3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde
Uses- Product Name
- 3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde
- CAS No.
- 269058-49-3
- Chemical Name
- 3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde
- Synonyms
- 3-BROMO-6-METHOXYPICOLINALDEHYDE;3-bromo-2-formyl-6-methoxypyridine;3-Bromo-6-methoxy-pyridine-2-carbaldehyde;3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde;2-Pyridinecarboxaldehyde, 3-bromo-6-methoxy-
- CBNumber
- CB32629903
- Molecular Formula
- C7H6BrNO2
- Formula Weight
- 216.03
- MOL File
- 269058-49-3.mol
3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde Property
- Boiling point:
- 253.3±35.0 °C(Predicted)
- Density
- 1.606±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- -0.16±0.10(Predicted)
- Appearance
- Off-white to light yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
N-Bromosuccinimide Price
- Product number
- B429353
- Product name
- 3-bromo-6-methoxypicolinaldehyde
- Packaging
- 500mg
- Price
- $310
- Updated
- 2021/12/16
- Product number
- FB143420
- Product name
- 3-Bromo-6-methoxypicolinaldehyde
- Packaging
- 1g
- Price
- $324
- Updated
- 2021/12/16
- Product number
- 119826
- Product name
- 3-Bromo-6-methoxypicolinaldehyde
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $540
- Updated
- 2021/12/16
- Product number
- FB143420
- Product name
- 3-Bromo-6-methoxypicolinaldehyde
- Packaging
- 2g
- Price
- $563
- Updated
- 2021/12/16
- Product number
- Z4526
- Product name
- 3-Bromo-6-methoxypicolinaldehyde
- Packaging
- 100mg
- Price
- $89
- Updated
- 2021/12/16
3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde Chemical Properties,Usage,Production
Uses
3-bromo-6-methoxypicolinaldehyde is a useful research chemical.
Synthesis
623942-84-7
269058-49-3
Step F. Synthesis of 3-bromo-6-methoxy-2-pyridinecarboxaldehyde. A mixture of 3-bromo-2-hydroxymethyl-6-methoxypyridine (3.25 g, 14.9 mmol) and manganese dioxide (9.07 g, 104 mmol) in chloroform (50 mL) was heated to reflux for 18 hours. After completion of the reaction, the reaction mixture was filtered while hot and the filtrate was concentrated. The residue was purified by silica gel column chromatography (eluent: 10% ethyl acetate/hexane) to afford 3-bromo-6-methoxy-2-pyridinecarboxaldehyde (2.55 g, 80% yield). Mass spectrum (ESI): calculated value C7H6BrNO2, 214.96; measured value m/z 218.2 [M + H]+. 1H NMR (CDCl3): δ 10.13 (s, 1H), 7.80 (d, J = 8.7 Hz, 1H), 6.83 (d, J = 8.7 Hz, 1H), 3.99 (s, 3H).
References
[1] Tetrahedron Letters, 2000, vol. 41, # 12, p. 2007 - 2009
[2] Organic and Biomolecular Chemistry, 2003, vol. 1, # 16, p. 2865 - 2876
[3] Patent: US2006/287292, 2006, A1. Location in patent: Page/Page column 29
[4] Patent: US2016/75711, 2016, A1. Location in patent: Paragraph 0570; 0574
3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde Preparation Products And Raw materials
Raw materials
Preparation Products
3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde Suppliers
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View Lastest Price from 3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde manufacturers
- Product
- 3-BroMo-6-Methoxy-2-pyridinecarboxaldehyde 269058-49-3
- Price
- US $8.00-1.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-04-03