2-(broMoMethyl)-6-Methoxypyridine
- Product Name
- 2-(broMoMethyl)-6-Methoxypyridine
- CAS No.
- 156094-63-2
- Chemical Name
- 2-(broMoMethyl)-6-Methoxypyridine
- Synonyms
- -6-methoxypyridine;2-(broMoMethyl)-6-Methoxypyridine;Pyridine, 2-(bromomethyl)-6-methoxy-
- CBNumber
- CB32616792
- Molecular Formula
- C7H8BrNO
- Formula Weight
- 202.05
- MOL File
- 156094-63-2.mol
2-(broMoMethyl)-6-Methoxypyridine Property
- Boiling point:
- 229.3±25.0 °C(Predicted)
- Density
- 1.484±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 1.61±0.12(Predicted)
- Appearance
- Colorless to light yellow Liquid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H301Toxic if swalloed
H315Causes skin irritation
H318Causes serious eye damage
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B847143
- Product name
- 2-(Bromomethyl)-6-methoxypyridine
- Packaging
- 10mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- HCH0363350
- Product name
- 2-(BROMOMETHYL)-6-METHOXYPYRIDINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $498.8
- Updated
- 2021/12/16
- Product number
- A152844
- Product name
- 2-(Bromomethyl)-6-methoxypyridine
- Purity
- 98%
- Packaging
- 100mg
- Price
- $39
- Updated
- 2021/12/16
- Product number
- A152844
- Product name
- 2-(Bromomethyl)-6-methoxypyridine
- Purity
- 98%
- Packaging
- 250mg
- Price
- $67
- Updated
- 2021/12/16
- Product number
- A152844
- Product name
- 2-(Bromomethyl)-6-methoxypyridine
- Purity
- 98%
- Packaging
- 1g
- Price
- $175
- Updated
- 2021/12/16
2-(broMoMethyl)-6-Methoxypyridine Chemical Properties,Usage,Production
Synthesis
63071-03-4
156094-63-2
Under nitrogen protection, 1.07 g (6.01 mmol) of N-bromosuccinimide (NBS) and 49.3 mg (0.300 mmol) of azobisisobutyronitrile (AIBN) were dissolved in 8 mL of carbon tetrachloride (CCl4). Subsequently, the mixture was heated to reflux and 0.73 mL (6.00 mmol) of 2-methoxy-6-methylpyridine was slowly added. After keeping the reaction at reflux for 8 hours in an oil bath, the reaction mixture was cooled to room temperature. The crude product was concentrated under reduced pressure and purified by silica gel column chromatography [eluent: chloroform/hexane = 1:1 (v/v)] to afford 619 mg (66% yield) of the target compound 2-(bromomethyl)-6-methoxypyridine as a colorless liquid.1H NMR (400 MHz, CDCl3) δ 7.55 (dd, J = 8.2 Hz, J = 7.3 Hz, 1H ), 7.32 (d, J = 7.3 Hz, 1H), 6.99 (d, J = 8.2 Hz, 1H), 4.56 (s, 2H), 3.94 (s, 3H).
References
[1] Bulletin of the Chemical Society of Japan, 2015, vol. 88, # 7, p. 963 - 965
2-(broMoMethyl)-6-Methoxypyridine Preparation Products And Raw materials
Raw materials
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