2-(broMoMethyl)-6-Methoxypyridine

Product Name: 2-(broMoMethyl)-6-Methoxypyridine
CAS No.: 156094-63-2
Chemical Name: 2-(broMoMethyl)-6-Methoxypyridine
Synonyms: -6-methoxypyridine;2-(broMoMethyl)-6-Methoxypyridine;Pyridine, 2-(bromomethyl)-6-methoxy-
CBNumber: CB32616792
Molecular Formula: C7H8BrNO
Formula Weight: 202.05
MOL File: 156094-63-2.mol

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2-(broMoMethyl)-6-Methoxypyridine Property

Boiling point:: 229.3±25.0 °C(Predicted)
Density: 1.484±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 1.61±0.12(Predicted)
Appearance: Colorless to light yellow Liquid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H301Toxic if swalloed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B847143
Product name: 2-(Bromomethyl)-6-methoxypyridine
Packaging: 10mg
Price: $65
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0363350
Product name: 2-(BROMOMETHYL)-6-METHOXYPYRIDINE
Purity: 95.00%
Packaging: 5MG
Price: $498.8
Updated: 2021/12/16

Ambeed

Product number: A152844
Product name: 2-(Bromomethyl)-6-methoxypyridine
Purity: 98%
Packaging: 5g
Price: $593
Updated: 2021/12/16

Ambeed

Product number: A152844
Product name: 2-(Bromomethyl)-6-methoxypyridine
Purity: 98%
Packaging: 100mg
Price: $39
Updated: 2021/12/16

Ambeed

Product number: A152844
Product name: 2-(Bromomethyl)-6-methoxypyridine
Purity: 98%
Packaging: 250mg
Price: $67
Updated: 2021/12/16

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2-(broMoMethyl)-6-Methoxypyridine Chemical Properties,Usage,Production

Synthesis

63071-03-4

156094-63-2

Under nitrogen protection, 1.07 g (6.01 mmol) of N-bromosuccinimide (NBS) and 49.3 mg (0.300 mmol) of azobisisobutyronitrile (AIBN) were dissolved in 8 mL of carbon tetrachloride (CCl4). Subsequently, the mixture was heated to reflux and 0.73 mL (6.00 mmol) of 2-methoxy-6-methylpyridine was slowly added. After keeping the reaction at reflux for 8 hours in an oil bath, the reaction mixture was cooled to room temperature. The crude product was concentrated under reduced pressure and purified by silica gel column chromatography [eluent: chloroform/hexane = 1:1 (v/v)] to afford 619 mg (66% yield) of the target compound 2-(bromomethyl)-6-methoxypyridine as a colorless liquid.1H NMR (400 MHz, CDCl3) δ 7.55 (dd, J = 8.2 Hz, J = 7.3 Hz, 1H ), 7.32 (d, J = 7.3 Hz, 1H), 6.99 (d, J = 8.2 Hz, 1H), 4.56 (s, 2H), 3.94 (s, 3H).

References

[1] Bulletin of the Chemical Society of Japan, 2015, vol. 88, # 7, p. 963 - 965

2-(broMoMethyl)-6-Methoxypyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(broMoMethyl)-6-Methoxypyridine Suppliers

China 42 Germany 1 India 1 United States 3 Global 47

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156094-63-2, 2-(broMoMethyl)-6-MethoxypyridineRelated Search:

2-(broMoMethyl)-6-Methoxypyridine

-6-methoxypyridine

Pyridine, 2-(bromomethyl)-6-methoxy-

156094-63-2