalen-1-one;6-(benzyloxy)-1,2,3,4-tetrahydronaphthalen-1-one;1(2H)-Naphthalenone, 3,4-dihydro-6-(phenylMethoxy)-
- CBNumber
- CB32610013
- Molecular Formula
- C17H16O2
- Formula Weight
- 252.31
- MOL File
- 32263-70-0.mol
6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one Property
- Melting point:
- 96-99 °C(Solv: cyclohexane (110-82-7))
- Boiling point:
- 433.4±34.0 °C(Predicted)
- Density
- 1.160±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Light brown to brown Solid
- InChI
- InChI=1S/C17H16O2/c18-17-8-4-7-14-11-15(9-10-16(14)17)19-12-13-5-2-1-3-6-13/h1-3,5-6,9-11H,4,7-8,12H2
- InChIKey
- SAYPPJQQGVXKAP-UHFFFAOYSA-N
- SMILES
- C1(=O)C2=C(C=C(OCC3=CC=CC=C3)C=C2)CCC1
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- FB141115
- Product name
- 6-(Benzyloxy)-3,4-dihydronaphthalen-1(2H)-one
- Packaging
- 500mg
- Price
- $85
- Updated
- 2021/12/16
- Product number
- FB141115
- Product name
- 6-(Benzyloxy)-3,4-dihydronaphthalen-1(2H)-one
- Packaging
- 1g
- Price
- $135
- Updated
- 2021/12/16
- Product number
- FB141115
- Product name
- 6-(Benzyloxy)-3,4-dihydronaphthalen-1(2H)-one
- Packaging
- 2g
- Price
- $210
- Updated
- 2021/12/16
- Product number
- FB141115
- Product name
- 6-(Benzyloxy)-3,4-dihydronaphthalen-1(2H)-one
- Packaging
- 5G
- Price
- $410
- Updated
- 2021/12/16
- Product number
- FB141115
- Product name
- 6-(Benzyloxy)-3,4-dihydronaphthalen-1(2H)-one
- Packaging
- 10g
- Price
- $650
- Updated
- 2021/12/16
6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one Chemical Properties,Usage,Production
Synthesis
3470-50-6
100-39-0
32263-70-0
General procedure: 6-hydroxy-1-tetralone (0.3 g, 1.85 mmol) was suspended in acetone (15 mL) containing K2CO3 (3.70 mmol). Benzyl bromide (2.035 mmol) was added to the reaction mixture and heated under reflux conditions for 6 hours. The reaction process was monitored by silica gel thin layer chromatography (TLC) using ethyl acetate with petroleum ether (1:2) as mobile phase. Upon completion of the reaction, the mixture was filtered through a diatomaceous earth pad and the filtrate was subsequently concentrated under vacuum. The resulting crude product was purified by recrystallization from cyclohexane to give 6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one.
References
[1] Bioorganic and Medicinal Chemistry Letters, 2014, vol. 24, # 12, p. 2758 - 2763
[2] Bioorganic and Medicinal Chemistry Letters, 2014, vol. 24, # 12, p. 2758 - 2763
[3] Patent: US2018/155322, 2018, A1. Location in patent: Paragraph 1502; 1503
[4] European Journal of Organic Chemistry, 2003, # 15, p. 2799 - 2812
[5] Bioorganic and Medicinal Chemistry Letters, 2012, vol. 22, # 1, p. 144 - 148
6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one Preparation Products And Raw materials
Raw materials
Preparation Products
6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one Suppliers
- Tel
- 13658618215
- 308410472@qq.com
- Country
- China
- ProdList
- 58
- Advantage
- 58
- Tel
- 512-62857507
- sales@sinorarechem.com
- Country
- China
- ProdList
- 690
- Advantage
- 58
- Tel
- 0571-86828652 18857119830
- Fax
- 0571-83522824
- sales@chemtrue-bio.com
- Country
- China
- ProdList
- 252
- Advantage
- 58
- Tel
- 021-021-58432009 400-005-6266
- Fax
- 021-58436166
- sales8178@energy-chemical.com
- Country
- China
- ProdList
- 44801
- Advantage
- 61
- Tel
- 28-83379370 13880556291
- Fax
- 028-87747383
- tcy@tcypharm.com
- Country
- China
- ProdList
- 510
- Advantage
- 57
- Tel
- 13526569071
- sales@leadmedpharm.com
- Country
- China
- ProdList
- 7892
- Advantage
- 64
- Tel
- +86-021-54824098 15317552526
- Fax
- 021-54824069
- sales@chemzq.com
- Country
- China
- ProdList
- 254
- Advantage
- 55
- Tel
- +86057186818502 13588463833
- Fax
- Pls mail us for more information!
- info@sagechem.com
- Country
- China
- ProdList
- 10266
- Advantage
- 58
- Tel
- 15928766785 15928766785
- Fax
- QQ961458712
- wupengcheng@astatech.cn
- Country
- China
- ProdList
- 1987
- Advantage
- 55
- Tel
- +86-021-61727342 13611721451
- Fax
- 021-61294107
- chainpharm@163.com
- Country
- China
- ProdList
- 980
- Advantage
- 58
View Lastest Price from 6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one manufacturers
- Product
- 6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one 32263-70-0
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 500000kg
- Release date
- 2024-11-04
- Product
- 6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one 32263-70-0
- Price
- US $9.80-8.00/KG
- Min. Order
- 1KG
- Purity
- 95%~99.99%
- Supply Ability
- 10 MT/ Month
- Release date
- 2020-10-28
- Product
- 6-(benzyloxy)-3,4-dihydronaphthalen-1(2H)-one 32263-70-0
- Price
- US $30.00-10.00/kg
- Min. Order
- 10kg
- Purity
- 99%
- Supply Ability
- 100000kg
- Release date
- 2024-08-14